Gas chromatographic oven using symmetrical flow of preheated - premixed ambient air

• US 4,420,679 A
• Filed: 02/26/1982
• Issued: 12/13/1983
• Est. Priority Date: 02/26/1982
• Status: Expired due to Fees

• Current Assignee: Spectra-Physics Incorporated (MKS Instruments Incorporated)
• Original Assignee: Delta Associates, Inc.
• Inventors: Howe, Robert L.
• Primary Examiner(s): Reynolds, B. A.
• Assistant Examiner(s): Walberg, Teresa J.
• Application Number:
  US06/352,656
• Time in Patent Office: 655 Days
• Field of Search: 219/400, 219/386, 219/387, 219/413, 432/178, 432/179, 34/209, 34/227, 34/219-225, 34/235, 99/473-476, 126/21 A, 126/21 R, 422/70, 422/89, 73/23.1
• US Class Current: 219/400
• CPC Class Codes: F24C 15/325 electrically-heated
• CPC Class Codes: F27B 17/0083 with means for circulating the atmosphere
• CPC Class Codes: F27D 19/00 Arrangements of controlling devices
• CPC Class Codes: F27D 2019/0018 Monitoring the temperature of the atmosphere of the kiln
• CPC Class Codes: F27D 2019/0031 through control of the flow of the exhaust gases
• CPC Class Codes: F27D 2019/0084 Controlling closure systems, e.g. doors
• CPC Class Codes: G01N 2030/3084 ovens
• CPC Class Codes: G01N 30/30 of temperature

Abstract

A temperature controlled oven apparatus having a central chamber with a heater element and a pivotal inner baffle door, located within a removable outer access door, periodically opened or closed to regulate the exhaust of oven air and the admission of ambient air into the oven through a preheated plenum chamber.

Claims

1. Apparatus for operating a gas chromatographic oven at near ambient temperature with minimal temperature gradients, comprising in combination:

a housing means with an outer access door and a central chamber consisting of an anterior chamber for providing a heated environment for chromatographic test apparatus and a posterior chamber for minimizing thermal gradients by providing a homogeneous oven temperature about said test apparatus;

insulation means located within the walls of the housing means for providing a thermal boundary between said central chamber and the ambient environment;

plenum chamber means positioned between said central chamber and the housing means for preheating intake air prior to introduction of said air into said central chamber to eliminate temperature differentials in said central chamber;

adjustable inner baffle means positioned between the housing means and said outer access door for regulating the flow of said intake air to the plenum chamber and exhaust air from said anterior chamber;

partition means connected to the inner baffle means for isolating said intake air to the plenum chamber from exhaust air of said anterior chamber;

actuator means located outside the housing means and in mechanical communication with the inner baffle means for positioning the inner baffle means;

air distribution means positioned within said posterior chamber for premixing said intake air with existing central chamber air and distributing said premixed air to said anterior chamber;

heater means positioned within said posterior chamber for heating said premixed air to a program temperature to minimize oven thermal gradients;

sensor means positioned within said posterior chamber of the housing means for sensing the temperature within said central chamber; and

an automatic control means connected to said actuator means and said heater means for receiving temperature data from said sensor means and for transmitting control signals to said heater and actuator means in response to temperature.

2. The apparatus of claim 1 further including a spring pivot means for connecting the inner baffle means to said outer access door, whereby the inner baffle means may be rotated about said spring pivot means by the translational motion of said actuator.

3. The apparatus of claim 1 further including a compression spring positioned between said outer access door and the inner baffle means for sealing the inner baffle means when said actuator is withdrawn.

4. The apparatus of claim 1 wherein said outer access door is removable to increase access to said test apparatus.

5. The apparatus of claim 1 wherein said automatic control means comprises a computer programmed to drive a stepper motor and energize said heater means responsive to oven sensor data supplied to said computer.

6. The apparatus of claim 1 wherein said heater means comprises a temperature controlled electric filament.

7. The apparatus of claim 1 wherein said air distribution means comprises an electrical driven fan for premixing and distributing said preheated intake air with existing central chamber air.