Proximate analyzer

• US 4,522,788 A
• Filed: 03/05/1982
• Issued: 06/11/1985
• Est. Priority Date: 03/05/1982
• Status: Expired due to Term

• Current Assignee: LECO Corporation
• Original Assignee: LECO Corporation
• Inventors: Walker, Sherman L., Sitek, George J.
• Primary Examiner(s): Bernstein, Hiram H.
• Application Number:
  US06/355,221
• Time in Patent Office: 1,194 Days
• Field of Search: 422/64, 422/78, 422/104, 436/157, 436/160, 177/50, 177/54, 177/55
• US Class Current: 422/78
• CPC Class Codes: G01G 19/52 Weighing apparatus combined with other objects, e.g. furniture with walking sticks A45B3/08
• CPC Class Codes: G01N 5/00 Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid G01N9/00 takes precedence ; weighing per se G01G

Abstract

The specification discloses a proximate analyzer for the analysis of fossil fuels such as coal and coke. The analyzer includes a temperature-controllable and atmosphere-controllable furnace chamber, a balance having a weigh platform positioned within the furnace chamber, and a platter positioned within the chamber and adapted to support a plurality of sample-containing crucibles. The furnace further includes means for continuously depositing the crucibles in a predetermined sequence on the weigh platform and means for monitoring the weights of the crucibles to determine when analysis is complete and for calculating the proximate analysis results based on weight loss. A method of proximate analysis using the proximate analyzer is also disclosed.

Claims

1. A fossil fuel proximate analyzer comprising:

a furnace;

a balance having a weigh platform positioned in said furnace;

support means for supporting a plurality of crucibles in a generally horizontal, circular configuration, each of the crucibles holding a sample of a material to be analyzed;

oxygen line means for selectively flooding said furnace with oxygen to facilitate oxidation of the samples during analysis, said oxygen line means including a first end to be coupled to an oxygen source, a second end communicating with said furnace, and a valve means between said first and second ends for controlling the flow of oxygen through said line means;

rotation means for rotating said support means to sequentially vertically align the crucibles with said weigh platform;

elevator means for vertically shifting said support means to deposit and remove the aligned crucible on and from said weigh platform;

control means for controlling said rotation means and said elevator means to repeatedly weigh the crucibles sequentially;

circuit means connected to said balance for monitoring the weights of the crucibles to monitor the weights of the samples, said circuit means including means for determining when the weights of the samples have reached a generally constant value indicating that a proximate analysis step is complete.

2. A proximate analyzer as defined in claim 1 wherein said support means comprises a generally planar plate.

3. A proximate analyzer as defined in claim 2 wherein said plate includes an aperture for receiving each of the crucibles.

4. A proximate analyzer as defined in claim 1 further comprising nitrogen line means for selectively flooding said furnace with nitrogen to prevent oxidation of the samples during analysis, said nitrogen line means including a first end to be coupled to a nitrogen source, a second end communicating with said furnace, and a valve means between said first and second ends for controlling the flow of nitrogen through said line means.

5. A proximate analyzer as defined in claim 1 wherein said furnace comprises a container with an upper open end and a cover, and further wherein said elevator means includes means for elevating said support means to a position proximate said upper open end to facilitate loading and unloading of the samples.

6. A proximate analysis device comprising:

a furnace chamber;

a balance having a weigh platform positioned in said furnace chamber;

sample-holding means for supporting a plurality of crucibles, each of the crucibles containing a sample of a material to be analyzed;

oxygen line means for selectively flooding said furnace with oxygen to facilitate oxidation of the samples during analysis, said oxygen line means including a first end to be coupled to an oxygen source, a second end communicating with said furnace chamber, and a valve means between said first and second ends for controlling the flow of oxygen through said line means;

transport means for moving said sample-holding means to individually repetitively deposit the crucibles in a predetermined sequence on said weigh platform, said transport means including elevator means for vertically shifting said sample-holding means with respect to said weigh platform to deposit a crucible on, and lift a crucible off, said weigh platform;

control circuit means coupled to said balance for monitoring the individual weights of the crucibles to determine individual weight loss of the samples and calculate proximate analysis results, said control circuit means including computer means for determining when the weights of the samples have attained constant values indicating that a proximate analysis step is complete; and

means coupled to said circuit means for displaying said results.

7. A device as defined in claim 6 further comprising gas line means for selectively flooding said furnace with a gas devoid of oxygen to prevent oxidation of the samples during analysis, said gas line means including a first end to be coupled to a gas source, a second end communicating with said furnace chamber, and a valve means between said first and second ends for controlling the flow of gas through said line means.

8. A device as defined in claim 6 wherein said furnace comprises a lower container having an upper open end and a cover for selectively closing said container, said cover movable between open and closed positions, and wherein said transport means includes means for elevating said sample-holding means to a position proximate said upper end when said cover is in said open position to facilitate loading of the crucibles.