Continuous process mixing of pulverized solids and liquids and mixing apparatus

• US 4,257,710 A
• Filed: 01/15/1979
• Issued: 03/24/1981
• Est. Priority Date: 02/08/1978
• Status: Expired due to Term

• Current Assignee: Saint-Gobain Isover (Compagnie De Saint-Gobain)
• Original Assignee: Saint-Gobain Isover (Compagnie De Saint-Gobain)
• Inventors: Delcoigne, Adrien, Lanneau, Jacques
• Primary Examiner(s): JENKINS, ROBERT
• Application Number:
  US06/003,416
• Time in Patent Office: 799 Days
• Field of Search: 366/16, 366/8, 366/17, 366/18, 366/19, 366/21, 366/27, 366/28, 366/29, 366/34, 366/40, 366/131, 366/132, 366/134
• US Class Current: 366/8
• CPC Class Codes: B01F 23/50 Mixing liquids with solids displacing one liquid by another in dispersions of solids in liquids B01D12/00
• CPC Class Codes: B01F 23/51 Methods thereof
• CPC Class Codes: B01F 23/56 by introducing solids in liquids, e.g. dispersing or dissolving
• CPC Class Codes: B01F 25/64 of the centrifugal-pump type, i.e. turbo-mixers
• CPC Class Codes: B01F 27/80 with stirrers rotating about a substantially vertical axis
• CPC Class Codes: B01F 35/20 Measuring; Control or regulation
• CPC Class Codes: B01F 35/2218 Weight of at least one component to be mixed
• CPC Class Codes: B01F 35/75435 using means for discharging the mixture in a pulsating or intermittent manner
• CPC Class Codes: B01F 35/7547 using valves, gates, orifices or openings
• CPC Class Codes: B01F 35/83 by controlling the ratio of two or more flows, e.g. using flow sensing or flow controlling devices
• CPC Class Codes: B28B 1/16 for producing layered articles coating B28B11/04
• CPC Class Codes: B28B 13/02 Feeding the unshaped material to moulds or apparatus for producing shaped articles
• CPC Class Codes: B28B 19/00 Machines or methods for applying the material to surfaces to form a permanent layer thereon making shaped articles on mandrels B28B1/30; applying liquids or other fluent materials to surfaces in general B05C; glazing or engobing C04B
• CPC Class Codes: B28B 23/0006 the reinforcement consisting of aligned, non-metal reinforcing elements
• CPC Class Codes: B28B 5/027 the moulding surfaces being of the indefinite length type, e.g. belts, and being continuously fed feeding B28B13/02
• CPC Class Codes: E04C 2/043 of plaster E04C2/049 takes precedence
• CPC Class Codes: F16K 7/07 by means of fluid pressure
• CPC Class Codes: G05D 9/04 with auxiliary non-electric power
• CPC Class Codes: G05D 9/12 characterised by the use of electric means
• CPC Class Codes: Y10T 137/7339 By weight of accumulated fluid
• CPC Class Codes: Y10T 428/24413 : Metal or metal compound

Abstract

The invention deals with continuous process mixing of pulverized solids and liquids. It offers a mixing process comprising:

continuously introducing a liquid into a mixing container;

continuously introducing a solid powder into said container at such a rate that specified proportions of solid and liquid in the mixture are maintained;

rotating the products in the container in such a way as to establish a vortex;

regulating the solid and liquid supply rate in such a way that a given level of filling of container is constantly maintained;

continuously emptying the products mixture so that level of filling is maintained.

It offers as well a mechanism to implement the process including a mixing container having an intermediate bottom and a runoff opening, a turbine mounted above the intermediate bottom, and mechanism for supplying a liquid and a solid. Advantageously, the liquid is used to wash down the walls of the mixing container and may be applied to parts of the turbine to avoid retention of solids in the container. It can be applied to hydraulic binders preparations and specifically to continuous process preparation of a plaster and water mixture.

Claims

1. A continuous process for mixing pulverized solids and liquids such as plaster powder and water characterized in that it comprises:

continuously introducing the liquid in a mixing container at a selected flow rate,

continuously introducing the pulverized solid in said container at a selected flow rate,

said flow rates being selected to provide a desired proportion of solid and liquid,

rotating the solid and liquid in the container in order to create a vortex thereof,

withdrawing the thus mixed solid and liquid from the container and controlling the rate of withdrawing such that a desired level of the mixture in the container is maintained, the mean stay time for the mixture in the mixing container being determined by the said level of the mixture in the container.

5. A process according to claim 1 characterized in that the mean stay time for products to be mixed in the mixing container is at least equal to 3 seconds and preferably from 15 to 30 seconds.

6. A process according to claims 1, 2, 3, or 4 characterized by the fact that mixture is passed into an ejection device and is discharged at the periphery of the ejection device.

7. A process according to claim 6 characterized in that the pulverized solid is plaster and the liquid is water.

8. A process according to any of claims 1-3, 4 and 5 characterized in that the withdrawing is done through the bottom of the mixing container.

