Particle size analyzer

• US 4,179,218 A
• Filed: 05/15/1978
• Issued: 12/18/1979
• Est. Priority Date: 05/15/1978
• Status: Expired due to Term

• Current Assignee: The Boeing Co.
• Original Assignee: The Boeing Co.
• Inventors: Gellert, Robert I., Erdmann, Joachim C., Skaugset, Richard L.
• Primary Examiner(s): Corbin, John K.
• Assistant Examiner(s): Arnold, B. Y.
• Application Number:
  US05/905,793
• Time in Patent Office: 582 Days
• Field of Search: 356/335, 356/336, 356/337, 356/338, 356/342, 356/28.5, 250/574
• US Class Current: 356/336
• CPC Class Codes: G01N 15/1429 Signal processing
• CPC Class Codes: G01N 15/1433 using image recognition
• CPC Class Codes: G01N 15/1436 the optical arrangement forming an integrated apparatus with the sample container, e.g. a flow cell
• CPC Class Codes: G01N 15/1459 the analysis being performed on a sample stream
• CPC Class Codes: G01N 2015/1486 Counting the particles

Abstract

A particle size analyzer that measures the intensity of light scattered by moving particles passing through the probe of a crossed beam laser anemometer, verifies that the measured signal was produced by a particle passing through a region near the center of the probe, and stores count values related to the number of particles producing the same scattered light intensity value is disclosed. Since scattered light intensity values are related to particle size, the stored count values equal the number of particles of the same size detected by the analyzer. In the preferred form of the invention, the measured light intensity determines the address of a particular intensity bin of a storage system. After verification to determine if a measured intensity value was produced by a particle passing through a region near the center of the probe, the count value stored in an intensity bin related to the measured value is updated by one. When any bin reaches the maximum value that can be stored therein, the particle light intensity measuring mode of operation ends and the particle size analyzer is placed in a readout mode of operation. In the readout mode of operation, the intensity bin count values are sequentially read out, converted into analog form, and displayed.

Claims

1. A particle size analyzer comprising:

a crossed beam laser anemometer that produces a non-contacting probe formed of a series of fringes that produce blinking scattered light when a particle passes transversely through the series of fringes, detects the blinking scattered light produced by particles passing through said fringes and produces a fluctuating output signal having a magnitude related to the magnitude of the light scattered by particles passing through said fringes;

analyzing means for;

(a) receiving the fluctuating output signal of said crossed beam laser anemometer;

(b) verifying that a particle causing a fluctuating output signal has passed through a number of fringes of said probe above a predetermined number; and

(c) producing a coded output signal if the particle causing said fluctuating output signal has passed through said number of fringes, said coded output being a function of the magnitude of said fluctuating output signal;

storage means, including a plurality of data bins, for;

(a) receiving said coded output of said analyzing means;

(b) reading out the data stored in a particular data bin each time a coded output occurs;

(c) changing said data; and

(d) writing the changed data back into the same data bin; and

,

readout means connected to said storage means for sequentially reading out the data stored in said data bins.

2. A particle size analyzer as claimed in claim 1 wherein said analyzing means verifies that the particle causing said fluctuating output signal has passed through said number of fringes by analyzing the number of fluctuations of said fluctuating output signal.

3. A particle size analyzer as claimed in claim 2 wherein the analysis of the number of fluctuations of said fluctuating output signal is done by counting the fluctuations of said fluctuating output signal and comparing the resultant count value with a set value equal to said number of fringes.

4. A particle size analyzer as claimed in claim 3 wherein said analyzing means includes a comparison system that measures the intensity of said fluctuating output signal by stepwise comparing the magnitude of said fluctuating output signal with step related reference voltages, decoding the results of said stepwise comparison and producing said coded output in accordance therewith.

