Liquid purification using reverse osmosis hollow fibers

• US 4,414,113 A
• Filed: 09/29/1982
• Issued: 11/08/1983
• Est. Priority Date: 09/29/1982
• Status: Expired due to Fees

• Current Assignee: Ecodyne Corp. (Berkshire Hathaway Incorporated)
• Original Assignee: Ecodyne Corp. (Berkshire Hathaway Incorporated)
• Inventors: LaTerra, Terrance
• Primary Examiner(s): Sadowski, David R.
• Application Number:
  US06/427,863
• Time in Patent Office: 405 Days
• Field of Search: 210/636, 210/639, 210/652-655, 210/777, 210/778, 210/321, 210/323.2, 210/333.01, 210/340, 210/341, 210/411, 210/433.2, 210/456, 210/497.1, 210/500.2
• US Class Current: 210/636
• CPC Class Codes: B01D 2313/125 Discharge manifolds
• CPC Class Codes: B01D 2321/04 Backflushing
• CPC Class Codes: B01D 2321/168 Use of other chemical agents
• CPC Class Codes: B01D 2321/185 Aeration
• CPC Class Codes: B01D 61/025 Reverse osmosis; Hyperfiltration
• CPC Class Codes: B01D 63/024 with a single potted end
• CPC Class Codes: B01D 63/025 Bobbin units
• CPC Class Codes: B01D 63/043 with separate tube sheets
• CPC Class Codes: B01D 65/02 Membrane cleaning or sterilisation ; Membrane regeneration

Abstract

A method and apparatus for removing dissolved solids from a liquid which utilizes the technique of reverse osmosis (RO). The liquid to be treated is directed into a pressure vessel which contains a plurality of filter elements positioned therein. The filter elements have hollow RO fibers wound around foraminous center cores such that the liquid flows in a direction from the outside of the filter elements towards the center cores. The pure permeate liquid passes into the center bores of the fibers and the concentrate liquid passes into the center cores of the elements.

The method and apparatus provide for the backwashing of the filter elements when they become fouled. Further, an outer filter septum may be applied around the hollow RO fibers of the elements to remove particulate matter which would otherwise foul the hollow RO fibers.

Claims

1. A method for removing dissolved solids and suspended particuate matter from a liquid to be treated, comprising the steps of:

(a) passing a feedstream of liquid to be treated into a pressure vessel having a plurality of filter elements vertically positioned therein;

(b) directing the liquid to be treated through an outer filter septum positioned around the filter elements for removal of suspended particulate matter in the liquid to be treated;

(c) directing the liquid to be treated that passes through the filter septum through a layer of hollow RO fibers spirally wrapped around formaninous center cores of the filter elements such that the liquid to be treated flows in a direction from the outside of the filter elements towards the foraminous center cores, so as to cause substantially pure permeate liquid to permeate into the center bores of the hollow RO fibers and concentrate liquid to pass into the foraminous center cores;

(d) collecting the permeate liquid from the center bores of the hollow RO fibers in a common collector manifold and removing the collected permeate liquid from the pressure vessel;

(e) collecting at least a portion of the concentrate liquid from the center cores in a common concentrate liquid collection compartment and removing the collected concentrate liquid from the pressure vessel;

(f) periodically terminating passage of the liquid to be treated into the pressure vessel and directing backwash liquid into the concentrate liquid collection compartment and then across the layer of hollow RO fibers and the filter septum into the pressure vessel, so as to remove particular matter that is trapped in the hollow RO fibers and the filter septum and;

(g) removing the backwash liquid along with the suspended particulate matter from the pressure vessel.

2. The method as defined in claim 1 including the further step of facing the portions of the hollow RO fibers adjacent the upper ends of the filter elements so as to permit the permeate liquid to pass through such faced portions into the collector manifold.

3. The method as defined in claim 2 including the step of maintaining the remaining portions of said hollow RO fibers in an unfaced state so as to preclude the permeate liquid from exiting from the hollow RO fibers.

4. The method as defined in claim 1 wherein the filter septum is an inert fiberous material spirally wrapped around the layer of RO fibers.

5. The method as defined in claim 1 wherein the filter septum is a precoat layer of filter aid material applied around the layer of RO fibers and the backwash liquid passing across the layer of RO fibers removes the precoat filter aid material along with the suspended particulate matter trapped in the layer of hollow RO fibers.

6. An apparatus for removing dissolved solids and suspended particulate matter from a liquid to be treated, comprising:

(a) a pressure vessel having a tube sheet which divides said pressure vessel into an upper influent compartment and a lower concentrate compartment and a collector manifold which is positioned in an upper portion of said influent compartment;

(b) a plurality of vertically extending filter elements each extending between said tube sheet and said collector manifold, said filter elements each having foraminous center cores which extend through said tube sheet into and in fluid communication with said concentrate compartment;

(c) a layer of hollow RO fibers spirally wrapped around said center cores, said hollow RO fibers having center bores in fluid communication with said collector manifold;

(d) a filter septum means positioned around each of said layers of hollow RO fibers for removing suspended particulate matter from liquid passing therethrough;

(e) means for directing a feedstream of liquid to be treated under pressure into said influent compartment of said pressure vessel such that the liquid to be treated flows in a direction from the outside of the filter elements through said filter septum means for removing particulate matter and then through said layer of hollow RO fibers for causing substantially pure permeate liquid to permeate into the center bores of said hollow RO fibers and concentrate liquid to pass into said foraminous center cores;

(f) means for directing the permeate liquid in the center bores of said hollow RO fibers into said collector manifold and removing the permeate liquid in said collector manifold from said pressure vessel;

(g) means for directing the concentrate liquid in said foraminous center cores into said concentrate compartment and removing at least a portion of the concentrate liquid in said concentrate compartment from said pressure vessel; and

(h) backwash means for periodically passing backwash liquid into said concentrate compartment and up into said foraminous center cores and then outward across said layer of hollow RO fibers and said filter septum means into said influent compartment for removing particular matter that is trapped in said hollow RO fibers and the filter septum means.

7. The invention as defined in claim 6 wherein a tube sheet is provided to divide said pressure vessel into an upper influent compartment and a lower concentrate compartment, said filter elements being positioned within said influent compartment and having open lower ends which extend through said tube sheet into said concentrate compartment so as to direct concentrate liquid from said foraminous central cores into said concentrate compartment.

8. The invention as defined in claim 6 wherein a liquid feedstream line is provided to direct liquid to be treated into said influent compartment.

9. The invention as defined in claim 8 wherein a concentrate outlet line is provided to remove concentrate liquid from said concentrate compartment.

10. The invention as defined in claim 9 wherein portions of said hollow RO fibers are faced so as to permit removal of permeate liquid therefrom into said collector manifold.

11. The invention as defined in claim 10 wherein said hollow RO fibers are faced adjacent the upper ends of said filter elements.

12. The invention as defined in claim 11 wherein a permeate outlet line is provided in said pressure vessel to receive permeate liquid from said collector manifold.

13. The invention as defined in claim 6 wherein inert fiberous material is applied as a layer around said layer of hollow RO fibers.

14. The invention as defined in claim 6 wherein said filter septum means includes a layer of precoat filter aid material applied around said layer of hollow RO fibers and said backwash liquid passing across said layer of hollow RO fibers removes said layer of precoat filter aid material from said filter elements.

15. The invention as defined in claim 14 wherein a means is provided to pass a slurry of precoat filter aid material into said influent compartment to apply a layer of precoat filter aid material around said layer of hollow RO fibers.