Process for producing ethanol by continuous fermentation of polysaccharide-containing raw materials

• US 4,376,163 A
• Filed: 09/23/1980
• Issued: 03/08/1983
• Est. Priority Date: 10/01/1979
• Status: Expired due to Term

• Current Assignee: ALFA Laval AB
• Original Assignee: ALFA Laval AB
• Inventors: Ehnstrom, Lars K. J.
• Primary Examiner(s): Jones, Raymond N.
• Assistant Examiner(s): Tarcza, John E.
• Application Number:
  US06/189,571
• Time in Patent Office: 896 Days
• Field of Search: 435/161, 435/162, 435/163, 435/813, 435/163, 435/164, 203/19, 426/7, 426/11, 426/13, 426/14
• US Class Current: 435/162
• CPC Class Codes: C12P 7/06 Ethanol, i.e. non-beverage
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel

Abstract

This invention relates to a process for producing ethanol by continuous fermentation of polysaccharide-containing raw materials. The fermentation is carried out in one or several fermentors, a stream of fermentation liquor being separated into a yeast concentrate stream and a yeast-free stream, and possibly one sludge stream, of which the yeast concentrate stream is recirculated to the fermentor, at least part of the yeast-free stream being fed to a simple evaporator unit, corresponding to one or a few distilling stages, wherein it is separated, partly into a first vapor stream, enriched in ethanol, which is fed to a plant for production of the desired ethanol grade, and partly into a first liquid bottom stream, which is at least in part recirculated to the fermentor. Especially characterizing for the new process is, that a raw material stream is fed to a circulation circuit, comprising said fermentor and said evaporator unit, and that the raw material stream is hydrolyzed, in the evaporator unit, to a fermentable state. It is especially advantageous to carry out this hydrolysis by enzymes, preferably by a gluco-amylase at a temperature within the range 35° C. to 75° C.

Claims

1. A process for making ethanol which comprises adding a fermentable feed substance to a fermentor, fermenting said feed substance, continuously withdrawing fermentation liquor from said fermentor, continuously dividing said withdrawn fermentation liquor into a yeast-concentrate stream and a yeast-free stream, continuously recirculating said yeast-concentrate steam to the fermentor, continously passing the yeast-free stream to the separator, feeding to said separator polysaccharides and at least one hydrolytic enzyme, separating the yeast-free stream into a first ethanol enriched vapor phase and a first liquid bottoms stream, feeding said first ethanol enriched vapor phase to an ethanol recovery plant, conducting the separation of the ethanol enriched vapor phase from the yeast-free stream in the separator under a temperature higher than the fermentation temperature and under conditions suitable for enzymatic hydrolysis, whereby, during the separation of said yeast-free stream, the polysaccharides are hydrolysed by the action of at least one hydrolytic enzyme to fermentable saccharides, and recirculating part of said first bottoms stream containing said fermentable saccharides to the fermentor.

2. The process of claim 1 wherein part of said yeast-free stream is fed to a stripping unit where it is separated into a second vapor phase enriched in ethanol and into a third liquid bottom stream exhausted of ethanol.

3. The process of claim 1, in which said fermentation liquor is separated in a centrifugal separator.

4. The process claimed in claim 1, in which the part of the first liquid bottoms stream recirculated to the fermentor is sieved to remove undigested particles.

5. The process claimed in claim 1 wherein the fermentation liquor drawn from the fermentor is sieved to remove particles.

6. The process of claim 5, in which in that the stream containing particles separated by a sieve means is fed to a stripping unit.

7. The process claimed in claim 1 comprising separating the withdrawn fermentation liquor into a yeast concentrate stream, a yeast-free stream and a sludge stream of impurities.

8. The process of claim 7, in which at least part of said sludge stream is fed to a stripping unit.

9. The process claimed in claim 1 wherein the ethanol recovery plant contains a fractionating unit generating a second bottoms stream and transferring heat from said second bottoms stream to the polysaccharide containing feed stream.

10. The process claimed in claim 1 in which the polysaccharide is first liquified to a prehydrolysate before adding the polysaccharide to the yeast-free stream and said prehydrolysate is further hydrolysed to a fermentable state by enzymes during ethanol separation of said yeast-free stream.

11. The process claimed in claim 10 wherein the enzymes which further hydrolyse the prehydrolysate are fed to the fermentor or the separator.

12. The process of claim 10 in which the further hydrolysis in the separator is carried out at a temperature within the range 35°

C.-75°

C.

13. The process of claim 10, in which the further hydrolysis is carried out by means of a glucoamylase.

14. The process of claim 10, in which the further hydrolysis is carried out by means of a cellulase.

15. The process of claim 10, in which the further hydrolysis is carried out simultaneously with enzymes breaking down starch and enzymes breaking down cellulose.