Apparatus for near infrared quantitative analysis with temperature variation correction

• US 4,404,642 A
• Filed: 05/15/1981
• Issued: 09/13/1983
• Est. Priority Date: 05/15/1981
• Status: Expired due to Term

• Current Assignee: Trebor Industries Incorporated (Brownie's Marine Group Incorporated)
• Original Assignee: Trebor Industries Incorporated (Brownie's Marine Group Incorporated)
• Inventors: Rosenthal, Robert D.
• Primary Examiner(s): Chin, Gary
• Application Number:
  US06/263,881
• Time in Patent Office: 851 Days
• Field of Search: 364/496-499, 364/526, 364/557, 364/571, 250/338, 250/341, 250/343, 250/345, 356/416, 356/418
• US Class Current: 702/85
• CPC Class Codes: G01N 21/3563 for analysing solids; Preparation of samples therefor
• CPC Class Codes: G01N 21/359 using near infrared light
• CPC Class Codes: G01N 21/85 Investigating moving fluids or granular solids
• CPC Class Codes: G01N 33/10 Starch-containing substances, e.g. dough
• CPC Class Codes: Y10S 250/91 Food sample analysis using invisible radiant energy source

Abstract

A near infrared quantitative analysis instrument provides for correction of wide temperature variations in unground cereal grain sample by providing a thermistor to measure the temperature of the sample and utilizing this measurement as an additional variable in multiple regression equations.

Claims

1. An apparatus for near infrared quantitative analysis providing for correcting wide temperature variations of a sample, the apparatus comprising:

(a) means for holding a sample to be analyzed including at least a portion of a wall thereof being transparent to infrared energy,

(b) a plurality of infrared emitting diodes positioned to transmit infrared energy toward the sample in the holding means,

(c) means for sequentially pulsing the infrared emitting diodes,

(d) a plurality of narrow bandpass filters between the infrared emitting diodes and the sample holding means to produce desired wavelengths required for quantitative analysis,

(e) sensor means positioned to receive and sense infrared energy transmitted through the sample to be analyzed contained in the holding means, said sensor means producing a signal related to the infrared energy received thereby,

(f) temperature measuring means positioned in the sample holding means to measure the temperature of the sample therein and to produce a signal related thereto,

(g) computer means for receiving the signals from the sensor means and the temperature measuring means and combining them in a multiple regression equation to compensate for variations in sample temperature, and

(h) means for reading out the results of the analysis from the computer means.

2. An apparatus as in claim 1 further comprising:

switch means in a circuit between the output of the sensor means and temperature measuring means and before the computer means for providing a signal to the computer from the temperature measuring means and sensing means at least once each cycle of the pulsed infrared emitting diodes.

3. An apparatus as in claim 2 wherein the temperature measuring means is a thermister.

4. An apparatus as defined in claim 3 further comprising a timer for controlling the switch and the pulsing of the infrared emitting diodes to provide data produced from said sensor means and said thermistor in a cycle.

5. An apparatus as defined in claim 4 wherein the reading out means includes a digital display operated by the computer in response to the result of solving the multiple regression equation.

6. An apparatus as defined in claim 5 wherein the sample is an unground cereal grain.