Method and apparatus for preparing emulsions

• US 4,495,086 A
• Filed: 07/14/1982
• Issued: 01/22/1985
• Est. Priority Date: 08/19/1981
• Status: Expired due to Fees

• Current Assignee: Ransburg Japan Limited
• Original Assignee: Ransburg Japan Limited
• Inventors: Hiroshima, Koichi, Tada, Yoshinori
• Primary Examiner(s): Lovering, Richard D.
• Application Number:
  US06/398,441
• Time in Patent Office: 923 Days
• Field of Search: 252/314, 252/359 A, 252/359 B, 366/165, 366/167, 118/626, 427/30
• US Class Current: 516/20
• CPC Class Codes: B01F 23/41 Emulsifying
• CPC Class Codes: B01F 23/43 using driven stirrers
• CPC Class Codes: B01F 25/74 with rotating parts, e.g. discs
• CPC Class Codes: B01F 25/742 for spraying a liquid on falling particles or on a liquid curtain B01F25/7411 takes precedence
• CPC Class Codes: B01F 27/00 Mixers with rotary stirring devices in fixed receptacles magnetic mixers B01F33/45; Kneaders
• CPC Class Codes: B05B 5/001 incorporating means for heating or cooling, e.g. the material to be sprayed
• CPC Class Codes: B05B 5/04 characterised by having rotary outlet or deflecting elements , i.e. spraying being also effected by centrifugal forces
• CPC Class Codes: B05B 5/0407 with a spraying edge, e.g. like a cup or a bell
• CPC Class Codes: B05B 5/0426 Means for supplying shaping gas
• CPC Class Codes: B05B 5/16 Arrangements for supplying liquids or other fluent material
• CPC Class Codes: B29B 7/16 with paddles or arms
• CPC Class Codes: B29B 7/286 measuring properties of the mixture, e.g. temperature, density B29B7/283 takes precedence
• CPC Class Codes: Y10S 516/929 Specified combination of agitation steps, e.g. mixing to make subcombination composition followed by homogenization

Abstract

Method and apparatus for continuously producing emulsions with particles of a disperse phase liquid in a continuous phase liquid, employing an emulsifying vessel which is interiorly provided with a gravitative flow surface and a feeder for supplying the continuous phase liquid to the flow surface for forming thereon a stream of the continuous phase liquid. On the other hand, disposed within the emulsifying vessel is a rotary atomizing head which is connected to a disperse phase liquid source and a rotational drive means and maintained at a high voltage to stratify and form a spray of atomized particles of the disperse phase liquid flying toward the flow surface under the influence of centrifugal force and electrostatic action. The disperse phase particles from the rotary atomizing head are entrained and dispersed in the stream of the continuous phase liquid on the flow surface of the emulsifying vessel to form an emulsion. The resulting emulsion is collected in a receptacle. In some cases, the emulsifier is provided with a hot steam feed pipe for feeding hot steam to the rotary atomizing head to prevent solidification of atomized disperse phase particles on the atomizing head.

Claims

1. An apparatus for producing emulsions by spraying particles of a disperse phase liquid into a continuous phase liquid, said apparatus comprising in combination:

(a) an emulsifying vessel interiorly providing a gravitiative flow surface for forming thereon a stream of said continuous phase liquid;

(b) a continuous phase liquid feeder for directing said continuous phase liquid to said gravitative flow surface of said emulsifying vessel;

(c) a rotary atomizing head disposed in said emulsifying vessel in communication with a disperse phase liquid supply;

(d) a rotational drive means for rotatably driving said rotary atomizing head within said emulsifying vessel;

(e) a high voltage power supply connected to said rotary atomizing head to apply thereto a high voltage to atomize said disperse phase liquid in cooperation with said rotational drive means and to direct electrostatically charged particles of said disperse phase liquid toward said gravitative flow surface of said emulsifying vessel along lines of electric force formed between said rotary atomizing head and said emulsifying vessel, thereby continuously dispersing the atomized particles of said disperse phase liquid in said stream of said continuous phase liquid; and

(f) a receptacle located beneath said gravitative flow surface of said emulsifying vessel for collecting the resulting dispersion.

2. An emulsifying apparatus as defined in claim 1, further comprising a hot steam feed pipe led into said emulsifying vessel and opened toward said rotary atomizing head.