5. A particle size analyzer as claimed in claim 4 wherein said storage means includes:

a sample address control connected to said comparison system for receiving said coded output and producing, in accordance therewith, an address signal;

a data storage system, including said plurality of data bins, connected to said sample address control for receiving said address signals and producing the data stored in a data bin related to an address signal produced by said sample address control; and

,

a data update control connected to said data storage system for receiving the data from the data bin addressed by the output of said sample address control, incrementing said data and storing said incremented data in the same data bin that produced said data.

6. A particle size analyzer as claimed in claim 5 wherein said fluctuating output signal of said laser anemometer includes two fluctuating components, one of said fluctuating components being a video signal whose magnitude is related to the magnitude of the light scattered by a particle passing through said probe and the other of said fluctuating components being a square wave signal that tracks the fluctuations of said video signal.

7. A particle size analyzer as claimed in claim 6 wherein said analyzing means also includes a sample control, said sample control adapted to receive and buffer said video signal and apply said video signal to said comparison system, said sample control also including counting means for counting the fluctuations of said square wave signal and comparing the resultant count value with said set value equal to said number of fringes, said sample control also including sample control means for producing a sample signal if the number of fluctuations counted by said counting means reaches a level equal to said set value equal to said number of fringes, said sample signal being applied to said sample address control for enabling said sample address control to receive said coded output and produce, in accordance therewith, said address signal.

8. A particle size analyzer as claimed in claim 7 wherein said readout means includes a readout address control for producing and applying to said data storage system address signals related to the addresses of said plurality of data bins included in said data storage system and converter means for receiving data stored in said plurality of data bins of said data storage system as said data bins are addressed and converting said received data into a form suitable for receipt by a display or recording medium.

9. A particle size analyzer as claimed in claim 8 wherein said data storage system includes means for selectively receiving said address signals produced by said sample address control and said readout address control and using said address signals to control the data read out from said data bins.

10. A particle size analyzer as claimed in claim 1 wherein read out data is changed by incrementing said read out data.

11. A particle size analyzer as claimed in claim 1 wherein said analyzing means includes a comparison system that measures the intensity of said fluctuating output signal by stepwise comparing the magnitude of said fluctuating output signal with step related reference voltages, decoding the results of said stepwise comparison and producing said coded output in accordance therewith.

12. A particle size analyzer as claimed in claim 11 wherein said storage means includes:

a sample address control connected to said comparison system for receiving said coded output and producing, in accordance therewith, an address signal;

a data storage system, including a plurality of data bins, connected to said sample address control for receiving said address signals and producing the data stored in a data bin related to an address signal produced by said sample address control; and

,

a data update control connected to said data storage system for receiving the data from the data bin addressed by the output of said sample address control, incrementing said data and storing said incremented data in the same data bin that produced said data.

13. A particle size analyzer as claimed in claim 12 wherein said fluctuating output signal of said laser anemometer includes two fluctuating components, one of said fluctuating components being a video signal whose magnitude is related to the magnitude of the light scattered by a particle passing through said probe and the other of said fluctuating components being a square wave signal that tracks the fluctuations of said video signal.

14. A particle size analyzer as claimed in claim 13 wherein said analyzing means also includes a sample control, said sample control adapted to receive and buffer said video signal and apply said video signal to said comparison system, said sample control also including counting means for counting the fluctuations of said square wave signal and comparing the resultant count value with said set value equal to said number of fringes, said sample control also including sample control means for producing a sample signal if the number of fluctuations counted by said counting means reaches a level equal to or greater than said set value equal to said number of fringes, said sample signal being applied to said sample address control for enabling said sample address control to receive said coded output and produce, in accordance therewith, said address signal.

15. A particle size analyzer as claimed in claim 14 wherein said readout means includes a readout address control for producing and applying to said data storage system address signals related to the addresses of said plurality of data bins included in said data storage system and converter means for receiving data stored in said plurality of data bins of said data storage system as said data bins are addressed and converting said received data into a form suitable for receipt by a display or recording medium.

16. A particle size analyzer as claimed in claim 15 wherein said data storage system includes means for selectively receiving said address signals produced by said sample address control and said readout address control and using said address signals to control the data read out from said data bins.