Pumping system

• US 4,225,290 A
• Filed: 02/22/1979
• Issued: 09/30/1980
• Est. Priority Date: 02/22/1979
• Status: Expired due to Term

• Current Assignee: Instrumentation Specialties Company
• Original Assignee: Instrumentation Specialties Company
• Inventors: Allington, Robert W.
• Primary Examiner(s): Jenkins, Robert W.
• Application Number:
  US06/013,986
• Time in Patent Office: 586 Days
• Field of Search: 417/18, 417/19, 417/20, 417/21, 417/22, 417/23, 417/38, 318/48, 318/34, 318/41, 318/66
• US Class Current: 417/18
• CPC Class Codes: G01N 2030/326 pumps
• CPC Class Codes: G01N 30/34 of fluid composition, e.g. gradient G01N30/36 takes precedence
• CPC Class Codes: G01N 30/36 in high pressure liquid systems

Abstract

An improved chromatographic pump control circuit for compensating for pulsation in pump flow over a wide range of flow-rates and pressures and for providing improved protection against pump pressure and motor torque fault conditions. The control circuit is coupled to a pump motor to provide motor speed-up during the repressurization portion of the pump cycle as a function of the set point pump flow rate. The circuit also includes a summing circuit for developing a repressurization signal based on the flow-rate and detected pressure. The signal is coupled to compensate for pulsation by controlling the duration of repressurization with respect to both pressure and the set point of the flow rate. The circuit is additionally coupled to sense pump pressure and motor torque to initiate alarm and pump shutdown during high and low pressure and motor over-torque fault conditions.

Claims

1. A circuit for compensating for pulsations in pump flow-rate by controlling pump motor speed during delivery, refill, and repressurization periods of a pump cycle comprising:

a first pump driven by a first motor;

means for providing at least one signal representing pump flow-rate;

first motor control means coupled to said motor and responsive to said flow-rate signal for driving the first motor at a speed proportional to said flow-rate signal during the delivery period of the pump cycle and at an increased speed during the refill and repressurization periods of the pump cycle; and

interface control means coupled to said motor control means and responsive to said flow-rate signal for providing a repressurization signal causing the first motor control means to increase motor speed during repressurization for a time period proportional to the magnitude of the repressurization signal.

2. The circuit of claim 1 wherein said interface control means includes:

means for providing a signal representing pump pressure;

sample and hold means coupled to sample said pressure signal during the delivery portion of a pump cycle for providing a delivery pressure signal; and

summing means coupled to sum said delivery pressure signal and said flow-rate signal to produce said repressurization signal.

3. The circuit of claim 1 wherein said interface control means further includes means for adjusting the magnitude of the repressurization signal relative to a baseline level.

4. The circuit of claim 1 wherein said interface means includes a flow-rate adjust means for adjusting the tracking and varying the magnitude of the flow-rate signal.

5. The circuit of claim 4 wherein said interface control means further includes:

high limit set means for providing a first reference signal;

low limit set means for providing a second reference signal;

high pressure detector means coupled to receive said pressure signal and said first reference signal for providing an output signal when said pressure signal exceeds said first reference signal;

low pressure detector means coupled to receive said pressure signal and said second reference signal for providing an output signal when said pressure signal is less than said second reference signal; and

alarm control means coupled to said high and low pressure detector means for providing an alarm signal upon receipt of an output signal from either of said detector means.

6. The circuit of claim 1 further including:

a second pump driven by a second motor;

a second motor control means coupled to said second motor and responsive to a flow-rate signal for driving the second pump motor at a speed proportional to the flow-rate signal during the delivery period of the pump cycle and at an increased speed during the refill and repressurization periods of the pump cycle, and wherein said means for providing at least one flow-rate signal includes;

a single pump flow-rate setting means for providing a single flow-rate signal; and

gradient program control means for providing programmable first and second flow-rate signals, and further wherein said interface control means includes;

first repressurization control means coupled to said first motor control means and responsive to an input signal for providing a first repressurization signal causing the first motor control means to increase motor speed during repressurization for a time period proportional to the magnitude of the first repressurization signal; and

second repressurization control means coupled to said second motor control means and responsive to an input signal for providing a second repressurization signal causing the second motor control means to increase motor speed during repressurization for a time period proportional to the magnitude of the second repressurization signal; and

switch means for selectively coupling the single pump flow-rate signal to the first motor control means and as the input signal to said first means in one switch position and the first and second flow-rate signals to the first and second motor control means respectively and as the input signals to said first and second means respectively in a second switch position.