3. An emulsifying apparatus as defined in claim 2, wherein said rotational drive means includes a heated air feeder adapted to direct heated air towards said rotary atomizing head.

4. An emulsifying apparatus as defined in claim 1, wherein said rotational drive means includes a heated air feeder adapted to direct heated air toward said rotary atomizing head.

5. An emulsifying apparatus as defined in claim 1, wherein said emulsifying vessel is provided with a conical gravitative flow surface.

6. An emulsifying apparatus as defined in claim 1, wherein said emulsifying vessel is provided with a gravitative flow surface of a truncated cone shape.

7. An emulsifying apparatus as defined in claim 1, wherein said emulsifying vessel is provided with a gravitative flow surface of a cup-like shape.

8. An emulsifying apparatus as defined in claims 5, 6 or 7, wherein said rotary atomizing head is supported on a lift mechanism vertically movably along with said rotational drive means.

9. An emulsifying apparatus as defined in claim 1, wherein said rotary atomizing head is provided with a bell-shaped surface for forming a filmy stream of said disperse phase liquid.

10. An emulsifying apparatus as defined in claim 1, wherein said rotary atomizing head is provided with a disc-like surface for forming a filmy stream of said disperse phase liquid.

11. An emulsifying apparatus as defined in claims 9 or 10, wherein said film-forming surface for said disperse phase liquid is provided with a multitude of grooves at a predetermined pitch along the lower marginal edge thereof.

12. An emulsifying apparatus as defined in claim 1, wherein said continuous phase liquid feeder is constituted by an annular tube.

13. An emulsifying apparatus as defined in claim 12, wherein said annular tube is provided with a multitude of small spout holes opening toward said gravitative flow surface of said emulsifying vessel.

14. An emulsifying apparatus as defined in claim 12, wherein said annular tube is provided with slits opening toward said gravitative flow surface of said emulsifying vessel.

15. An emulsifying apparatus as defined in claim 12, wherein said annular tube is provided with a plural number of nozzle units each having a nozzle hole for spouting said continuous phase liquid and a baffle plate located in front of said nozzle hole.

16. An emulsifying apparatus as defined in claim 1, wherein the output voltage of said high voltage power supply is variable.

17. An emulsifying apparatus as defined in claim 1, wherein said rotational drive means is a variable speed motor.

18. An emulsifying apparatus as defined in claim 1, wherein said emulsifying vessel is split into a lower emulsifying vessel and an upper emulsifying vessel rotatable relative to said lower emulsifying vessel.

19. A method for producing an emulsion by spraying particles of a disperse phase liquid into a continuous phase liquid, said method comprising the steps of:

(a) feeding said continuous phase liquid to a gravitative flow surface on the inner periphery of an emulsifying vessel and allowing said continuous phase liquid to flow therealong due to the force of gravity in the form of a thin filmy stream;

(b) feeding said disperse phase liquid to a rotary atomizing head;

(c) rotating said rotary atomizing head in said emulsifying vessel while applying a predetermined high voltage to said rotary atomizing head to thereby atomize said disperse phase liquid to form a spray of disperse phase particles of a desired size; and

(d) directing said spray of disperse phase particles to impact on said filmy stream of said continuous phase liquid on the gravitative flow surface on the inner periphery of said emulsifying vessel to thereby disperse said disperse phase particles in said continuous phase liquid.

20. A method for producing an emulsion by spraying particles of a disperse phase liquid into a continuous phase liquid, said method comprising the steps of:

(a) feeding said continuous phase liquid to a gravitative flow surface on the inner periphery of an emulsifying vessel and allowing said continuous phase liquid to flow therealong due to the force of gravity int he form of a thin filmy stream;

(b) feeding said disperse phase liquid to a rotary atomizing head;

(c) rotating said rotary atomizing head in said emulsifying vessel while applying a predetermined high voltage and feeding hot steam in said rotary atomizing head to thereby atomize said disperse phase liquid to form a spray of atomized disperse phase particles; and

(d) directing said spray of disperse phase particles to impact on said filmy stream of said continuous phase liquid on the gravitative flow surface on the inner periphery of said emulsifying vessel to thereby disperse said dispersed phase particles in said continuous phase liquid.