Oilseed extraction process

• US 4,456,556 A
• Filed: 05/07/1982
• Issued: 06/26/1984
• Est. Priority Date: 05/07/1982
• Status: Expired due to Fees

• Current Assignee: Shell Oil Company (Shell Plc)
• Original Assignee: Shell Oil Company (Shell Plc)
• Inventors: Grimsby, Frank N.
• Primary Examiner(s): Sneed, Helen M. S.
• Application Number:
  US06/376,086
• Time in Patent Office: 781 Days
• Field of Search: 260/412.4
• US Class Current: 554/13
• CPC Class Codes: C11B 1/108 after-treatment, e.g. of miscellae

Abstract

A process for the extraction of oilseeds which comprises extracting oil from oilseeds by contacting the seeds with an isopropanol-based solvent to obtain an extract miscella of seedoils in solvent and a seed meal containing absorbed liquids, cooling and phase separating the miscella to recover solvent from the extracted oil, recycling said solvent from the miscella to the extraction step, heating the seed meal in a desolventizing/toasting zone to produce a solvent vapor, contacting in a vapor/liquid contact zone the solvent vapor from the desolventizing toasting zone with a contact liquid which is a process solvent stream having a lesser content of water than the solvent vapor, withdrawing and condensing effluent vapor from the contact zone, passing at least a portion of the effluent vapor condensate to the extraction step as solvent, withdrawing effluent liquid from the contact zone and introducing said liquid into the desolventizing/toasting zone, and withdrawing a process meal product from the desolventizing/toasting zone. This process provides an energy efficient means for controlling water content in the process solvent, particularly in preventing the build-up of water in recycle streams to unacceptable levels.

Claims

1. In a process for the solvent extraction of oil from oil-containing seeds, comprising steps for (a) contacting in an extractor the oilseeds with an isopropanol-based extraction solvent to obtain an extract miscella of seedoil in solvent and a seed meal containing adsorbed solvent, (b) cooling and phase separating the miscella to recover solvent from the extracted oil, (c) recycling said solvent recovered from the miscella to the extractor, (d) heating the seed meal in a desolventizing/toasting zone to obtain a solvent vapor, (e) condensing the solvent vapor, and (f) recycling solvent vapor condensate to the extractor, the improvement which comprises additional steps for contacting in a vapor/liquid contact zone the solvent vapor evaporated from the seed meal, before condensation, with a contact liquid which is an isopropanol-based process solvent stream having a water content less than the water content of the solvent vapor, withdrawing vapor from the contact zone and introducing said vapor to the condensation zone as solvent vapor, and withdrawing liquid from the contact zone and introducing said liquid to the desolventizing/toasting zone.

2. The process of claim 1, wherein a portion of the condensed solvent vapor is introduced as contact liquid into the contact zone.

3. The process of either claim 1 or claim 2, wherein the quantity of contact liquid is between about 5 and 75 percent by weight, calculated on the quantity of solvent vapor with which it is contacted in the contact zone.

4. The process of claim 3, wherein the process includes a step for stripping a solvent vapor from the phase separated miscella oil, and the improvement additionally comprises contacting both this stripped solvent vapor and the solvent vapor evaporated from seed meal with the contact liquid in the contact zone.