Fluid measuring apparatus

• US 4,109,510 A
• Filed: 04/14/1977
• Issued: 08/29/1978
• Est. Priority Date: 04/14/1977
• Status: Expired due to Term

• Current Assignee: Jerome A. Rodder
• Original Assignee: Jerome A. Rodder
• Inventors: Rodder, Jerome A.
• Primary Examiner(s): Queisser, Richard C.
• Assistant Examiner(s): Kreitman, Stephen A.
• Application Number:
  US05/787,468
• Time in Patent Office: 502 Days
• Field of Search: 73/27 R, 73/204, 338/34, 338/318
• US Class Current: 73/23.4
• CPC Class Codes: G01F 1/684 Structural arrangements; Mounting of elements, e.g. in relation to fluid flow
• CPC Class Codes: G01F 1/69 of resistive type
• CPC Class Codes: G01N 27/18 caused by changes in the thermal conductivity of a surrounding material to be tested G01N27/20 takes precedence
• CPC Class Codes: G01N 30/66 Thermal conductivity detectors

Abstract

A housing has elongated cavities in which four hot wires forming the arms of a bridge are disposed. Each hot wire comprises a first segment bent in half to extend along the length of the cavity away from a junction, and a second segment bent in half to extend along the length of the cavity away from the junction in the opposite direction from the first segment. The junction is centrally located relative to the ends of the cavity. The first and second segments are electrically connected to each other at one end and are electrically connected to other hot wires in the bridge at the other end by a printed circuit board at the junction. The middle of each segment is wrapped around first and second closely spaced rods deformed to exert tension on the segment. The circuit board is located in a chamber having a larger cross section than the cavities. In using the apparatus for chromatography, unknown gases in a carrier enter one of the cavities near the chamber. A reference gas enters the chamber to prevent the unknown gases from flowing to the chamber. The gases exit from the ends of the cavity.

Claims

1. Fluid measuring apparatus comprising:

a housing having an elongated cavity enclosed on its sides;

a first thin elongated hot wire bent in half to extend along the length of the cavity away from a junction;

a second thin elongated hot wire bent in half to extend along the length of the cavity away from the junction;

first means at the junction for supporting the ends of each hot wire in spaced electrically isolated relationship from each other and connecting one end of the first and second hot wires to each other to form in effect a first single hot wire equal in length to the first and second hot wires;

second means spaced along the length of the cavity from the junction for supporting the middle of the first hot wire to exert tension thereon as the length of the first hot wire changes;

third means spaced along the length of the cavity from the junction for supporting the middle of the second hot wire to exert tension thereon as the length of the second hot wire changes;

means for forming in the housing a fluid entrance to the cavity;

means for forming in the housing a fluid exit from the cavity longitudinally spaced from the entrance so the hot wires lie between the entrance and the exit; and

means for measuring the change in resistance of the hot wires.

2. The apparatus of claim 1, in which the junction is centrally located relative to the ends of the cavity, the first hot wire extends in one direction from the junction, the second hot wire extends in the opposite direction from the junction, the second supporting means is located near one end of the cavity, and the third supporting means is located near the other end of the cavity.

3. The apparatus of claim 2, in which the first supporting means supports the ends of each of the first and second hot wires in fixed relationship longitudinally and laterally with respect to each other.

4. The apparatus of claim 3, in which the first supporting means comprises a printed circuit board having a first electrically conductive pad to which one end of each of the first and second hot wires is soldered, a second electrically conductive pad to which the other end of the first hot wire is soldered, and a third electrically conductive pad to which the other end of the second hot wire is soldered, the pads being electrically isolated from each other.

5. The apparatus of claim 4, in which the circuit board is circular and the pads are arcuate and concentric.

6. The apparatus of claim 5, in which the second and third supporting means each comprise a pair of closely spaced rods around which the middle of the respective hot wires are wrapped, the rod pairs being deformed to exert tension on the respective hot wires to keep the corresponding hot wires taut as their length changes.

7. The apparatus of claim 6, in which the rods are spaced to support the halves of the corresponding hot wire parallel to each other.

