Method for the production of glass fiber-reinforced gypsum sheets and gypsum board formed therefrom

• US 4,233,368 A
• Filed: 06/05/1978
• Issued: 11/11/1980
• Est. Priority Date: 06/05/1978
• Status: Expired due to Term

• Current Assignee: United States Gypsum Company (GEBR Knauf Verwaltungsgesellschaft KG)
• Original Assignee: United States Gypsum Company (GEBR Knauf Verwaltungsgesellschaft KG)
• Inventors: Izard, David G., Baehr, Donald O.
• Primary Examiner(s): Kendell, Lorraine T.
• Application Number:
  US05/912,776
• Time in Patent Office: 890 Days
• Field of Search: 156/39, 156/4 Z, 156/62.2, 162/154, 162/156, 264/121, 264/333, 264/87, 264/284, 264/518, 428/538, 428/426
• US Class Current: 428/187
• CPC Class Codes: B28B 1/521 from dry mixtures to which a setting agent is applied after forming B28B1/526, B28B1/527 take precedence
• CPC Class Codes: B32B 13/12 of synthetic resin
• CPC Class Codes: B32B 2262/101 Glass fibres
• CPC Class Codes: B32B 2305/08 Reinforcements
• CPC Class Codes: B32B 2315/085 Glass fiber cloth or fabric
• CPC Class Codes: B32B 38/06 Embossing
• CPC Class Codes: B32B 7/12 using interposed adhesives or interposed materials with bonding properties
• CPC Class Codes: E04C 2/043 of plaster E04C2/049 takes precedence
• CPC Class Codes: Y10T 428/24736 Ornamental design or indicia

Abstract

A fiber-reinforced cementitious sheet is formed by first co-mixing in an air current reinforcing fibers such as glass fibers, and cementitious mineral materials in finely particulate form such as calcium sulfate hemihydrate, both in substantially dry form, depositing the mixture on a moving foraminous surface by means of the air current to form a sheet, applying water as by spraying in at least an amount which is stoichiometrically sufficient to hydrate the calcium sulfate hemihydrate to the dihydrate form and to provide the necessary degree of plasticity to the mixture, densifying the sheet by compression, and setting and drying the sheet. A pair of sheets may be utilized as face sheets and, prior to setting, combined with a core formed of for example a calcium sulfate hemihydrate slurry, and the sheets and core then set and dried to form a paper-free gypsum board having excellent strength, surface hardness, and fire-resistant properties.

Claims

1. A method for preparing a cementitious construction sheet having reinforcing fibers dispersed therein, which comprises:

(a) mixing together in a moving air current generated by an air blower a substantially dry water-settable calcium sulfate hemihydrate in finely particulate form with reinforcing glass fibers,

(b) providing a foraminous moving surface,

(c) depositing the mixture of calcium sulfate hemihydrate and glass fibers on said foraminous surface to form a sheet,

(d) applying water over the sheet,

(e) permitting the calcium sulfate hemihydrate to set, and

(f) drying said sheet to remove any excess water.

2. A method according to claim 1, wherein said water is applied by spraying.

3. A method according to claim 2, wherein a vacuum is applied below said moving foraminous surface to assist in directing said cementitious material and said fibers toward said surface.

4. A method according to claim 2, wherein said sheet is densified by compression prior to setting.

5. A method according to claim 2, wherein the amount of water is not substantially greater than the stoichiometric amount necessary to hydrate and set said cementitious material.

6. A method according to claim 1, wherein said calcium sulfate hemihydrate is in the beta form.

7. A method according to claim 1, wherein said calcium sulfate hemihydrate is in the alpha form.

8. A method according to claim 2, wherein said cementitious material is a mixture of alpha calcium sulfate hemihydrate and hydraulic cement.

9. A method according to claim 2, wherein said cementitious material is a hydraulic cement.

10. A method according to claim 2, wherein said cementitious material is very high early strength hydraulic cement.

11. A method according to claim 2, wherein the thickness of said sheet is from about 0.010 inch to about 0.250 inch.

12. A method according to claim 2, wherein the weight of fibers is from about 3% to about 25% based on the weight of the dry formed sheet.

13. A method according to claim 2, wherein the weight of fibers is from about 6% to about 10% based on the weight of the dry formed sheet.

14. A method according to claim 1, wherein said glass fibers are formed by chopping glass fiber strands and subsequently opening the chopped strands into individual fibers.

15. A method according to claim 5, wherein said sheet is densified by passing it between compression rolls.

16. A method according to claim 2, wherein a pattern is applied to one surface by embossing prior to setting said cementitious material.

17. A cementitious construction sheet having reinforcing fibers dispersed therein, said sheet being the product formed by the method which comprises:

(a) mixing together in a moving air current generated by an air blower a substantially dry water-settable calcium sulfate hemihydrate in finely particulate form with reinforcing glass fibers,

(b) providing a foraminous moving surface,

(c) depositing the mixture of calcium sulfate hemihydrate and glass fibers on said foraminous surface to form a sheet,

(d) applying water over the sheet,

(e) permitting the calcium sulfate hemihydrate to set, and

(f) drying said sheet to remove any excess water.

18. A sheet according to claim 17, wherein said water is applied by spraying.

19. A sheet according to claim 18, wherein a vacuum is applied below said moving foraminous surface to assist in directing said cementitious material and said fibers toward said surface.

20. A sheet according to claim 18, wherein said sheet is densified by compression prior to setting.

21. A sheet according to claim 18, wherein the amount of water is not substantially greater that the stoichiometric amount necessary to hydrate and set said cementitious material.

22. A sheet according to claim 17, wherein said calcium sulfate hemihydrate is in the beta form.

23. A sheet according to claim 17, wherein said hemihydrate is in the alpha form.

24. A sheet according to claim 18, wherein said cementitious material is a mixture of alpha calcium sulfate hemihydrate and hydraulic cement.

25. A sheet according to claim 18, wherein said cementitious material is a hydraulic cement.

26. A sheet according to claim 18, wherein said cementitious material is very high early strength hydraulic cement.

27. A sheet according to claim 18, wherein the thickness of said sheet is from about 0.010 inch to about 0.250 inch.

28. A sheet according to claim 18, wherein the weight of fibers is from about 3% to about 25% based on the weight of the dry formed sheet.

29. A sheet according to claim 18, wherein the weight of fibers is from about 6% to about 10% based on the weight of the dry formed sheet.

31. A sheet according to claim 20, wherein said sheet is densified by passing it between compression rolls.

32. A sheet according to claim 18, wherein a pattern is applied to one surface by embossing prior to setting said cementitious material.

30. A sheet according to claim 35, wherein said glass fibers are formed by chopping glass fiber strands and subsequently opening the chopped strands into individual fibers.