Method of cooking cellulose material and preserving the heat and terpentine content of the cooking liquor

• US 4,274,911 A
• Filed: 07/26/1979
• Issued: 06/23/1981
• Est. Priority Date: 07/27/1978
• Status: Expired due to Term

• Current Assignee: Obbola Linerboard AB
• Original Assignee: Obbola Linerboard AB
• Inventors: Andersson, Per-Erik, Kroneld, Erik G.
• Primary Examiner(s): Bashore, S. Leon
• Assistant Examiner(s): Alvo, Steve
• Application Number:
  US06/060,930
• Time in Patent Office: 698 Days
• Field of Search: 162/46, 162/47, 162/68, 162/49, 162/15, 162/16, 162/14, 162/19, 162/239, 162/240, 162/246, 162/DIG. 12, 159/47 WL, 202/185 R, 203/88, 203/22, 203/DIG. 8
• US Class Current: 162/15
• CPC Class Codes: D21C 11/06 Treatment of pulp gases; Recovery of the heat content of the gases; Treatment of gases arising from various sources in pulp and paper mills; Regeneration of gaseous SO2, e.g. arising from liquors containing sulfur compounds

Abstract

A method of cooking cellulose material and effectively preserving the heat and terpentine content of the cooking liquor is disclosed. The cooking liquor is allowed to expand and the expansion steam (blow steam) is conveyed into a bed of cellulose material in a storage container (3'"'"', 3) to heat and impregnate the cellulose material before cooking. A heated zone is maintained in the bed of material below the surface of the bed by regulating the flow of expansion steam into the container. Uncondensed, evil-smelling and poisonous gases are at the same time prevented from flowing out into the atmosphere. These gases are drawn off from the storage container for destruction.

Claims

1. A method for producing chemical pulp by cooking cellulosic material containing terpentine comprising feeding said cellulosic material into a storage container so as to produce a bed of said cellulosic material therein, transporting said cellulosic material from said storage container into a digester, cooking said cellulosic material in said digester so as to produce a cooking liquor containing terpentine therein, removing said cooking liquor from said digester, producing expansion steam containing terpentine from said cooking liquor, introducing at least a portion of said expansion steam into the lower portion of said bed of cellulosic material in said storage container so as to transfer a substantial portion of the heat and terpentine contents of said expansion steam to said cellulosic material and produce a heated zone therein, regulating the flow of said expansion steam introduced into said bed of cellulosic material so that said heated zone is maintined below the surface of said bed, and withdrawing uncondensed gases from said storage container countercurrently to the flow of said cellulosic material into said storage container so as to prevent the entry of air contained in said cellulosic material into said storage container.

2. The method of claim 1 wherein said uncondensed gases withdrawn from said storage container are combusted.

3. The method of claim 1 wherein said cooking is carried out in batches in said digester, and wherein said cooked cellulosic material and said cooking liquor are withdrawn from said digester into a pulp container where said cooking liquor is expanded and said expansion steam is separated therefrom.

4. The method of claim 3 wherein said expansion steam separated from said digester is divided into a first expansion steam portion and a second expansion steam portion, said first expansion steam portion being introduced into said lower portion of said bed of cellulosic material.

5. The method of claim 4 wherein said second expansion steam portion is condensed in a condenser, and wherein said condensate is collected in a condensate container.

6. The method of claim 5 wherein uncondensed gases from said condensate container are introduced into said storage container.

7. The method of claim 6 wherein said uncondensed gases from said condensate container are introduced into said storage container along with said first expansion steam portion.

8. The method of claim 6 wherein said uncondensed gases from said condensate container are introduced into said storage container at a point above the point of introduction of said first expansion steam portion.

9. The method of claim 4 wherein the point of introduction of said first expansion steam portion into said storage container is selected on the basis of the steam content of said gaseous streams with lower steam contents being introduced at higher levels within said bed.

10. The method of claim 5 wherein said condensate container includes a liquid lock to prevent said uncondensed gases from flowing out of said condensate container into the atmosphere while at the same time air is prevented from flowing into said condensate container.

11. The method of claim 10 including supplying liquid to said liquid lock so as to fill said liquid lock and to prevent blocking of said liquid lock with said cellulosic material.

12. The method of claim 1 including recovering said terpentine from steam withdrawn from said digester, and returning any uncondensed gases produced during said recovery step to said storage container.

13. The method of claim 1 wherein said cooking is carried out continuously, and including steaming said cellulosic material transported from said storage container prior to said cooking.

14. The method of claim 13 wherein said expansion steam is produced from said cooking liquor in a plurality of stages, so as to produce a first expansion steam portion and a second expansion steam portion, said first expansion steam portion being introduced into the lower portion of said bed of cellulosic material, and said second expansion steam portion being used for steaming said cellulosic material prior to its entry into said digester.

15. The method of claim 14 wherein uncondensed gases containing terpentine are produced from said cooking liquor and are introduced into said storage container.

16. The method of claim 15 wherein said uncondensed gases are introduced into said storage container at a level above the heated zone in said bed but below the surface of said bed of cellulosic material.

17. The method of claim 14 wherein said first expansion steam portion is divided into a third expansion steam portion and a fourth expansion steam portion, said third expansion steam portion being introduced into the lower portion of said bed of cellulosic material and said fourth expansion steam portion being condensed to produce a condensate therefrom.

18. The method of claim 17 wherein uncondensed terpentine is removed from said condensate in a column wherein said condensate is contacted with steam.