Gas chromatographic chamber

• US 4,286,456 A
• Filed: 08/09/1979
• Issued: 09/01/1981
• Est. Priority Date: 11/22/1978
• Status: Expired due to Term

• Current Assignee: Carlo ERBA Strumentazione SPA
• Original Assignee: Carlo ERBA Strumentazione SPA
• Inventors: Riva, Ermete, Sisti, Giorgio, Sala, Learco
• Primary Examiner(s): Goldberg, Gerald
• Assistant Examiner(s): ROSKOS, JOSEPH
• Application Number:
  US06/065,333
• Time in Patent Office: 754 Days
• Field of Search: 73/23.1, 219/201
• US Class Current: 73/23.25
• CPC Class Codes: B01D 53/025 with wetted adsorbents; Chromatography analytical chromatography G01N30/00 - G01N30/96; for liquids B01D15/08
• CPC Class Codes: G01N 2030/3084 ovens
• CPC Class Codes: G01N 30/30 of temperature

Abstract

A gas chromatographic chamber in the form of an oven is disclosed, including an outer envelope including insulated walls defining the chromatographic chamber which can be made air tight, an inner housing section within that chamber for housing the chromatographic column, and including an air distributor to maintain the uniform distribution of air within the inner housing section, as well as a heater to heat the air therein, non-thermally insulating partitions within the chamber and spaced from the insulated wall to provide a pneumatically insulated space between the insulated walls and the inner housing section, and a fluid circulator to create the controlled circulation of fluid within the pneumatically insulated space to effect the temperature within the inner housing section.

Claims

1. A gas chromatographic chamber comprising an outer envelope including insulated wall members defining said chamber which may be closed in an air-tight manner, an inner housing section within said chamber, said inner housing section adapted to include at least one chromatographic column and including inner housing section air distribution means for maintaining a uniform distribution of the air within said inner housing section and inner housing section heating means for heating the air within said inner housing section, non-thermally insulating partition means within said chamber and spaced from said insulated wall members so as to provide a pneumatically insulated space between said insulated wall members and said inner housing section, said non-thermally insulating partition means defining said inner housing section, and circulation means for creating a controlled circulation of fluid within said pneumatically insulated space so as to affect the temperature within said inner housing section.

2. The gas chromatographic chamber of claim 1 including inlet duct and outlet duct means connected to said penumatically insulated space through said insulated wall members whereby a fluid may be circulated through said pneumatically insulated space from said inlet duct means to said outlet duct means.

3. The gas chromatographic chamber of claim 2 including baffle means located in said pneumatically insulated space for dividing said fluid being circulated through said pneumatically insulated space into a plurality of fluid currents.

4. The gas chromatographic chamber of claim 2 wherein said fluid comprises ambient air.

5. The gas chromatographic chamber of claim 2 wherein said fluid comprises a gas maintained at a temperature below ambient temperature.

6. The gas chromatographic chamber of claim 2 including conduit means for connecting said inlet duct means to said outlet duct means to create a closed circuit including said pneumatically insulated space, and including cooling means located in said closed circuit between said outlet duct means and said inlet duct means for cooling said fluid circulated therethrough.

7. The gas chromatographic chamber of claim 6 wherein said cooling means comprises a heat exchanger of a refrigeration system.

8. The gas chromatographic chamber of claim 7 wherein said conduit means includes opening means for selectively permitting connection of said conduit means with a source of air.

9. The gas chromatographic chamber of claim 8 including a plurality of said opening means.