Oilseed extraction process

• US 4,456,557 A
• Filed: 05/07/1982
• Issued: 06/26/1984
• Est. Priority Date: 05/07/1982
• Status: Expired due to Fees

• Current Assignee: Shell Oil Company (Shell Plc)
• Original Assignee: Shell Oil Company (Shell Plc)
• Inventors: Grimsby, Frank N.
• Primary Examiner(s): Sneed, Helen M. S.
• Application Number:
  US06/376,087
• Time in Patent Office: 781 Days
• Field of Search: 260/412.4
• US Class Current: 554/13
• CPC Class Codes: C11B 1/102 in counter-current; utilisation of an equipment wherein the material is conveyed by a screw

Abstract

A process for the extraction of oilseeds which comprises steps for extracting oil from oilseeds by contacting the seeds in a presoaking zone with an isopropanol-based presoak solvent to obtain presoaked seeds, extracting the presoaked seeds by contact with an isopropanol-based extraction solvent in a multi-stage countercurrent extraction zone to obtain an extraction miscella and an extracted seed meal, and recovering oil from the extraction miscella. Processing efficiency is enhanced by the presoaking contact step when the relative water content of the presoak solvent is less than that of the extraction miscella.

Claims

1. A process for the separation of oils from seeds containing extractible oils, which comprises steps for contacting the seeds in a presoaking zone with an isopropanol-based presoak solvent to obtain presoaked seeds, extracting the presoaked seeds by contact with an isopropanol-based extraction solvent containing between about 10 and 20 percent by weight water in a multi-stage countercurrent extraction zone to obtain an extraction miscella and an extracted seed meal, and recovering oils from the extraction miscella, under the provision that the weight ratio of water to isopropanol in the presoak solvent is less than the weight ratio of water to isopropanol in the extraction miscella.

2. The process of claim 1, wherein the presoak solvent contains less than about 16 percent by weight of water, calculated on the total weight of isopropanol and water in the presoak solvent.

3. The process of claim 2, wherein the presoak solvent contains less than about 12 percent by weight water, calculated on total weight of presoak solvent.

4. The process of claim 3, wherein the presoak solvent contains less than about 10 percent by weight water, calculated on total weight of presoak solvent.

5. The process of claim 4, wherein the presoak solvent contains less than about 7 percent by weight water, calculated on the total weight of presoak solvent.

6. A process for the separation of oils from seeds containing extractible oils, which comprises steps for contacting the seeds in a presoaking zone with an isopropanol-based presoak solvent to obtain presoaked seeds, extracting the presoaked seeds by contact with an isopropanol-based extraction solvent containing between about 10 and 20 percent by weight water in a multi-stage countercurrent extraction zone to obtain an extraction miscella and an extracted seed meal, cooling and phase separating the extraction miscella to obtain a solvent-rich stream and an oil-rich stream, evaporating residual solvent from the oil-rich stream, and recycling the evaporated solvent to the presoak zone as presoak solvent.