9. A process according to claim 8 characterized in that the pulverized solid is plaster and the liquid is water.

10. A process according to any of claims 1-3, 4 and 5 characterized by the fact that at least a portion of the liquid is introduced along the interior of the mixing container wall in order to create a continuous sheet of liquid around said wall and by the fact that the withdrawing is done through the bottom of the mixing container.

11. A process according to claim 10 characterized in that the pulverized solid is plaster and the liquid is water.

12. A process according to any of claims 1-3, 4 and 5 characterized in that the pulverized solid is introduced into the center of the vortex, at least a portion of the liquid is introduced along the interior of the mixing container wall in order to create a continuous sheet of liquid aroung said wall, and the withdrawing is done through the bottom of the mixing container.

13. A process according to claim 12 characterized in that the pulverized solid is plaster and the liquid is water.

14. A process according to any of claims 1-3, 4 and 5 characterized in that solid or liquid additives are introduced in the liquid.

15. A process according to claim 14 characterized in that the pulverized solid is plaster and the liquid is water.

16. A process according to claim 14 characterized in that the solid additives are introduced in solid phase.

17. A process according to claim 16 characterized in that the pulverized solid is plaster and the liquid is water.

18. A process according to any of claims 1-3, 4 and 5 characterized in that solid or liquid additives are introduced into the mixer.

19. A process according to claim 18 characterized in that the solid additives are introduced in solid phase.

20. A process according to claim 19 characterized in that the pulverized solid is plaster and the liquid is water.

21. A process according to claim 18 characterized in that the pulverized solid is plaster and the liquid is water.

22. A process in accordance with any of claims 1-3, 4 and 5 characterized in that the pulverized solid is plaster and the liquid is water.

29. A mixer according to claim 20 characterized in that the intermediate bottom is constituted by the top surface of a downward tapered solid of revolution core placed inside of the container'"'"'s tapered extension and centered on said container'"'"'s axis, said core having a section smaller than the container'"'"'s extension in order to provide for a ring shaped space in cross-section between it and said container'"'"'s inner wall.

30. A mixer according to claim 29 characterized in that the core placed inside the container'"'"'s extension is a straight cone positioned with its tip down and whose flat base constitutes the intermediate bottom, the container'"'"'s tapered extension also being conical.

31. A mixer according to claim 29 characterized in that the run-off valve flow regulation means is an elastic sleeve valve which is placed downstream of an ejection device in communication with the container run-off opening, said ejection device receiving the mixture discharging from the container and transforming its flow into a full stream for entry into the valve.

32. A mixer according to claim 31 characterized in that the ejection device is shaped like an inverted cyclone having a conical casing placed with its tip upward with an inlet at the tip of the cone and has a flat base, and a collector pipe comes out of the ejection pipe flush with said base and tangentially to the comical casing in the direction of rotation of the turbine.

33. A mixer according to claim 31 characterized in that the ejection device is an impact crown formed by a vertical can with a bottom and a lateral discharge pipe.

2. A continuous process for mixing pulverized solids and liquids such as plaster powder and water characterized in that it comprises:

continuously introducing the liquid in a mixing container at a selected flow rate,

continuously introducing the pulverized solid in said container at a selected flow rate,

said flow rates being selected to provide a desired proportion of solid and liquid,

rotating the solid and liquid in the container in order to create a vortex thereof, and

withdrawing the thus mixed solid and liquid from the container at a rate such that the desired level of the mixture in the container is maintained,

said process being further characterized in that its starting period includes the following steps;

introducing the liquid and solid into the mixing container in a weight ratio selected beforehand until a selected filling level of said mixing container is reached,

rotating the liquid and solid in the container and maintaining the rotating motion for a selected time, and then, at the same time continuously introducing into the container liquid and solid at flow rates such that weight ratio of the mixture is maintained, and continuously withdrawing the mixture from the container at a flow rate that will maintain the filling level.

3. A process according to claim 2 characterized in that the ratio of pulverized solid to water is 100 to 80 by weight.

4. A process according to claim 2 characterized in that the means stay time for products to be mixed in the mixing container is determined by said container filling level.

23. A vertical mixer, for pulverized solids and liquids characterized in that it comprises:

a container formed by a hollow solid of revolution and equipped in its lower end with a run-off opening, run-off flow rate regulation means in communication with said run-off opening, said container having an intermediate bottom spaced from the interior of the side wall of the container, a turbine mounted inside of the container above the intermediate bottom and revolving around a vertical axis on the container'"'"'s axis, means for continuously supplying a liquid in the container and means for continuously supplying a pulverized solid to the container.

24. A mixer according to claim 23 characterized in that the intermediate bottom offers a top surface whose shape assumes corresponding top mixing zone flow lines.

25. A mixer according to claim 23 characterized in that the intermediate bottom offers a flat top surface which is perpendicular to the container'"'"'s axis and is placed in the immediate vicinity of the turbine.

26. A mixer according to claim 23 characterized in that the intermediate bottom has a depending circular wall centered on the container'"'"'s axis and with a diameter smaller than said container inner diameter.

27. A mixer according to claim 23 characterized in that the container has the form of a vertical cylinder with a downward extension which tapers toward the run-off opening.

28. A mixer according to claim 27 characterized in that the intermediate bottom is located at the level where the cylinder and tapered extension of the container are joined.