8. The fluid measuring apparatus of claim 7, additionally comprising:

a third thin elongated hot wire bent in half to extend along the length of the cavity away from the junction;

a fourth thin elongated hot wire bent in half to extend along the length of the cavity away from the junction in the opposite direction from the third hot wire;

fourth means at the junction for supporting the ends of each of the third and fourth hot wires in spaced electrically isolated relationship from each other and from the first and second hot wires, and electrically connecting one end of the third and fourth hot wires to each other to form in effect a second single hot wire equal in length to the third and fourth hot wires;

fifth means spaced along the length of the cavity from the junction for supporting the middle of the third hot wire to exert tension thereon as the length of the third hot wire changes;

sixth means spaced along the length of the cavity from the junction for supporting the middle of the fourth hot wire to exert tension thereon as the length of the fourth hot wire changes;

a source of electrical excitation energy having first and second output terminals;

first and second bridge balancing resistors;

means for connecting the first single hot wire and the first resistor in series with the first single hot wire connected to the first output terminal and the first resistor connected to the second output terminal; and

means for connecting the second single hot wire and the second resistor in series with the second single hot wire connected to the second output terminal and the second resistor connected to the first output terminal, whereby the first and second single hot wires and the first and second resistors form a bridge having an output between the junction of the first single hot wire and the first resistor and the junction of the second single hot wire and the second resistor.

9. The apparatus of claim 8 additionally comprising:

a chamber wider than the first cavity, the circuit board being located in the chamber and the means for forming a fluid entrance comprising a first conduit leading to the chamber and a second conduit leading to the cavity near the chamber;

a source of one or more unknown gases in a carrier gas;

means for connecting the source to the second conduit; and

means for coupling the carrier gas without unknown gases to the first conduit to prevent the one or more unknown gases from flowing to the chamber.

10. The apparatus of claim 1, in which the second and third supporting means each comprise a pair of closely spaced rods around which the middle of the respective hot wires are wrapped, the rod pairs being deformed to exert tension on the respective hot wires to keep the corresponding hot wires taut as their length changes.

11. The apparatus of claim 1, additionally comprising:

a chamber wider than the first cavity at the junction, the means for forming a fluid entrance comprising a first conduit leading to the chamber and a second conduit leading to the cavity near the chamber;

a source of one or more unknown gases in a carrier gas;

means for connecting the source to the second conduit; and

means for coupling the carrier gas without unknown gases to the first conduit to prevent the one or more unknown gases from flowing to the chamber.

12. The fluid measuring apparatus of claim 2, additionally comprising:

a third thin elongated hot wire bent in half to extend along the length of the cavity away from the junction;

a fourth thin elongated hot wire bent in half to extend along the length of the cavity away from the junction in the opposite direction from the third hot wire;

fourth means at the junction for supporting the ends of each of the third and fourth hot wires in spaced electrically isolated relationship from each other and from the first and second hot wires, and electrically connecting one end of the third and fourth hot wires to each other to form in effect a second single hot wire equal in length to the third and fourth hot wires;

fifth means spaced along the length of the cavity from the junction for supporting the middle of the third hot wire to exert tension thereon as the length of the third hot wire changes;

sixth means spaced along the length of the cavity from the junction for supporting the middle of the fourth hot wire to exert tension thereon as the length of the fourth hot wire changes;

a source of electrical excitation energy having first and second output terminals;

first and second bridge balancing resistors;

means for connecting the first single hot wire and the first resistor in series with the first single hot wire connected to the first output terminal and the first resistor connected to the second output terminal; and

means for connecting the second single hot wire and the second resistor in series with the second single hot wire connected to the second output terminal and the second resistor connected to the first output terminal, whereby the first and second single hot wires and the first and second resistors form a bridge having an output between the junction of the first single hot wire and the first resistor and the junction of the second single hot wire and the second resistor.

13. The apparatus of claim 12, in which

the first resistor comprises:

a second elongated cavity enclosed on its sides in the housing;

a fifth thin elongated hot wire bent in half to extend along the length of the second cavity away from a second junction centrally located relative to the ends of the second cavity;

a sixth thin elongated hot wire bent in half to extend along the length of the second cavity away from the second junction in the opposite direction from the fifth hot wire;

seventh means at the second junction supporting the ends of each of the fifth and sixth hot wires in spaced electrically isolated relationship from each other and electrically connecting one end of the fifth and sixth hot wires to each other to form in effect as the first resistor a single hot wire equal in length to the fifth and sixth hot wires;

eighth means spaced along the length of the second cavity from the second junction for supporting the middle of the fifth hot wire to exert tension thereon as the length of the fifth hot wire changes; and

