Spectrophotometer

• US 4,464,051 A
• Filed: 03/02/1982
• Issued: 08/07/1984
• Est. Priority Date: 03/02/1982
• Status: Expired due to Term

• Current Assignee: Perkinelmer Instruments LLC (Revvity, Inc.)
• Original Assignee: Perkinelmer Incorporated
• Inventors: Talmadge, Paul C., Vergato, Joseph A.
• Primary Examiner(s): Evans, F. L.
• Application Number:
  US06/354,254
• Time in Patent Office: 889 Days
• Field of Search: 356/319, 356/323-325, 356/332-334
• US Class Current: 356/323
• CPC Class Codes: G01J 3/06 Scanning arrangements arrangements for order-selection
• CPC Class Codes: G01J 3/08 Beam switching arrangements
• CPC Class Codes: G01J 3/42 Absorption spectrometry; Double beam spectrometry; Flicker spectrometry; Reflection spectrometry beam switching arrangements G01J3/08

Abstract

Disclosed herein is a spectrophotometer which includes a source of radiation; an optical system for forming a beam of radiation from the source and directing it along a sample path and along a reference path, which paths come together at a location to form a combined path that impinges on a detector; a chopper mounted at said location for successively directing one or the other of the beams along the combined path or providing a blank chopper area for blocking radiation from the combined path; a monochromator having a grating and slits disposed in the combined path, the angular position of the grating being adjustable for passing selected successive wavelengths of radiant energy through the optical system; and controls are provided for controlling the movement of the grating and/or slits so that movement only occurs when the blank chopper area is blocking the combined path.

Claims

1. A spectrophotometer comprising, in combination:

a source of radiation;

an optical system for forming a beam of radiation from said source and directing it along a sample path and along a reference path, which paths come together at a location to form a combined path that impinges on a detector;

chopper means mounted at said location for successively directing one or the other of said beams along said combined path or providing a blank chopper area for blocking radiation from said combined path, said chopper means including a chopper motor controller and a chopper motor

monochromator means having grating means mounted in said combined path, means for adjusting the angular position of said grating means for passing selected successive wavelengths of radiant energy through said optical system;

control means for controlling the movement of said means for moving the grating so that movement only occurs when said blank chopper area is blocking said combined path, said control means including a microprocessor and memory, and

a master timer for inputting timing signals to said chopper motor controller and to said microprocessor, said chopper motor controller being arranged to input into said microprocessor a plurality of pulses per cycle, one corresponding to each position of the chopper, said chopper motor being arranged to input into said microprocessor one sync pulse per cycle.

2. A spectrophotometer according to claim 1 wherein said chopper means has a cycle that successively in the order of occurrence consists of six positions, a blank, a reference, a sample, a blank, a sample, a reference and the cycle is repeated with another blank.

3. A spectrophotometer according to claim 1 wherein said plurality of pulses is six pulses per cycle.

4. A spectrophotomer according to claim 1 or claim 3 wherein said microprocessor is operative to adjust for the phase difference in the pulses received with respect to the actual position of said chopper means.

5. A spectrophotomer according to claim 1 further including monochromator adjustable slit means, means for adjusting said slit means, and wherein said control means for controlling the movement of said means for moving the grating also controls said means for adjusting said slit means so that movement only occurs when said blank chopper area is blocking said combined path.