Process for the recovery of a concentrated stillage

• US 4,447,535 A
• Filed: 04/14/1983
• Issued: 05/08/1984
• Est. Priority Date: 06/26/1980
• Status: Expired due to Term

• Current Assignee: Dorr-Oliver Deutschland GmbH
• Original Assignee: Supraton F J Zucker KG
• Inventors: Osthaus, Georg, Zucker, Friedrich J.
• Primary Examiner(s): Penland, R. B.
• Application Number:
  US06/484,929
• Time in Patent Office: 390 Days
• Field of Search: 435/161, 435/162, 435/165, 435/96, 435/99, 435/813
• US Class Current: 435/162
• CPC Class Codes: C12F 3/10 from distillery slops
• CPC Class Codes: C12P 7/06 Ethanol, i.e. non-beverage
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel

Abstract

A concentrated stillage with a high solids content may be recovered in such a manner that starch or starch-containing raw materials in a suitably crushed form are coaxially introduced into the center of a homogenizer together with enzymes, which are suitable for making alcohol, while simultaneously introducing steam and are suddenly gelatinized therein mechanically and thermally at temperatures of not less than 50° C. and not more than 115° C. while ultrafinely dividing the enzyme; the starch paste after liquefaction is converted to the glucose and the resultant mash is fermented in such a manner that the stillage obtained with reduced dry matter, after removal of merely the coarse contaminations by, for example, centrifuging is repeatedly recycled without further purification and reused as process liquor.

Claims

1. A process for the recovery of a concentrated stillage in the production of alcohol from starch or starch-containing raw materials, comprising the steps of:

(a) mixing said starch or starch-containing materials in finely divided form with an aqueous process liquor;

(b) introducing the mixture from step (a) together with steam and enzymes suitable for making alcohol coaxially to the center of a rotor-stator homogenizer wherein the starch is rapidly gelatinized thermally and mechanically in a zone of high density of shear and cavitation forces at a temperature between 70°

C. and 115°

C. and the enzyme is ultrafinely distributed;

(c) enzymatically liquefying the starch in the product of step (a);

(d) saccharifying and fermenting the product of step (c);

(e) distilling the product of step (d) to produce alcohol and stillage;

(f) separating solid coarse particles from said stillage; and

(g) repeating the cycle of steps (a) through (f) using the stillage essentially as obtained from step (f) at least three times without further purification as the process liquor in step (a), until the dry solids content of the stillage has increased to about 30%.

2. A process according to claim 1 wherein the gelatinization is effected at temperatures between 85°

C. and 95°

C.