Liquid cell for spectroscopic analysis

• US 4,405,235 A
• Filed: 03/19/1981
• Issued: 09/20/1983
• Est. Priority Date: 03/19/1981
• Status: Expired due to Term

• Current Assignee: Val J. Rossiter
• Original Assignee: Val J. Rossiter
• Inventors: Rossiter, Val J.
• Primary Examiner(s): McGraw, Vincent P.
• Application Number:
  US06/245,427
• Time in Patent Office: 915 Days
• Field of Search: 356/246, 356/440, 356/410
• US Class Current: 356/246
• CPC Class Codes: G01N 2021/0346 Capillary cells; Microcells
• CPC Class Codes: G01N 21/05 Flow-through cuvettes G01N21/09 takes precedence; handling fluid samples G01N1/10
• CPC Class Codes: G01N 30/74 Optical detectors measurement of intensity, velocity, spectral content, polarisation, or phase of infrared, visible or ultraviolet light G01J

Abstract

A liquid cell for use in spectroscopic analysis of flowing liquids formed by a front plate (1) as an optical window, a back plate (2) providing a reflecting surface (6), and a sealing means (3) between the two plates. In the back plate there are entry part (4) and exit part (5) for liquids to the cell. This arrangement is convenient to connect for liquid through-put, and gives extra sensitivity and allows detection of very small quantities of material present in the flow.

Claims

1. A liquid cell for use in spectroscopic analysis of flowing liquids formed by a front plate as an optical window, a back plate having spaced apart apertures therein, a tapered reflecting surface on the back plate between the apertures, and a sealing means between said two plates, each of said apertures being an entry and an exit port, respectively, for liquids to the cell.

2. A liquid cell according to claim 1 wherein said entry and exit ports are formed as a circular hole on the outside of said back plate which opens to a triangular taper on the inside of said back plate.

3. A liquid cell according to claim 1 wherein the dimensions of said cell are about 15 mm in length, a breath of about 6 mm and a thickness of about 0.15 mm.

4. A liquid cell according to claim 1 wherein the back plate is metal.

5. A liquid cell according to claim 1 wherein said reflecting surface has a coating to increase reflectivity.

6. A liquid cell according to claim 1 wherein the reflecting surface is non-parallel with the window whereby the path length between them varies along the cell.

7. A liquid cell according to claim 6 wherein the degree of variation of path length corresponds to the difference in wave length of the upper and lower wave lengths of the radiation used.

8. A liquid cell according to claim 1 wherein said sealing means being polytetrafluoroethylene.

9. A liquid cell for use in spectroscopic analysis of flowing liquids formed by a front plate as an optical window, a back plate having an inlet port and an outlet port, a tapered reflecting surface between said ports, and a sealing means between said two plates, said plates being removably attached to said sealing means by clamping means.

10. A liquid cell according to claim 9 wherein said cell being adapted to contain a volume of liquid in the microliter range.