ninth means spaced along the length of the second cavity from the second junction for supporting the middle of the sixth hot wire to exert tension thereon as the length of the sixth hot wire changes;

and the second resistor comprises;

a seventh thin elongated hot wire bent in half to extend along the length of the second cavity away from the second junction;

an eighth thin elongated hot wire bent in half to extend along the length of the second cavity away from the second junction in the opposite direction from the seventh hot wire;

tenth means at the second junction for supporting the ends of each of the seventh and eighth hot wires in spaced electrically isolated relationship from each other and from the fifth and sixth hot wires, and, electrically connecting one end of the seventh and eighth hot wires to each other to form in effect as the second resistor a single hot wire equal in length to the seventh and eighth hot wires;

eleventh means spaced along the length of the second cavity from the second junction for supporting the middle of the seventh hot wire to exert tension thereon as the length of the seventh hot wire changes; and

twelfth means spaced along the length of the second cavity from the second junction for supporting the middle of the eighth hot wire to exert tension thereon as the length of the eighth hot wire changes.

14. The apparatus of claim 12, in which the first and fourth supporting means comprise a printed circuit board having on one surface a first electrically conductive pad to which one end of each of the first and second hot wires is soldered, a second electrically conductive pad to which one end of the first hot wire is soldered, a third electrically conductive pad to which the other end of the second hot wire is soldered, a fourth electrically conductive pad to which one end of each of the third and fourth hot wires is soldered, a fifth electrically conductive pad to which the other end of the third hot wire is soldered, and a sixth electrically conductive pad to which the other end of the fourth hot wire is soldered, the pads being electrically isolated from each other.

15. The apparatus of claim 14, in which the printed circuit board is circular, the pads are arcuate and concentric, and the first and fourth pads surround the second, third, fifth, and sixth pads.

16. The apparatus of claim 15, additionally comprising seventh, eighth, ninth, and tenth mutually isolated pads on the surface of the printed circuit board opposite the one surface and plated through holes connecting the second, third, fifth, and sixth pads respectively with the seventh, eighth, ninth, and tenth pads.

17. Fluid measuring apparatus comprising:

a housing having an elongated cavity enclosed on its sides;

a thin elongated hot wire bent in half to extend along the length of the cavity;

means at one area of the cavity for supporting the ends of the hot wire in closely spaced, electrically isolated relationship from each other;

first and second closely spaced rods at another area of the cavity spaced from the one area to support the middle of the wire, the middle of the wire being wrapped around the rods and the rods being deformed to exert tension on the hot wire to keep the hot wire taut as its length changes;

means for maintaining the spacing of the first and second rods;

means for forming in the housing a fluid entrance to the cavity;

means for forming in the housing a fluid exit from the cavity longitudinally spaced from the entrance so the hot wire lies between the entrance and the exit; and

means for measuring the change in resistance of the hot wire.

18. The fluid measuring apparatus of claim 17, in which the rods are spaced apart a distance to maintain the halves of the hot wire in parallel relationship.

19. Gas chromatographic apparatus comprising:

a housing having a first elongated cavity and a second elongated cavity;

a chamber at one end of the first cavity having a cross section larger in area than the first cavity;

a first thin elongated hot wire extending along the length of the first cavity;

first means in the chamber for supporting the first hot wire in spaced relationship from the sides of the cavity;

second means at an area of the cavity spaced from the chamber for supporting the first hot wire in spaced relationship from the sides of the cavity;

means for forming in the housing a fluid entrance to the chamber;

means for forming in the housing near the chamber a fluid entrance to the first cavity;

means for forming in the housing a fluid exit from the first cavity longitudinally spaced from the entrance to the first cavity so the hot wire lies between the entrance to the first cavity and the exit from the first cavity;

a second thin elongated hot wire supported to extend along the length of the second cavity in spaced relationship from the sides thereof;

means for forming in the housing a fluid entrance to the second cavity;

means for forming in the housing a fluid exit from the second cavity longitudinally spaced from the entrance to the second cavity so the hot wire lies between the entrance to the second cavity and the exit from the second cavity;

a source of one or more unknown gases in a carrier of reference gas coupled to the entrance to the first cavity;

a source of reference gas coupled to the entrance to the second cavity;

means for coupling a reference gas to the chamber to prevent the one or more unknown gases in a carrier from flowing to the chamber; and

means for measuring the difference in the change in resistance of the first and second hot wires responsive to the reference gas and the one or more unknown gases in a carrier.