Droplet forming apparatus for use in producing uniform particles

• US 4,302,166 A
• Filed: 03/15/1979
• Issued: 11/24/1981
• Est. Priority Date: 04/22/1976
• Status: Expired due to Term

• Current Assignee: Coulter Electronics, Inc.
• Original Assignee: Coulter Electronics, Inc.
• Inventors: Fulwyler, Mack J., Hatcher, C. William
• Primary Examiner(s): Czaja, Donald E.
• Assistant Examiner(s): Hall, James R.
• Application Number:
  US06/020,818
• Time in Patent Office: 985 Days
• Field of Search: 425/6, 425/5, 264/9, 264/4
• US Class Current: 425/6
• CPC Class Codes: B01J 13/04 by physical processes, e.g. drying, spraying
• CPC Class Codes: Y10S 376/916 Methods of making fusion fuel targets

Abstract

Uniform particles are produced by introducing a laminar stream of a core liquid into a laminar flowing body of an immiscible sheath liquid. The core liquid or the sheath liquid, or both liquids, can contain one or more materials dispersed (dissolved or suspended) in them from which the uniform particles are formed. The two liquids and the dispersed material are expelled from a nozzle to form a liquid jet. The liquid jet is disturbed at a uniform, periodic rate to form liquid droplets which contain a uniform amount of the core liquid, the sheath liquid and the dispersed material. The droplets are collected and held in a catch liquid until the core and the sheath liquid in each droplet have diffused into the catch liquid leaving the uniform particles formed from the dispersed materials. There can be more than one sheath liquid which can also contain one or more materials dispersed in it.

Claims

1. A droplet forming apparatus for producing uniformly sized solid particles from dispersed material in at least one of a core and sheath liquids which are immiscible with each other and supplied to the apparatus from a source of said liquids, said apparatus comprising:

means for connecting the source of core liquid to the apparatus;

means for connecting the source of sheath liquid to the apparatus;

means for forming a moving body of at least one sheath liquid for laminar movement through the apparatus;

means for introducing said core liquid as a laminar stream into said moving body at a selected location along the path of movement of the moving body through the apparatus;

means for producing a liquid jet from said moving body after said introduction of said core liquid;

disturbance means for periodically disturbing said liquid jet to separate said liquid jet including said core and said sheath liquids into unconnected uniform droplets containing a uniform amount of said disbursed material, said core liquid and said sheath liquid; and

means to collect said formed droplets in a catch liquid in which said sheath liquid and said core liquid are each soluble, whereby said sheath liquid and said core liquid are dissolved therein to render the material dispersed in said core liquid into said uniformily sized solid particles.

2. An apparatus according to claim 1 wherein said disturbance means includes:

means for uniformly and periodically disturbing said liquid jet at a constant rate in a transverse direction thereto.

3. An apparatus according to claim 1 wherein said means for introducing includes:

means for introducing said core liquid substantially into the center of said moving body of sheath liquid.

4. An apparatus according to claim 1 wherein said means for introducing includes:

means for introducing said core liquid substantially coaxial with the axis of said moving body of sheath liquid.

5. An apparatus according to claim 1 further including:

charging means for applying like-repelling charges to each of said uniform droplets.