Method for manufacture of powder composition for cordierite

• US 4,367,292 A
• Filed: 07/29/1981
• Issued: 01/04/1983
• Est. Priority Date: 08/05/1980
• Status: Expired due to Fees

• Current Assignee: Kabushiki Kaisha Square Enix
• Original Assignee: Agency of Industrial Science & Technology (Government of Japan), Ministry of International Trade & Industry (Government of Malaysia)
• Inventors: Takagi, Hiroyoshi, Sano, Shiro
• Primary Examiner(s): Poer, James
• Application Number:
  US06/288,022
• Time in Patent Office: 524 Days
• Field of Search: 501/109, 501/118, 501/19, 501/153, 501/154, 423/328, 423/329, 423/330
• US Class Current: 501/119
• CPC Class Codes: C01B 33/26 Aluminium-containing silicates , i.e. silico-aluminates
• CPC Class Codes: C04B 35/195 Alkaline earth aluminosilicates, e.g. cordierite or anorthite

Abstract

A powder composition for producing cordierite is obtained by mixing a water-soluble magnesium salt; a water-soluble aluminum salt; a silicon source selected from the group consisting of organic silicon compounds, silica, silica sol and, silica gel; and an organic solvent, adding to the resultant mixture an ammonia-alkaline solution of ammonium carbonate thereby producing a precipitate, separating the precipitate, and drying the separated precipitate.

Claims

1. A method for the manufacture of a powder composition for cordierite, which comprises preparing water containing a water-soluble magnesium salt, a water-soluble aluminum salt, and at least one silicon source selected from the group consisting of (a) an organic silicon compound and (b) at least one member selected from the group consisting of finely divided silicon oxide, silica gel, and silica sol in amounts calculated to correspond to a cordierite percentage composition as Mg, Al, and Si, mixing this water with a water-soluble organic solvent thereby producing a mixed solution, then adding to said mixed solution an ammonia-alkaline ammonium carbonate solution thereby inducing precipitation, and separating and drying the precipitate.

3. The method according to claim 1, wherein the mixed solution of the water containing Mg, Al, and Si in the proportions corresponding to a cordierite percentage composition and the water-soluble organic solvent is produced by preparing an aqueous solution having dissolved therein a water-soluble magnesium salt, a water-soluble aluminum salt, and at least one member selected from the group consisting of finely divided silicon oxide, silica sol, and silica gel, and then adding to said aqueous solution a water-soluble organic solvent, with said salts and silicon oxide used in amounts calculated to give said proportions.

4. The method according to claim 1, 2 or 3, wherein the water-soluble organic solvent is at least one member selected from the group consisting of methanol, ethanol, propanol, acetone, and ethylene glycol.

2. A method for the manufacture of a powder composition for cordierite, which comprises, preparing an aqueous solution having dissolved therein a water-soluble magnesium salt and a water-soluble aluminum salt, then adding to said aqueous solution a water-soluble organic solvent, and further adding thereto first an organic silicon compound and then an acid, with said salts and organic silicon compound used in amounts calculated to correspond to a cordierite percentage composition.