Series ultrafiltration with pressurized permeate

• US 4,435,289 A
• Filed: 12/23/1981
• Issued: 03/06/1984
• Est. Priority Date: 12/23/1981
• Status: Expired due to Fees

• Current Assignee: Koch Membrane Systems, Inc. (KOCH Industries Incorporated)
• Original Assignee: Romicon Incorporated
• Inventors: Breslau, Barry R.
• Primary Examiner(s): SPEAR JR, FRANK
• Application Number:
  US06/333,743
• Time in Patent Office: 804 Days
• Field of Search: 210/638, 210/433.2, 210/637, 210/333.01, 210/411
• US Class Current: 210/637
• CPC Class Codes: B01D 2313/44 Cartridge types
• CPC Class Codes: B01D 61/146 comprising multiple ultrafiltration steps
• CPC Class Codes: B01D 63/046 in separate housings

Abstract

Process and apparatus for providing separation of solutes, colloidal particles or suspended matter by ultrafiltration wherein increased cost efficiency and reduced energy requirements are realized by series flow configuration, utilizing increased operating pressures, and back pressurization of permeate.

Claims

1. A method for separating solutes, colloidal particles or suspended matter from a solution or suspension of such matter by ultrafiltration which comprises:

(a) connecting multiple ultrafiltration membrane containing separatory units in series flow configuration, thereby providing, at least, a first unit, a last unit and optionally intermediate units;

(b) introducing a solution or suspension to be separated into the first unit at a pressure exceeding the maximum allowable transmembrane pressure difference for said membrane;

(c) concurrently applying a back pressure on the permeate side of said membrane to produce a transmembrane pressure difference in said first unit not exceeding the maximum allowable transmembrane pressure difference for said membrane;

(d) repeating steps (b) and (c) in at least each intermediate unit;

(e) withdrawing permeate from each unit; and

(f) recovering concentrate containing solutes, colloidal particles or suspended matter from the last serially connected unit.

2. A method as defined by claim 1 wherein said membranes are hollow fiber membranes.

3. A method as defined by claim 2 wherein two units are connected in series.

4. A method as defined by claim 3 wherein an inlet pressure in the range of about 40 to 80 psig and a back pressure in the range of about 15 to 55 psig is applied to the initial unit in said series.

5. A method as defined by claim 3 wherein an inlet pressure of about 40 psig and a back pressure of about 15 psig is applied to the initial unit in said series.

6. A method as defined by claim 2 wherein three units are connected in series.

7. A method as defined by claim 6 wherein an inlet pressure of about 50 to 120 psig and a back pressure of about 25 to 95 psig is applied to the initial unit in said series, an inlet pressure of about 40 to 80 psig and a back pressure of about 15 to 55 psig is applied to the second unit in said series.

8. A method as defined by claim 6 wherein an inlet pressure of about 55 psig and a back pressure of about 30 psig is applied to the initial unit in said series, an inlet pressure of about 40 psig and a back pressure of about 15 psig is applied to the second unit in said series.

9. A method according to claim 1 wherein steps (b) and (c) are repeated in the last unit.

10. A method as defined by claim 1 wherein said membrane has an average porosity in the range of from about 1 to about 50 millimicrons.

11. An apparatus for conducting ultrafiltration which comprises:

(a) multiple pressure-resistant filter cartridges containing ultrafiltration membranes, said cartridges connected in series flow configuration;

(b) inlet means situate in each of said cartridges;

(c) concentrate takeoff means in each cartridge;

(d) permeate takeoff means in each cartridge;

(e) means for introducing a solution or suspension to be separated into each but the last unit at a pressure exceeding the maximum allowable transmembrane pressure difference for each membrane;

(f) means for concurrently providing back pressure on the permeate side of each but said last unit to produce a transmembrane pressure difference in each unit not exceeding the maximum allowable transmembrane pressure difference for said membrane; and

(g) means for coupling said cartridges in said series.

12. An apparatus as defined by claim 11 wherein two cartridges are connected in series.

13. An apparatus as defined by claim 11 wherein three cartridges are connected in series.

14. The apparatus as defined in claim 11 including meanes to back pressure the last cartridge in said series.