Modified amine curing agents and epoxy resins cured therewith
First Claim
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1. A composition for use in the curing of a 1,2-epoxy resin comprising an alkylene carbonate solution of a normally solid cured elastomeric polyurethane in admixture with a primary amine curing agent.
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Abstract
In accordance with the present invention an epoxy resin is cured with an amine curative comprising an alkylene carbonate solution of a solid elastomeric polyurethane in admixture with an amine-type curing agent.
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Citations
22 Claims
- 1. A composition for use in the curing of a 1,2-epoxy resin comprising an alkylene carbonate solution of a normally solid cured elastomeric polyurethane in admixture with a primary amine curing agent.
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6. A method for the preparation of a composition useful in the curing of a 1,2-epoxy resin which comprises the steps of:
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a. heating an alkylene carbonate to a temperature of 100 to about 200 degrees C. and dissolving therein a soluble amount of a cured solid elastomeric polyurethane, and b. adding the resultant solution to a primary amine curing agent. - View Dependent Claims (7, 8, 9, 10)
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- 11. A method for curing a 1,2-epoxy resin which comprises intimately mixing said epoxy resin with an effective amount of a primary amine curing agent comprising an alkylene carbonate solution of a normally cured solid polyurethane elastomer and a primary amine curing agent, whereby reaction of amino hydrogens of said amine with epoxy groups in said epoxy resin composition will result in the curing of said epoxy resin.
- 16. An epoxide resin composition prepared by curing a 1,2-epoxy resin with an epoxy curative comprising a primary amine curing agent admixed with an alkylene carbonate solution of a cured solid elastomeric polyurethane.
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21. A method for preparing an epoxide resin composition which comprises the steps of:
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(a) heating an alkylene carbonate to a temperature of about 100°
to 200°
C.,(b) dissolving a primary amine curing agent and a soluble amount of a cured solid elastomeric polyurethane in said thus-heated alkylene carbonate, (c) to thereby provide an epoxy resin curing composition comprising a solution of said solid elastomeric polyurethane and said amine curing agent in said alkylene carbonate, and (d) mixing a 1,2-epoxy resin with an effective amount of said epoxy resin curing composition whereby reaction of amino hydrogens in said amine with epoxy groups in said epoxy resins will result in the curing of said epoxy resin.
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22. An epoxide resin composition formed by curing a 1,2-epoxy resin with an epoxy resin curing composition comprising an alkylene carbonate having a primary amine curing agent and a cured solid elastomeric polyurethane dissolved therein, said epoxy resin curing composition having been prepared by heating said alkylene carbonate at a temperature of about 100°
- to about 200°
C. and dissolving said amine curing agent and a soluble amount of said solid elastomeric polyurethane therein.
- to about 200°
Specification