Filter indexing for spectrophotometer system

• US 4,342,516 A
• Filed: 03/07/1980
• Issued: 08/03/1982
• Est. Priority Date: 03/07/1980
• Status: Expired due to Term

• Current Assignee: Perkinelmer Incorporated
• Original Assignee: Perkinelmer Incorporated
• Inventors: Williams, Paul B., Chamran, Morteza M., Scott, Larkin B.
• Primary Examiner(s): McGraw, Vincent P.
• Application Number:
  US06/128,030
• Time in Patent Office: 879 Days
• Field of Search: 356/326, 356/328, 356/329, 356/332, 356/333, 356/334
• US Class Current: 356/332
• CPC Class Codes: G01J 3/12 Generating the spectrum; Monochromators

Abstract

A spectrophotometer system has an optical system for transmitting a beam from a source at select wavelengths onto a detector. A plurality of filters are positioned in a tray. A stepper mechanism indexes the tray along a path. A microcomputer controls the stepper mechanism and the optical system. The wavelength is successively changed over a range, the tray is indexed to move a select filter into the beam at a predetermined wavelength and the changing is discontinued during indexing.

Claims

1. A spectrophotometer system comprising a first radiant energy source and a second radiant energy source for generating a beam of radiant energy, an optical system for transmitting the beam of radiant energy at preselected wavelengths through a sample cell and onto a detector, the combination further comprising:

a filter tray movably mounted for movement along a path, said filter tray including control means for selecting the source of radiant energy to be transmitted depending on the position occupied by said tray;

a plurality of filters positioned in said tray for movement through the beam of radiant energy as said filter tray is moved along said path, said filters being positioned on said tray for independent presentation in said beam;

stepper means for indexing said tray in discrete steps along said path and

microcomputer means for controlling said optical system for successively changing the wavelength of the beam of radiant energy over a predetermined spectral range, and said microcomputer means including means for selecting any limited wavelength range to scan within the larger spectral range of the system, said microcomputer means being connected to said stepper means for indexing said tray a plurality of steps for moving a select filter into the radiant energy beam and for selecting the source of radiant energy at only predetermined wavelengths of said spectral range, said microcomputer means being caused to discontinue changing said wavelength during indexing of said tray.

2. A spectrophotometer system according to claim 1 and further including:

recorder means for recording an indication of the results computed from the response of said detector, said recorder means having an area of record receiving material and a motor means for driving traversing said area, and wherein said microcomputer means electrically communicates with said motor means for stopping recording on said area of record material during indexing of said tray.

3. A spectrophotometer system according to claim 1 and further including:

display means operationally controlled by said microcomputer means for visually displaying an indication of the wavelength of the radiant energy beam being transmitted by the optical system; and

wherein said microcomputer means electrically communicates with said display means for indexing the visual display in relation to each said change in wavelength of the energy beam.

4. A spectrophotometer system according to claim 1 wherein said plurality of filters includes an ultra-violet filter and a red filter.

5. A spectrophotometer system according to claim 1,

wherein said radiant energy source includes an incandescent lamp for generating radiant energy and a deuterium lamp for generating radiant energy;

and wherein said filter tray includes control means operable when said tray occupies a preselected range of positions along said path for transmitting radiant energy from said deuterium lamp to said optical system; and

wherein said microcomputer means indexes said tray to said preselective range of positions at predetermined wavelengths of said spectral range.

8. A spectrophotometer system according to claim 1 or claim 5 wherein said control means includes a mirror section and a light permeable section on said filter tray positionable in the radiant energy paths from said radiant energy sources for selecting the source of radiant energy to be transmitted.

6. A spectrophotometer system comprising:

first and second source means for generating a radiant energy beam;

filter means comprising at least a first filter and a second filter, a filter and source changer for independently presenting a separate one of said first and second filters to a position for filtering said radiant energy beam and for selecting one of said first and second source means for generating a radiant energy beam;

an optical system including a diffraction means for receiving said radiant energy beam and for generating monochromatic radiant energy, said optical system responsive to a wavelength control signal for sequencing the wavelength of said monochromatic radiant energy over a predetermined spectral range;

detection means positioned for receiving said radiant energy transmitted by said optical system and responsively producing a sample signal;

recorder means for recording information carried by said sample signal for generating a record of the results computed from the response of said detection means; and

microcomputer means for transmitting said wavelength control signal to said optical system for sequencing said wavelength, and for actuating said filter and source changer, and said microcomputer means including means for selecting any limited wavelength range to scan within the larger spectral range of the system, said microcomputer means discontinuing transmission of said wavelength control signal during actuation of said filter means to present a separate filter to said position.

7. A spectrophotometer system according to claim 6 and further including a mechanical indexing stop, the microcomputer means being further programmed for controlling the stepper means to index the tray to the stop when establishing an initial position of the wavelength control means.