Mixing apparatus

• US 4,333,356 A
• Filed: 04/15/1980
• Issued: 06/08/1982
• Est. Priority Date: 04/27/1979
• Status: Expired due to Term

• Current Assignee: Ciba-Geigy Corporation (Novartis Ag)
• Original Assignee: Ciba-Geigy Corporation (Novartis Ag)
• Inventors: Huber, Walter, Bartels, Hermann, Mez, Hans-Christian, Stolz, Hans-Peter
• Primary Examiner(s): Swisher, S. Clement
• Application Number:
  US06/140,536
• Time in Patent Office: 784 Days
• Field of Search: 73/423 A, 422/62, 422/63, 422/64, 422/65, 422/67, 422/81, 422/82, 364/502, 364/510, 222/134, 222/135, 222/144.5, 222/145, 137/99, 137/100, 417/3, 417/4, 417/5, 417/6, 417/426
• US Class Current: 73/864.21
• CPC Class Codes: B01F 35/8821 involving controlling
• CPC Class Codes: G01N 1/38 Diluting, dispersing or mixing samples
• CPC Class Codes: G05D 11/132 by controlling the flow of the individual components G05D11/133 takes precedence
• CPC Class Codes: Y10T 137/2516 Interconnected flow displacement elements

Abstract

A mixing apparatus utilizes piston burettes driven by stepping motors as metering pumps to deliver component liquids to be mixed into a liquid stream in a selectable constant mixing ratio. A computer-based automatic control system is used to control the regulated take up of the respective components by the burettes and the delivery of them to a mixing device. The computer calculates the rates of stepping of the respective motors so that each component is delivered over the same period of time and at a respective uniform rate. The computer also controls associated switching valves via an interface device and may be a desk top machine with keyboard or pre-programmed data input.

Claims

1. In a mixing apparatus for producing a liquid having a plurality of components mixed in a selected ratio which comprises flow means for receiving the respective components, and a plurality of metering pumps for the respective components connected to said flow means and operable to cause delivery thereto of the components, each pump having a respective stepping motor as a drive motor and comprising a piston burette, the piston of which is driven by said stepping motor to sweep a predetermined increment of volume in response to each step of the stepping motor,

the improvement comprising an automatic control means connected to the pump motors to control same and being operable to supply individual control signals thereto as respective trains of pulses, said control means having input means for receiving input data determining the selected mixing ratio and including computer means (a) being responsive to such input data to compute and establish the pulse interval for each pulse train such that the pumps cause quantities of the respective components to be delivered to said flow means in the same period of time in accord with said selected ratio and at a respective uniform rate during said period and (b) being arranged to compute initial piston positions for the burettes in accord with the quantities of the respective components to be delivered to the flow means in accord with said selected ratio;

and said automatic control means further including an interface device connected to each stepping motor and responsive to commands generated by the computer means to supply pulses to the associated stepping motor to establish the initial position of the associated burette piston and to subsequently control the supply of the train of pulses to the stepping motor to cause delivery of the associated component to said flow means.

2. Apparatus as claimed in claim 1 in which the automatic control means includes a pulse clock source and the computer computes the pulse interval for each pulse train as an integral multiple of the clock pulse interval.

3. Apparatus as claimed in claim 2 in which the computer means is arranged to perform a set of computational steps comprising:

computing from input data determining the ratio of the quantities of two components to be delivered to the flow means by first and second metering pumps and from a first number of clock source intervals assigned as the pulse interval for the pulse train to the stepping motor of said first pump, a second number (not necessarily integral) of clock pulse intervals required to be assigned to the pulse interval of the pulse train to the stepping motor of said second metering pump to cause delivery to said flow means in the same period of time of the quantities of respective components by said first and second pumps in said selected ratio, and computing the extent by which the second number deviates from an integer;

the computer means being arranged to repeat this set of computational steps incrementing the first number employed in the previous set of steps by one until the extent of deviation of the second number from an integer does not exceed a predetermined limit, and to establish the integer so obtained as the number of clock pulse intervals constituting the pulse interval for the train of pulses to the stepping motor of said second pump.

4. Apparatus as claimed in claim 3 in which, in response to the input data, said computer means is arranged to express the ratio of the components pertaining to said first and second pumps in terms of respective numbers of step increments of the piston burettes and use the ratio of said numbers of step increments in performing said set of computational steps.

5. Apparatus as claimed in claim 1 in which said interface device includes a microprocessor device providing two-way communication between said computer means and each metering pump, whereby the automatic control system operates with distributed processing.

6. Apparatus as claimed in claim 1 in which said flow means comprises a mixing device connected to each piston burette through a respective controllable change-over valve, said automatic control means being arranged to control said change-over valve and being operable in a first condition to set said change-over valves to first positions connecting the piston burettes to the mixing device for the delivery thereto of quantities of respective components in accord with the selected ration, and being operable in a second condition to set said change-over valves to second positions in which the piston burettes are able to receive further quantities of the respective components.

7. Apparatus as claimed in claim 6 further comprising a controllable multi-way valve connected to one of said change-over valves so as to be in communication with the associated piston burette associated with said one change-over valve in the second position of the latter, said automatic control means being arranged to control said multi-way valve to select one of a plurality of liquid component sources for connection to said associated piston burette during said second condition of said automatic control means.

8. Apparatus as claimed in claim 1 in which each piston burette is connected to said flow means through a respective change-over having a first position in which the associated piston burette is in communication with said flow means for causing delivery thereto of a respective component and having a second position in which the associated piston burette is isolated from the flow means for setting to an initial piston position prior to such delivery, said automatic control means being arranged to control the change-over valves and being operable in first and second conditions to set all the valves to said first positions respectively.

9. Apparatus as claimed in claim 8 further comprising a controllable multi-way valve connected to one of said change-over valves to be coupled to the associated piston burette in the second position of said one change-over valve, automatic control means being arranged to control said multi-way valve to select one of a plurality of component sources.

10. Apparatus as claimed in claims 6 or 8 in which one of said change-over valves is connected to a discharge line in said second position thereof and further comprising an inlet line for a component connected to said one change-over valve through said flow means.

11. Apparatus as claimed in claim 1 further comprising a sample changer device for locating a selected one of a plurality of vessels at an operating station and an inlet line for one of said metering pumps located at said station to take up liquid from a vessel selectively located at said station, the sample changer being connected to said automatic control means for selective location of said vessels at said operating station.