Inert-gas stripping and distillation apparatus

• US 4,327,184 A
• Filed: 10/25/1979
• Issued: 04/27/1982
• Est. Priority Date: 10/25/1979
• Status: Expired due to Term

• Current Assignee: University of Utah Research Foundation (State of Utah)
• Original Assignee: University of Utah (State of Utah)
• Inventors: Johnson, Steven A., Seader, Junior D.
• Primary Examiner(s): Bascomb, Jr., Wilbur L.
• Application Number:
  US06/088,254
• Time in Patent Office: 915 Days
• Field of Search: 203/19, 203/49, 203/92, 203/93, 203/95-97, 203/87, 203/DIG. 13, 203/DIG. 16, 202/158, 202/234, 202/186, 435/161, 435/313, 435/93, 435/287, 435/162, 435/165, 435/163, 435/164, 426/494, 426/493, 568/916
• US Class Current: 435/300.1
• CPC Class Codes: B01D 3/001 Processes specially adapted for distillation or rectification of fermented solutions
• CPC Class Codes: B01D 3/14 Fractional distillation or use of a fractionation or rectification column
• CPC Class Codes: B01D 3/346 the gas being used for removing vapours, e.g. transport gas
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel
• CPC Class Codes: Y10S 203/14 Ejector-eductor
• CPC Class Codes: Y10S 203/17 Saline water conversion

Abstract

A distillation/evaporation/drying apparatus wherein alcohol is removed by a dry, warm carrier gas from an alcohol-containing slurry from a fermenter. Carbon dioxide from the fermenter is used as the carrier gas and is suitably dried, warmed and recycled into contact with the slurry to assist in removing alcohol therefrom. The apparatus includes a reflux section to upgrade the alcohol content of the carrier gas.

Claims

1. A distillation apparatus comprising:

distillation means;

first condenser means connected to the distillation means for condensing a product from a carrier gas;

circulation means for circulating the carrier gas through the distillation means and the first condenser means, the carrier gas carrying the product from the distillation means to the first condenser means;

fermentation means for producing a product-containing slurry;

first conduit means for delivering the product-containing slurry from the fermentation means to the distillation means;

second condenser means connected to the fermentation means for recovering gases generated in the fermentation means;

second conduit means for delivering the gases recovered in the second condenser means to the circulation means for use as at least a part of the carrier gas;

and

first removal means for removing the product from the first condenser means.

2. A distillation apparatus as defined in claim 1 wherein the distillation means has a lower, stripping section and an upper, rectifying section, said stripping section having a plurality of downwardly slanted baffles for exposing the product-containing slurry to the carrier gas.

3. A distillation apparatus as defined in claim 2 wherein the distillation means further comprises:

storage means for storing a bottoms product; and

recirculation means for recirculating the bottoms product to the stripping section of the distillation means.

4. A distillation apparatus as defined in claim 3 wherein the storage means for said bottoms product comprises a settling zone and a clarified zone.

5. A distillation apparatus as defined in claim 4 further comprising second removal means for removing the bottoms product from the settling zone of the storage means.

6. A distillation apparatus as defined in claim 1 further comprising:

a storage means for storing excess gases generated in the fermentation means for subsequent use in the distillation apparatus; and

means for transferring the gases from the second condenser means to the storage means.

7. A distillation apparatus as defined in claim 1 wherein the circulation means comprises means for forcing the carrier gas through the distillation column and heater means for heating the carrier gas.

8. An apparatus for the recovery of alcohol from a fermenting material comprising:

fermentation means for producing an alcohol-containing slurry;

a distillation column having a lower, stripping section and an upper, rectifying section, said stripping section having a plurality of downwardly slanted baffles;

first conduit means for delivering the alcohol-containing slurry from the fermentation means to the distillation column;

a first condenser connected to the distillation column for condensing alcohol from a carrier gas;

circulation means for circulating the carrier gas through the distillation column and first condenser, the carrier gas carrying the product from the distillation column to the first condenser;

a second condenser connected to the fermentation means for recovering carbon dioxide generated in the fermentation means;

second conduit means for delivering the carbon dioxide recovered in the second condenser to the circulation means for use as at least a part of the carrier gas;

and

first removal means for removing the product from the first condenser.

9. An apparatus as defined in claim 8 wherein the distillation column further comprises:

a vessel for storage of a bottoms product; and

recirculation means for recirculating said bottoms product to the stripping section of the distillation column.