Apparatus for measuring the concentrations of elements in a material by the capture gamma method

• US 4,278,885 A
• Filed: 05/02/1979
• Issued: 07/14/1981
• Est. Priority Date: 05/04/1978
• Status: Expired due to Term

• Current Assignee: Outokumpu Oyj
• Original Assignee: Outokumpu Oyj
• Inventors: Sipila, Heikki J., von Alfthan, Georg C., Uusitalo, Seppo J., Lukander, Tuula A., Rautala, Pekka
• Primary Examiner(s): Willis, Davis L.
• Application Number:
  US06/035,245
• Time in Patent Office: 804 Days
• Field of Search: 250/253, 250/302, 250/303, 250/358 R, 250/390, 250/391, 250/392, 250/435 R, 250/370
• US Class Current: 250/370.01
• CPC Class Codes: G01N 23/221 by activation analysis

Abstract

The invention provides an apparatus for measuring the concentrations of elements in a material sample by the capture gamma method, said apparatus including a neutron source in the form of an isotope source or a neutron generator, a moderator surrounding the neutron source and being at least partly constituted by heavy water, a semiconductor detector serving as gamma radiation detector and positioned in the immediate vicinity of the material to be analyzed and in the flux of slow neutrons, so much of the moderator being provided before the detector that this is reached only by a very low number of fast neutrons that have a damaging effect upon the detector. The material itself can form part of the moderator and also graphite is preferably used as a moderator around said heavy water. Furthermore, a body of bismuth having the shape of a cone or a double cone is preferably positioned in front of the neutron source so as to absorb gamma radiation and to scatter fast neutrons.

Claims

1. An apparatus for measuring the concentrations of elements in a material by the capture gamma method, said apparatus comprising

a neutron source,

a moderator surrounding the neutron source and being at least partly constituted by heavy water,

a gamma radiation detector in the form of a semiconductor detector, said detector being positioned close to the material to be measured and in a flux of slow neutrons, there being so much of the moderator between the neutron source and the detector that at most only a few fast neutrons can reach the detector.

2. An apparatus according to claim 1, wherein part of the moderator is graphite.

3. Apparatus according to claim 2 wherein the graphite is situated around the heavy water.

4. An apparatus according to claim 1 or 2, further comprising as moderator substance ordinary water.

5. An apparatus according to claim 1, wherein a heavy substance which absorbs neutrons only slightly is placed between the neutron source and the detector to absorb gamma-radiation and to scatter fast neutrons.

6. An apparatus according to claim 5, wherein the scattering substance has the shape of a cone, the neutron source being situated in the vicinity of the cone apex, and the base of the cone facing the detector.

7. An apparatus according to claim 5, wherein the distance between the scattering substance and the semiconductor detector in heavy water is at least about 10 cm.

8. Apparatus according to claim 5 wherein the heavy substance is bismuth.

9. Apparatus according to claim 5 wherein the scattering substance has the shape of two cones in succession, the neutron source being situated in the vicinity of the apex of one of the cones, and the base of the other cone facing the detector.

10. An apparatus according to any of claims 1, 2, 5 or 6, wherein the intensity of the neutron source is about 5.10⁷ neutrons/s, the distance between the neutron sourse and the detector is at least about 45 cm, this distance increasing by about 15 cm when the intensity increases by one decade.

11. Apparatus according to claim 10 further comprising as moderator substance ordinary water.

12. An apparatus according to any one of claims 1, 2, 5, or 6, wherein the intensity of the neutron source is about 5.10⁷ neutrons/s, the distance between the neutron source and the detector is at least about 45 cm, this distance increasing by about 15 cm when the intensity increases by one decade, and wherein the heavy water has been arranged around the neutron source, substantially in the form of a truncated cone, the neutron source being situated at the narrow end of the cone and the detector being situated at the wider end of the cone.

13. Apparatus according to claim 12 further comprising as moderator substance ordinary water.

14. An apparatus according to claim 1, wherein the material to be studied flows in a pipe, the detector being positioned inside the pipe in the flowing material, which itself partly serves as a moderator.

15. An apparatus according to claim 1, wherein the neutron source is an isotope source.

16. An apparatus according to claim 1, wherein the neutron source is a neutron generator.