7. The circuit of claim 6 wherein said interface control means further includes:

means for providing a signal representing pump pressure;

sample and hold means coupled to sample said pressure signal during the delivery portion of a pump cycle for providing a delivery pressure signal; and

wherein said first and second repressurization means each include;

summing means coupled to sum said delivery pressure signal and its associated flow-rate signal to produce said repressurization signal.

8. The circuit of claim 7 wherein each of said summing means includes means for adjusting the magnitude of the repressurization signal relative to a baseline level.

9. The circuit of claim 7 wherein said interface control means further includes:

a first flow-rate adjust means for tracking and varying the magnitude of the first flow-rate signal; and

a second flow-rate adjust means for tracking and varying the magnitude of the second flow-rate signal.

10. The circuit of claim 7 wherein said interface control means further includes:

high limit set means for providing a first reference signal;

low limit set means for providing a second reference signal;

high pressure detector means coupled to receive said pressure signal and said first reference signal for providing an output signal when said pressure signal exceeds said first reference signal;

low pressure detector means coupled to receive said pressure signal and said second reference signal for providing an output signal when said pressure signal is less than said second reference signal; and

alarm control means coupled to said high and low pressure detector means for providing an alarm signal upon receipt of an output signal from either of said detector means.

11. The circuit of claim 10 wherein said interface control means further includes:

select limit switch means coupled to said high and low limit set means for selectively providing one of said first or second reference signals as an output;

pressure limit read switch means coupled to receive said delivery pressure signal and the output of said select limit switch means for selectively providing an output of one of those signals; and

a digital voltmeter coupled to the output of said pressure limit read switch means in order to display a value proportional to the pressure signal of the first or second reference signals.

12. The circuit of claim 11 wherein each motor control means further includes:

torque detector means coupled to its respective motor for sensing motor armature current and providing a signal representing motor torque;

means responsive to said torque signal for providing a torque limit output signal when the motor torque signal exceeds a predetermined value, and wherein said interface control means further includes;

first limit control means responsive to the torque limit output signal from said first motor control means for providing an output signal when the first motor torque signal exceeds said predetermined value;

second limit control means responsive to the torque limit output signal from said second motor control means for providing an output signal when the second motor torque signal exceeds said predetermined value; and

said alarm means being coupled to said first and second limit control means for providing an alarm signal upon receipt of an output signal from either of said limit control means.

13. The circuit of claim 12 wherein each of said first and second limit control means includes an indicator means for providing a visual indication of a pump fault condition in response to the receipt of a torque limit output signal.

14. The circuit of claim 12 wherein said interface control means further includes:

a pump stop control means coupled to said first and second limit control means and said high and low detector means for providing a pump stop signal upon receipt of an output signal from any of said limit control means and detector means;

stop switch means coupled to said pump stop control means for providing shutdown signals upon receipt of a pump stop signal, and wherein each of said motor control means further includes;

means responsive to a shutdown signal for causing the motor to stop.

15. The circuit of claim 14 wherein said interface control means further includes:

first gate means coupled to said pump stop control means for preventing said first motor control means from receiving a flow-rate signal upon receipt of a pump stop signal; and

second gate means coupled to said pump stop control means for preventing said second motor control means from receiving a flow-rate signal upon receipt of a pump stop signal.

16. The circuit of claim 14 wherein said sample and hold means is coupled to be responsive to said pump stop signal to provide the pressure signal as the delivery pressure signal upon the occurrence of a pump stop signal.

17. The circuit of claim 7 wherein each motor control means further includes:

means for providing a strobe signal during the refill and repressurization periods of the pump cycle, and wherein said interface control means further includes;

gate drive circuit means for providing an output signal upon receipt of a strobe signal from either motor control means; and

said sample and hold means being coupled to be responsive to the output signal from said gate drive circuit means to prevent sampling of the pressure signal during refill and repressurization.

