Pressure responsive conditioning control gas sterilization
First Claim
1. Method for conditioning goods for sterilization and sterilizing goods with a chemically biocidal gas in a sealable chamber capable of operating at pressures other than atmospheric, the conditioning including heating the goods to a selected temperature related to the desired sterilization temperature and moistening the goods to a desired level for such biocidal gas sterilization, with conditioning steps being free of temperature and moisture measurement requirements in the goods and in the chamber, comprising the steps, after closing the chamber to permit operation at pressures other than atmospheric, ofevacuating the chamber to a preselected subatmospheric level,supplying a condensable conditioning vapor having heating and moisturizing properties for heating and moisturizing goods to be sterilized, such vapor having a determinable interrelationship between pressure level and temperature,injecting such conditioning vapor into the chamber to raise chamber pressure to a second preselected subatmospheric pressure level corresponding to approximately desired sterilization temperature based on the interrelationship of pressure level and temperature of the condensable conditioning vapor,such injecting of conditioning vapor being free of flow rate adjustment control requirements, thenholding the chamber in sealed condition for a predetermined time with evacuating and vapor injecting interrupted, thenrepeating such sequence, of evacuating the chamber followed by injecting conditioning vapor to repressurize the chamber to the preselected subatmospheric pressure corresponding to approximately desired sterilizing temperature and holding the chamber in sealed condition for a predetermined time with evacuating and vapor injecting interrupted, a preselected number of times to establish desired temperature and moisture conditions in goods to be sterilized, thenadding chemically biocidal gas while the chamber is otherwise sealed to raise chamber pressure to a desired supraatmospheric pressure, andholding such biocidal gas in the chamber for a time period to complete desired sterilization.
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Accused Products
Abstract
Biocidal gas sterilization methods and apparatus are disclosed in which goods are heated and moisturized prior to addition of the sterilizing gas utilizing repressurization after initial evacuation to provide drive power for the conditioning vapor and improve conditioning efficiency. After initial evacuation to a selected subatmospheric pressure level, the chamber is repressurized with a conditioning vapor comprising steam to a subatmospheric pressure level corresponding approximately to desired sterilizing temperature, then the chamber is held with evacuating and vapor injecting interrupted for a predetermined interval; this sequence of steps is repeated a selected number of times; and, conditioning to various sterilizing temperatures is available. Initial evacuation can be accompanied by intermittent injection of conditioning vapor. No chamber measurement of temperature or relative humidity is required for conditioning control and conditioning vapor injection is free of flow rate control requirements.
46 Citations
10 Claims
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1. Method for conditioning goods for sterilization and sterilizing goods with a chemically biocidal gas in a sealable chamber capable of operating at pressures other than atmospheric, the conditioning including heating the goods to a selected temperature related to the desired sterilization temperature and moistening the goods to a desired level for such biocidal gas sterilization, with conditioning steps being free of temperature and moisture measurement requirements in the goods and in the chamber, comprising the steps, after closing the chamber to permit operation at pressures other than atmospheric, of
evacuating the chamber to a preselected subatmospheric level, supplying a condensable conditioning vapor having heating and moisturizing properties for heating and moisturizing goods to be sterilized, such vapor having a determinable interrelationship between pressure level and temperature, injecting such conditioning vapor into the chamber to raise chamber pressure to a second preselected subatmospheric pressure level corresponding to approximately desired sterilization temperature based on the interrelationship of pressure level and temperature of the condensable conditioning vapor, such injecting of conditioning vapor being free of flow rate adjustment control requirements, then holding the chamber in sealed condition for a predetermined time with evacuating and vapor injecting interrupted, then repeating such sequence, of evacuating the chamber followed by injecting conditioning vapor to repressurize the chamber to the preselected subatmospheric pressure corresponding to approximately desired sterilizing temperature and holding the chamber in sealed condition for a predetermined time with evacuating and vapor injecting interrupted, a preselected number of times to establish desired temperature and moisture conditions in goods to be sterilized, then adding chemically biocidal gas while the chamber is otherwise sealed to raise chamber pressure to a desired supraatmospheric pressure, and holding such biocidal gas in the chamber for a time period to complete desired sterilization.
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10. Method for conditioning and sterilizing goods with a chemically biocidal gas in a sealable chamber capable of operating at pressures other than atmospheric, the conditioning including heating the goods to a selected temperature related to the desired sterilization temperature and moistening the goods to a desired level for such biocidal gas sterilization with conditioning steps being responsive to chamber pressure and independent of temperature and relative humidity measurement requirements, comprising the steps of
loading goods to be sterilized into the chamber and closing the chamber to permit operation at pressures other than atmospheric, supplying steam at a pressure of about 35 to 80 psig, evacuating the chamber to about 90 mm. Hg. while intermittently injecting steam in pulses of about five second duration spaced by selected time intervals of about thirty second duration, interrupting such intermittent steam injection while continuing such chamber evacuating to about 60 mm. Hg., then injecting steam to raise the pressure within the chamber to about 90 mm. Hg., such steam injection into the chamber and such earlier intermittent pulse steam injections being free of injection flow rate adjustment requirements, then holding the chamber in sealed condition for about three minutes with evacuating and steam injecting interrupted, then repeating such sequence of evacuating to about 60 mm. Hg., repressurizing to about 90 mm. Hg., and holding the chamber in sealed condition for about three minutes with evacuating and vapor injecting interrupted to heat and moisturize the goods to desired levels, then adding ethylene oxide and a diluent gas to raise chamber pressure above atmospheric pressure while maintaining the chamber in otherwise sealed condition, maintaining a wall portion of the chamber at approximately desired sterilization temperature to minimize heat losses from the load, then holding the ethylene oxide, diluent gas, and conditioning moisture at a pressure above atmospheric pressure in the sealed chamber to complete desired sterilization, and, then removing such gases from the chamber to return the chamber to atmospheric pressure for removal of the sterilized goods.
Specification
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- Resources
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Current AssigneeAmerican Sterilizer Company (Steris Corporation)
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Original AssigneeAmerican Sterilizer Company (Steris Corporation)
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InventorsBaran, Walter J.
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Primary Examiner(s)Richman, Barry S.
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Application NumberUS06/009,818Time in Patent Office686 DaysField of Search422/34, 422/27, 422/2, 422/3, 422/33, 422/37, 422/28, 422/26, 422/112, 422/114, 422/116, 422/117, 422/295, 422/300US Class Current422/2CPC Class CodesA61L 2/206 Ethylene oxideA61L 2/24 Apparatus using programmed ...
