Method of maintaining the strength of optical fibers

• US 4,118,211 A
• Filed: 06/22/1977
• Issued: 10/03/1978
• Est. Priority Date: 06/22/1977
• Status: Expired due to Term

• Current Assignee: The United States Of America As Represented By The Secretary Of The Army
• Original Assignee: The United States Of America As Represented By The Secretary Of The Army
• Inventors: Di Vita, Sam, Wade, Melvin J., Au Coin, Thomas R.
• Primary Examiner(s): Hoffman, James R.
• Application Number:
  US05/808,927
• Time in Patent Office: 468 Days
• Field of Search: 427/163, 65/3 R
• US Class Current: 65/423
• CPC Class Codes: C03C 25/1061 Inorganic coatings
• CPC Class Codes: C03C 25/42 Coatings containing inorganic materials
• CPC Class Codes: G02B 6/443 Protective covering
• CPC Class Codes: G02B 6/4479 Manufacturing methods of optical cables

Abstract

The mechanical strength of an optical fiber is maintained by coating the er with an inorganic ceramic material that is impervious to both moisture and chemically corrosive environments. The ceramic coating is applied immediately after the fiber is drawn.

Claims

1. Method of maintaining the mechanical strength of optical fibers after the fibers have been drawn from a melt, said method comprising hermetically sealing said fibers with a coating of silicon nitride that is impervious to both moisture and chemically corrosive environments immediately after the optical fiber has been drawn from the melt.

2. Method of maintaining the mechanical strength of optical fibers after the fibers have been drawn from a melt, said method comprising hermetically sealing said fibers with a coating of boron nitride that is impervious to both moisture and chemically corrosive environments immediately after the optical fiber has been drawn from the melt.

3. Method of maintaining the mechanical strength of optical fibers after the fibers have been drawn from a melt, said method comprising hermetically sealing said fibers with a coating of titanium dioxide that is impervious to both moisture and chemically corrosive environments immediately after the optical fiber has been drawn from the melt.

4. Method of producing an optical fiber of high mechanical strength from a high purity fused silica preform rod, said method including the steps of

(A) heating the preform rod at about 1800°

C to form a melt,

(B) drawing a fiber from the melt, and

(C) hermetically sealing the fiber with a coating of silicon nitride that is impervious to both moisture and chemically corrosive environments immediately after drawing the fiber from the melt.

5. Method of producing an optical fiber of high mechanical strength from a high purity fused silica preform rod, said method including the steps of

(A) heating the preform rod at about 1800°

C to form a melt,

(B) drawing a fiber from the melt, and

(C) hermetically sealing the fiber with a layer of boron nitride that is impervious to both moisture and chemically corrosive environments immediately after drawing the fiber from the melt.

6. Method of producing an optical fiber of high mechanical strength from a high purity fused silica preform rod, said method including the steps of

(A) heating the preform rod at about 1800°

C to form a melt,

(B) drawing a fiber from the melt, and

(C) hermetically sealing the fiber with a coating of titanium dioxide that is impervious to both moisture and chemically corrosive environments immediately after drawing the fiber from the melt.

7. Method of producing an optical fiber of high mechanical strength from a high purity fused silica preform rod, said method including the steps of

(A) heating the preform rod at about 1800°

C to form a melt,

(B) drawing a fiber from the melt, and

8. (C) hermetically sealing the fiber with a layer of silicon nitride of about 0.02 to 0.20 micrometer in thickness obtained by a chemical vapor deposition process using ammonia, silane, and nitrogen as a carrier gas at temperatures ranging from about 600°

C to about 1000°

C according to the reaction;

space="preserve" listing-type="equation">4NH.sub.3 + 3SiH.sub.4 .sup.600°

C to 1000°

C Si.sub.3 N.sub.4 + 12H.sub.2

immediately after drawing the fiber from the melt.