18. In a chromatographic system including a chromatographic means providing a stationary phase, a conduit coupled to supply a mobile phase to said stationary phase, first and second fluid reservoirs, a pump coupled to each reservoir to supply fluid from that reservoir to said conduit, a motor coupled to drive each pump, and means for controlling motor speed during delivery, refill and repressurization of each pump cycle to reduce pulsations in the system flow-rate, the improvement in said means for controlling comprising:

means for providing at least one signal representing pump flow-rate;

motor control means coupled to each pump motor and responsive to the flow-rate signal for driving the associated motor at a speed proportional to the flow-rate signal during the delivery period of the pump cycle and at an increased speed during the refill and repressurization periods of the pump cycle; and

interface control means coupled to said motor control means and responsive to at least one flow-rate input signal for providing at least one repressurization signal causing at least one of said motor control means to increase motor speed during repressurization for a time period proportional to the magnitude of the repressurization signal.

19. The system of claim 18 wherein means for providing at least one flow-rate signal includes:

a single pump flow-rate setting means for providing a single flow-rate signal; and

gradient program control means for providing programmable first and second flow-rate signals, and wherein said interface control means includes;

first repressurization control means coupled to one of said motor control means and responsive to an input signal for providing a first repressurization signal causing the one of said motor control means to increase motor speed during repressurization for a time period proportional to the magnitude of the first repressurization signal; and

second repressurization control means coupled to the other of said motor control means and responsive to an input signal for providing a second repressurization signal causing the other of said motor control means to increase motor speed during repressurization for a time period proportional to the magnitude of second repressurization signal; and

switch means for selectively coupling the single flow-rate signal as the input signal to the motor control means and first repressurization control means in one switch portion and the first and second flow-rate signals as the input signals to respective ones of said motor control means and the first and second repressurization control means in a second switch position.

20. The system of claim 19 wherein the improvement further comprises:

a pressure transducer coupled to sense the pressure in the conduit supplying the mobile phase, and wherein the interface control means further includes;

amplifier means coupled to said pressure transducer for providing a signal proportional to actual pressure;

sample and hold means coupled to said amplifier means to sample said pressure signal during the delivery portion of a pump cycle for providing a delivery pressure signal, and wherein said first and second repressurization control means each include;

summing means coupled to sum said delivery pressure signal and its associated flow-rate signal to produce said repressurization signal.

21. The system of claim 20 wherein each of said summing means includes means for adjusting the magnitude of the repressurization signal relative to a baseline level.

22. The system of claim 20 wherein said interface control means further includes:

a first flow-rate adjust means for tracking and varying the magnitude of the first flow-rate signal; and

a second flow-rate adjust means for tracking and varying the magnitude of the second flow-rate signal.

23. The system of claim 20 wherein said interface control means further includes means responsive to said pressure signal for providing an alarm signal when said pressure signal is greater than a first reference signal or less than a second reference signal.

24. The system of claim 23 wherein said means for providing an alarm signal comprises:

high limit set means for providing a first reference signal;

low limit set means for providing a second reference signal;

high pressure detector means coupled to said amplifier means and said high limit set means for providing an output signal when said pressure signal exceeds said first reference signal;

26. The system of claim 24 wherein said interface control means further includes:

separate indicator means coupled to each detector means for providing a visual indication of a pressure fault upon receipt of an output signal from said detector means.

27. The system of claim 20 wherein each of said motor control means includes:

means for sensing motor torque and providing a torque limit signal when said motor torque exceeds a predetermined value, and wherein said interface control means further includes;

means responsive to said torque limit control signal for providing a pump stop signal; and

means responsive to said pump stop signal for causing each of said motor control means to stop the pump motors upon the occurrence of a torque fault condition.

25. low pressure detector means coupled to said amplifier means and said low limit set means for providing an output signal when said pressure signal is less than said second reference signal;

and

alarm control means coupled to said high and low pressure detector means for providing said alarm signal upon receipt of an output signal from either of said detector means.