34. A mixer according to claim 23 characterized in that the run-off flow regulation means is an elastic sleeve valve.

35. A mixer according to claim 23 characterized in that the pluverized solid supply means comprises:

a supply hopper for a pulverized solid, trap means for regulating flow from the hopper, a constant weight weight-sensitive conveyor belt upon which pulverized solid from the hopper is poured and whose unbalance results in a change of trap means position, and a flow rate regulating means for receiving pulverized solid carried by the weight-sensitive conveyor belt comprising a vibrating spout.

36. A mixer according to claim 23 characterized in that the liquid supply means comprises:

a ring-shaped pouring spout adjacent the top of the container and distributing liquid along the inside of the container'"'"'s side wall, a tube directed toward the shaft of the turbine to discharge liquid thereon, and valve means for regulating the rate of flow.

37. A mixer according to claim 23 characterized in that the turbine is placed in the immediate vicinity of the intermediate bottom top surface.

38. A vertical mixer for pulverized solids and liquids comprising:

a container in the form of a vertical cylinder with a downward extension which tapers toward its lower end which has a run-off opening, a downwardly tapered core in the downward extension of the container providing for a ring-shaped space in cross-section between it and the container'"'"'s inner wall and its top providing an intermediate bottom at the level of the junction of the cylinder portion and tapered extension of the container, a turbine mounted inside of the container immediately above the intermediate bottom formed by the core, an ejection device in communication with the run-off opening for transforming the discharge from the run-off opening into a full stream, an elastic sleeve valve in communication with the ejection device and downstream thereof for run-off flow rate regulation, means for continuously supplying a liquid to the container including a ring-shaped pouring spout adjacent the top of the container and distributing liquid along the inside of the container'"'"'s side wall, a tube directed toward the shaft of the turbine to discharge liquid thereon, and valve means for regulating the rate of flow, and means for continuously supplying a pulverized solid to the container including a supply hopper for a pulverized solid, trap means for regulating flow from the hopper, a constant weight weight-sensitive conveyor belt upon which pulverized solid from the hopper is poured and whose unbalance results in a change of trap means position, and a flow rate regulating means for receiving pulverized solid carried by the weight-sensitive conveyor belt comprising a vibrating spout.

39. A continuous process for mixing pulverized solids and liquids such as plaster powder and water characterized in that it comprises

continuously introducing liquid into a mixing container at a selected flow rate,

continuously introducing pulverized solids into said container at a selected flow rate,

said flow rates being selected to provide a desired proportion of solid and liquid,

rotating the solids and liquid in the container to create a vortex thereof and a mixture of the solids and liquid,

rotating the mixture through a ring-shaped space in the container in a spiral descent into a discharge opening, and

continuously passing the mixture through the discharge opening.

40. The continuous process of claim 39,

said ring-shaped space tapering toward the discharge opening, and

rotating the mixture downwardly through the tapered space in ever decreasing circles in its spiral descent.

41. The continuous process of claim 39,

the speed of the mixture being rotated through the ring-shaped space being at least 30 cm per second to prevent premature deposits and mass setting of the mixture.

42. The continuous process of claim 39,

the speed of the mixture being rotated through the ring-shaped space being about 1 meter per second to prevent premature deposits and mass setting of the mixture.

43. The continuous process of claim 39,

the mean time of the solids and liquids in the container being about 15 to 20 seconds.

44. The continuous process of claim 39,

the time of the solids and liquids in the container being about 3 seconds.

45. The continuous process of claim 39, including

introducing at least a portion of the liquid along the interior of the mixing container wall in order to create a continuous sheet of liquid on said interior wall.

46. The continuous process of claim 39, including regulating the output flow of the mixture.

47. A continuous process for mixing pulverized solids and liquids such as plaster powder and water characterized in that it comprises

continuously introducing liquid into a mixing container at a selected flow rate,

continuously introducing pulverized solids into said container at a selected flow rate,

said flow rates being selected to provide a desired proportion of solid and liquid,

rotating the solids and liquid in the container to create a vortex thereof and a mixture of the solids and liquid,

rotating the mixture through a ring-shaped space in the container in a spiral descent into a discharge opening, and

continuously passing the mixture through the discharge opening,

said process including

passing the mixture from the discharge opening into an ejection zone and rotating the mixture in the ejection zone, and

discharging the mixture tangentially from the ejection zone into a collector pipe

48. A continuous process for mixing pulverized solids and liquids such as plaster powder and water characterized in that it comprises

continuously introducing liquid into a mixing container at a selected flow rate,

continuously introducing pulverized solids into said container at a selected flow rate,

said flow rates being selected to provide a desired proportion of solid and liquid,

rotating the solids and liquid in the container to create a vortex thereof and a mixture of the solids and liquid,

rotating the mixture through a ring-shaped space in the container in a spiral descent into a discharge opening, and

continuously passing the mixture through the discharge opening,

said process including

said ejection zone having an inverted cone shape, and

revolving the mixture in ever widening circles in the ejection zone in a spiral descent to the discharge opening so that no uncontrolled vortex is likely to create a motionless zone where mass setting could occur.