Fluid sample cell
First Claim
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1. A fluid sample cell for the spectroscopic analysis of a fluid sample, comprising:
- a sample compartment formed in said cell for the containment of a fluid sample, said compartment being defined on opposite sides by a radiation energy-transmitting window and a diffuse reflector spaced from said window, and means for supporting opposing surfaces of said window and said diffuse reflector in spaced fashion, said diffuse reflector being adapted to redirect light incident thereon through a fluid sample contained therebetween and said window, whereby all of said redirected light passing through said window has the character of being diffusely reflected.
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Abstract
A fluid sample cell comprising a sample compartment of precisely predetermined depth bounded by opposed surfaces of a transparent window and a diffuse mirror is disclosed, and comprises inlet and outlet ports for the flow of a series of successive samples into and through said sample compartment and the spectroscopic analysis thereof by irradiation and detection of transmitted and reflected radiation.
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Citations
11 Claims
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1. A fluid sample cell for the spectroscopic analysis of a fluid sample, comprising:
- a sample compartment formed in said cell for the containment of a fluid sample, said compartment being defined on opposite sides by a radiation energy-transmitting window and a diffuse reflector spaced from said window, and means for supporting opposing surfaces of said window and said diffuse reflector in spaced fashion, said diffuse reflector being adapted to redirect light incident thereon through a fluid sample contained therebetween and said window, whereby all of said redirected light passing through said window has the character of being diffusely reflected.
- View Dependent Claims (2, 3, 4)
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5. A spectroscopic analysis apparatus, comprising:
- a fluid sample cell including a sample compartment for the containment of a fluid sample to be analyzed, said compartment being defined by a radiation-transmitting window and a diffuse reflector spaced from said window, opposing surface portions of said window and said diffuse reflector being supported in spaced fashion, inlet and outlet ports extending into said compartment for passing successive fluids samples, in turn, through said compartment, a radiation energy source for directing energy through said window and into said compartment, and means for collecting radiation scattered, whether in a forward or back direction, and radiation transmitted by said sample contained within said compartment, at least a portion of said forward scattered and transmitted radiation being reflected back from said diffuse reflector and through said sample, so as to minimize the effects of variations in light scattering on the accuracy of the spectroscopic measurement.
- View Dependent Claims (6, 7, 8, 9, 10)
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11. A method for the spectroscopic analysis of a property of a fluid sample, comprising the steps of:
- locating a fluid sample between a radiant energy-transmitting window and a diffuse reflector, said window and said diffuse reflector being supported in spaced fashion, for irradiating said fluid sample with selected wavelengths of radiant energy, collecting at least a representative portion of radiation scattered, whether in a forward or backward direction, and radiation transmitted by said fluid sample, at least a portion of said forward scattered and transmitted radiation being reflected back from said diffuse reflector and through said fluid sample for collection, integrating said collected radiation, and generating a signal in accordance with said collected radiation, as an indication of said property, so as to minimize the effects of variations in light scattering on the accuracy of the spectroscopic measurement.
Specification