Solvent dumping apparatus

• US 4,517,824 A
• Filed: 07/01/1983
• Issued: 05/21/1985
• Est. Priority Date: 07/01/1983
• Status: Expired due to Term

• Current Assignee: Agilent Technologies, Inc.
• Original Assignee: Hewlett-Packard Company (HP Inc.)
• Inventors: Quimby, Bruce D.
• Primary Examiner(s): NOT, DEFINED
• Application Number:
  US06/510,127
• Time in Patent Office: 690 Days
• Field of Search: 73/23, 73/23.1, 422/89, 422/91, 55/197, 55/386, 137/239, 137/597
• US Class Current: 73/23.42
• CPC Class Codes: G01N 2030/383 by using auxiliary fluid
• CPC Class Codes: G01N 2030/402 purging a device
• CPC Class Codes: G01N 30/62 Detectors specially adapted therefor
• CPC Class Codes: G01N 30/84 Preparation of the fraction to be distributed
• CPC Class Codes: Y10T 137/4252 Reverse fluid flow

Abstract

A solvent dumping apparatus is described having an inlet enclosure coupled to the inlet of a detector and an outlet enclosure coupled to the outlet of a detector. Venting means are provided for both enclosures, one of which is controllable; means are provided for introducing sample gas into the inlet enclosure; and means are provided for introducing gas into the outlet enclosure. During a detection mode, at least one of the venting means is so adjusted as to cause sample gas to flow through the detector and out the venting means for the outlet enclosure, and during a diversionary mode, at least one of the venting means is so adjusted as to cause the gas introduced into the outlet enclosure to pass back through the detector and carry any sample gas out through the venting means for the inlet enclosure. In preferred forms of the invention, one of the venting means is a back pressure regulator.

Claims

1. Solvent dumping apparatus for a gas chromatographic detector, comprising

an inlet enclosure having an outlet port for coupling to the inlet of a detector, said inlet enclosure having venting means and means for permitting sample gas, when present, to be introduced therein,

an outlet enclosure having an inlet port for coupling to the outlet of a detector, said outlet enclosure having venting means and means for permitting gas, when available, to be introduced therein, and wherein

at least one of said venting means is controllable.

2. Solvent dumping apparatus as set forth in claim 1 wherein said controllable venting means is a back pressure regulator and one is a valve.

3. Solvent dumping apparatus as set forth in claim 1 wherein means are provided for permitting make-up gas, when available, to be introduced into said inlet enclosure at a point that is more remote from its outlet port than the point at which sample gas, when present, is introduced therein.

4. Solvent dumping apparatus as set forth in claim 1 wherein a detector is provided having an inlet coupled to said outlet port of said inlet enclosure and an outlet coupled to said inlet port of said outlet enclosure.

5. Solvent dumping apparatus as set forth in claim 3 wherein said venting means for said inlet enclosure and the means for permitting make-up gas to be introduced into said inlet enclosure are valve means, and wherein said venting means for said outlet enclosure and the means for permitting gas to be introduced therein are valve means.

6. Solvent dumping apparatus as set forth in claim 1 wherein said venting means for said inlet enclosure is a multi-position valve having a common port coupled by a first tube to said inlet enclosure, a port that communicates with said common port when said valve is in one position coupled to vent and a port that communicates with said common port when the valve is in said another position coupled to a restricted vent, and wherein the means for permitting make-up gas to be introduced into said inlet enclosure is a second tube coupled to said first tube.

7. Solvent dumping apparatus as set forth in claim 1 wherein said venting means for said inlet enclosure is a multi-position valve having a common port that communicates with said inlet enclosure, a port that communicates with said common port when said valve is in one position coupled to a restricted vent, and a port that communicates with said common port when said valve is in another position coupled to said vent,

wherein the means for permitting sample gas to be introduced into said inlet enclosure is a tube passing through said inlet enclosure to the outlet port thereof, and

wherein said means for permitting make-up gas to be introduced into said inlet enclosure is a tube passing through said inlet enclosure to a point that is more remote from said outlet port of said inlet enclosure than the end of the tube for introducing sample gas therein.

8. Solvent dumping apparatus as set forth in claim 1 wherein

said venting means for said inlet enclosure is a back pressure regulator coupled thereto,

said means for permitting sample gas to be introduced into said inlet enclosure is a tube passing through said inlet enclosure to said outlet port thereof, and

said means for permitting make-up gas to be introduced into said inlet enclosure is a tube passing through said inlet enclosure to a point that is more remote from said outlet port of said inlet enclosure than the end of said tube for introducing sample gas therein.

9. Solvent dumping apparatus as set forth in claim 1 wherein

said venting means for said inlet enclosure is a back pressure regulator,

said means for permitting sample gas to be introduced into said inlet enclosure is a first tube passing through said inlet enclosure to said outlet port thereof, and

said means for permitting make-up gas to be introduced into said inlet enclosure is a second tube coaxial with said first tube and passing through said inlet enclosure to a point that is more remote from said outlet port of said inlet enclosure than the end of said first tube.

10. Solvent dumping apparatus as set forth in claim 1 wherein

said venting means for said inlet enclosure is a multi-position valve having a common port communicating with said inlet enclosure, a port that communicates with said common port when said valve is in one position coupled to a restricted vent, and a port that communicates with said common port when said valve is in another position coupled to said vent,

said means for permitting sample gas to be introduced into said inlet enclosure is a first tube passing through said enclosure to the outlet port thereof,

said means for permitting make-up gas to be introduced into said inlet enclosure is a second tube coaxial with the first tube and passing through said inlet enclosure to a point that is more remote from said outlet port of said inlet enclosure than the end of said first tube, and

said venting means for said outlet enclosure is a back pressure regulator.

11. Solvent dumping apparatus as set forth in claim 1 wherein

said venting means for said inlet enclosure is a multi-position valve having a common port communicating with said inlet enclosure, a port that communicates with said common port when said valve is in one position coupled to a restricted vent, and a port that communicates with said common port when said valve is in another position coupled to said vent,

said means for permitting sample gas to be introduced into said inlet enclosure is a first tube passing through said enclosure to the outlet port thereof,

said means for permitting make-up gas to be introduced into said inlet enclosure is a second tube passing through said inlet enclosure to a point more remote from said outlet port thereof than the end of said first tube, and

said venting means for said outlet enclosure is a back pressure regulator.

12. Solvent dumping apparatus as set forth in any of claims 1 through 11 wherein

a transparent window is provided in said outlet enclosure, and

said venting means for said outlet enclosure and said means for permitting gas to be introduced therein are on opposite sides of said window on the way to the venting means, thereby inhibiting the deposition of matter on the inside surface of said window.