Carbon dioxide impregnation of tobacco by super cooling

• US 4,250,898 A
• Filed: 10/13/1978
• Issued: 02/17/1981
• Est. Priority Date: 10/13/1978
• Status: Expired due to Term

• Current Assignee: Philip Morris USA Incorporated (Altria Group, Inc.)
• Original Assignee: Philip Morris USA Incorporated (Altria Group, Inc.)
• Inventors: Utsch, Francis V., de la Burde, Roger Z., Aument, Patrick E.
• Primary Examiner(s): Millin, V.
• Application Number:
  US05/951,072
• Time in Patent Office: 858 Days
• Field of Search: 131/140 P, 131/121, 131/140 R, 131/120, 131/140 B
• US Class Current: 131/291
• CPC Class Codes: A24B 3/185 by impregnating with a liquid and subsequently freezing and evaporating this liquid

Abstract

A process for impregnating tobacco with carbon dioxide is provided. The process comprises: (a) contacting tobacco with carbon dioxide gas at relatively low pressure (b) rapidly cooling the tobacco-carbon dioxide system until the carbon dioxide condenses as liquid or solid within the tobacco and finally solidifies, and (c) releasing the pressure in the cooled system. Thereafter, the carbon dioxide-treated tobacco may be expanded conventionally, such as by subjecting it to heating conditions effective to liberate the carbon dioxide therein.

Claims

1. A process for impregnating tobacco with carbon dioxide comprising the steps of:

(a) contacting tobacco with gaseous carbon dioxide at a pressure of at least 50 psig; and

(b) rapidly cooling the carbon dioxide/tobacco system to a temperature where much of the carbon dioxide condenses and solidifies within the tobacco.

2. The process of claim 1 wherein the pressure in step (a) is between about 50 and 250 psig.

3. The process of claim 1 wherein the system is cooled to at least -70°

C. in step (b).

4. The process of claim 1 wherein the system is cooled in step (b) until the pressure thereof drops to no more than 20 psig.

5. The process of claim 1 which further comprises maintaining the pressure of the system during the initial portion of step (b) by continuing to admit carbon dioxide gas to the system.

6. A process for expanding tobacco comprising the steps of:

(a) contacting tobacco with gaseous carbon dioxide under a pressure of at least 50 psig;

(b) rapidly cooling the carbon dioxide/tobacco system to a temperature where the carbon dioxide condenses and solidifies within the tobacco to accomplish impregnation;

(c) releasing the pressure of the system; and

(d) thereafter heating the impregnated tobacco under conditions effective to liberate the carbon dioxide therein so as to cause expansion of the tobacco.

7. The process of claim 6 wherein the pressure is reduced to substantially atmospheric pressure in step (c).

8. The process of claim 6 wherein the tobacco is heated to a temperature between about 100°

to 370°

C. in step (d).