Alcohol recovery process

• US 4,309,254 A
• Filed: 04/17/1980
• Issued: 01/05/1982
• Est. Priority Date: 04/17/1980
• Status: Expired due to Term

• Current Assignee: Stone & Webster Engineering Corporation (Brookfield Asset Management Incorporated)
• Original Assignee: Stone & Webster Engineering Corporation (Brookfield Asset Management Incorporated)
• Inventors: Rubin, Jacob N., Dahlstrom, Rodney A.
• Primary Examiner(s): BASCOMB JR, WILBUR
• Application Number:
  US06/141,256
• Time in Patent Office: 628 Days
• Field of Search: 203/19, 203/39, 203/47, 203/100, 203/74-80, 203/98, 203/97, 203/96, 203/DIG. 13, 203/DIG. 16, 203/DIG. 8, 203/27, 203/26, 159/17 P, 159/47 R, 426/492-495, 426/624, 426/31, 426/18, 426/468, 426/456, 426/465, 426/469, 426/472, 426/478, 426/173, 202/174, 202/154, 202/234, 202/155, 202/176, 202/172, 435/161
• US Class Current: 203/47
• CPC Class Codes: B01D 1/26 Multiple-effect evaporating
• CPC Class Codes: B01D 3/001 Processes specially adapted for distillation or rectification of fermented solutions
• CPC Class Codes: B01D 3/148 in combination with at least one evaporator
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel
• CPC Class Codes: Y10S 203/11 Batch distillation
• CPC Class Codes: Y10S 203/14 Ejector-eductor
• CPC Class Codes: Y10S 203/17 Saline water conversion

Abstract

A process for the production of alcohol from a fermented feed wherein insoluble organic matter is separated prior to entry into a first distillation column. The insoluble organic matter is dried under pressure to produce dried distillers grain and wherein excess vapor is removed from the drying zone to provide heat to the distillation system. The present process also includes removing excess water vapor from the evaporation zone, obtained from supplemental heating supplied by the overhead from said first distillation column, compressing said water vapor, and recycling it to the distillation columns and the evaporation zone.

Claims

1. In a distillation method for the production of anhydrous alcohol from a fermented feed wherein the fermented feed is distilled in a first distillation column to obtain an alcohol portion as an overhead, introducing said alcohol portion to at least one additional distillation column, removing as a bottom from said first distillation column a lean mash primarily containing dissolved organic matter, separating said lean mash into a first spent feed and a second spent feed, introducing said first spent feed as a sidestream into an evaporation zone having at least two successively decreasing pressure regions, and removing a concentrated first spent feed from a lower pressure region of said evaporation zone, the improvement comprising:

(a) separating said fermented feed into a first fermented feed containing dissolved organic matter and a second fermented feed containing insoluble organic matter;

(b) introducing said first fermented feed as a sidestream into said first distillation column and said second fermented feed into a drying zone;

(c) drying said second fermented feed in said drying zone at a pressure greater than the pressure of a lower region of said distillation column;

(d) removing a pressurized vapor stream from said drying zone; and

(e) introducing said pressurized vapor stream as a sidestream into the lower region of said first distillation column.

2. The process of claim 1 further comprising introducing said concentrated first spent feed into said drying zone.

3. The process of claim 2 wherein said concentrated first spent feed is combined with said second fermented feed to thereby form a combined feed, introducing said combined feed into said drying zone and drying said combined feed to thereby obtain Distillers Dried Grain.

4. The process of claim 1 wherein said second spent feed is returned to a fermenting region.

5. The process of claims 1 or 2 wherein said drying zone has a pressure between about 15 and 70 psia.

6. The process of claim 5 wherein said pressure is between about 35 and 55 psia.

7. The process of claims 1 or 2 wherein said drying zone comprises a steam tube dryer having at least two drying tubes and is heated by steam under pressure in the range of between about 135 and 180 psia.

8. The process of claims 1 or 2 further comprising diverting a part of said pressurized vapor stream to said additional distillation columns.

9. The process of claims 1 or 2 further comprising removing water vapor as an overhead from one of said pressure regions of said evaporation zone, compressing said water vapor, introducing a first portion of said compressed water vapor to the highest pressure region of said evaporation zone, a second portion to said first distillation column and a third portion to said additional distillation columns.

10. The process of claim 9 wherein the highest pressure region of said evaporation zone has a pressure of between about 15 and 45 psia and a temperature of between about 212°

and 275°

F. and the lowest pressure region has a pressure of between about 1.0 and 20 psia and a temperature of between about 100° and

230°

F.

11. The process of claim 9 wherein the water vapor removed from one of said pressure regions is compressed to a pressure greater than the pressure of the lower region of said first distillation column.