Quantitative measurement of fat, protein and lactose in dairy products

• US 4,447,725 A
• Filed: 06/15/1981
• Issued: 05/08/1984
• Est. Priority Date: 06/15/1981
• Status: Expired due to Fees

• Current Assignee: Multispec Ltd. (NWF Group PLC)
• Original Assignee: Multispec, Inc.
• Inventors: Shields, John, Biggs, Delmar A.
• Primary Examiner(s): Willis, Davis L.
• Application Number:
  US06/273,392
• Time in Patent Office: 1,058 Days
• Field of Search: 250/338, 250/339, 250/340, 250/341, 250/343
• US Class Current: 250/339.12
• CPC Class Codes: G01N 2021/3129 Determining multicomponents by multiwavelength light
• CPC Class Codes: G01N 21/31 Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry G01N21/72 takes precedence
• CPC Class Codes: G01N 21/314 with comparison of measurements at specific and non-specific wavelengths dual wavelength spectrometry G01J3/427
• CPC Class Codes: G01N 33/06 Determining fat content, e.g. by butyrometer
• CPC Class Codes: Y10S 250/91 Food sample analysis using invisible radiant energy source

Abstract

Electro-optical apparatus for measurement of fat, protein, lactose and solids in milk wherein a milk sample in a test cell is irradiated with reference and measurement beams at differing wavelengths for fat, protein and lactose, and signals are stored indicative of uncorrected concentrations. A scaling and correction circuit includes cross-correction circuitry for compensating the effects on each reading caused by the other constituents. The signals so corrected are then provided in percentage by weight or weight over volume on suitable digital displays. For enhanced accuracy of fat concentration, infrared absorption is measured at both the carbon-hydrogen stretching wavelength (3.48 microns) and the wavelength of absorption at the ester linkages (5.72 microns), and the resulting readings are combined in a predetermined function for obtaining a reading of fat concentration.

Claims

1. Apparatus for measuring fat concentration in fat emulsions such as natural and synthetic dairy products comprising means for holding a product sample, means for irradiating said sample with energy in the infrared spectrum at a first wavelength characteristic of ester linkages and a second wavelength characteristic of saturated carbon-hydrogen bonds, and means for assessing fat concentration in the sample as a predetermined conjoint function of energy absorbed by said sample at both said first and second wavelengths.

2. The apparatus set forth in claim 1 wherein said irradiating means includes means for successively irradiating said sample at said first and second wavelengths.

3. The apparatus set forth in claim 1 or 2 further comprising means for irradiating said sample with energy at a third wavelength characteristic of peptide linkages and a fourth wavelength characteristic of hydroxy groups in the sample, and means coupled to said assessing means and responsive to absorption of energy at said third and fourth wavelengths for correcting said predetermined conjoint function for absorption due to said peptide linkages and hydroxy groups at said first and second wavelengths.

4. The apparatus set forth in claim 3 further comprising means for indicating protein and lactose concentrations in said sample as a function of absorption of energy at said third and fourth wavelengths.

5. A method of measuring fat concentration in dairy products comprising the steps of irradiating a test sample with infrared energy, determining infrared absorption of said sample at a first wavelength characteristic of carbon-hydrogen bonds and a second wavelength characteristic of ester linkages, and then quantitatively assessing the fat concentration of said sample as a predetermined function of absorption at both said first and second wavelengths.

6. The method set forth in claim 5 comprising the additional steps of determining infrared absorption of said sample at a third wavelength characteristic of peptide linkages and a fourth wavelength characteristic of hydroxy groups, and assessing said fat concentration as a predetermined function of absorption at all of said first, second, third and fourth wavelengths.

7. The method set forth in claim 6 comprising the additional step of assessing solids concentration in said sample as a predetermined function of absorption at all of said wavelengths.