Cell for the measurement of the dielectric constant of viscous or pasty substances

• US 4,546,312 A
• Filed: 03/04/1983
• Issued: 10/08/1985
• Est. Priority Date: 03/04/1982
• Status: Expired due to Fees

• Current Assignee: L'Oreal SA
• Original Assignee: L'Oreal SA
• Inventors: Mellul, Myriam, Marcotte, Louis, Brun, Alain M.
• Primary Examiner(s): Krawczewicz, Stanley T.
• Assistant Examiner(s): Solis, Jose M.
• Application Number:
  US06/472,247
• Time in Patent Office: 949 Days
• Field of Search: 324/71.1, 324/61 P, 324/61 R, 324/65 P
• US Class Current: 324/690
• CPC Class Codes: G01N 27/226 Construction of measuring vessels; Electrodes therefor
• CPC Class Codes: G01R 27/2635 Sample holders, electrodes or excitation arrangements, e.g. sensors or measuring cells

Abstract

A cell for the measurement of the dielectric properties of liquids, pastes or flowable solids (i.e. solids whose melting temperatures are low enough to allow them to be poured into the cell) comprises a bullet-shaped internal electrode having its cylindrical portion in register with a surrounding coaxial cylindrical external electrode which is extended at each end by electrically conductive annular guard members insulated from the external electrode by means of spacers of electrically insulating material.

The internal electrode is mounted coaxially within the external electrode by means of a tapered male-female centering connector whose male and female elements are both connected to earth.

Claims

1. In a cell for the measurement of the dielectric properties of a viscous or pasty substance comprising:

first and second separable elements, said first separable element having an outer cylindrical electrically conductive surface and forming an internal electrode and said second separable element having an inner cylindrical electrically conductive surface and forming an external electrode;

a first terminal connected to said first separable element;

a second terminal connected to said second separable element; and

centering means to keep said first and second separable elements in cooperation with each other in an operating position wherein said inner and outer cylindrical electrically conductive surfaces are substantially coaxial and are at least partly disposed opposite each other;

the improvement comprising;

(a) inner cylindrical surface means extending said inner cylindrical surface of the external electrode at each one of its ends, said inner cylindrical surface means comprising means defining an electrically insulating surface adjacent to said inner cylindrical surface of the external electrode and also an electrically conductive cylindrical surface therebeyond, the said electrically conducting inner surfaces of the inner surface means being insulated in relation to the external electrode;

(b) a third terminal electrically connected to both of said electrically conductive inner surfaces of the inner surface means;

(c) a frustoconical male element of said centering means, formed on said first element and having the same axis of revolution as said internal electrode thereof; and

(d) a frustoconical female element of said centering means, formed in said second element and having the same axis of revolution as the external electrode thereof, said male and female elements of said centering means having respective frustoconoical surfaces which are both electrically conductive and said third terminal comprising an electrical conductor connected to the conductive surfaces of said first element and a separate electrical conductor connected to the conductive surface of said second element whereby said conductive surfaces of said first and second elements may be connected to a potential ground, said first element having a base with said male element being formed on said base and insulating means being disposed between said internal electrode and said male element.

2. A cell according to claim 1, wherein said inner cylindrical surface means are formed by first and second electrically insulating annular members and first and second electrically conductive annular members;

including screw means holding said annular members held on the external electrode, said screw means passing through said first electrically conductive annular member, said first electrically insulating annular member, the external electrode and said second electrically insulating annular member, and including means electrically insulating said screw means in relation to the external electrode and means electrically contacting said screw means with said first and second electrically conducting annular members.

3. A cell according to claim 2, wherein said internal electrode has first and second ends with said centering means at said first end, and wherein said second end of said internal electrode projects beyond said first electrically conductive annular member.

4. A cell according to claim 2, wherein said second electrically conductive annular member forms said female element of the centering means.

5. A cell according to claim 1, wherein said third and fourth terminals are earth terminals to be interconnected during operation of said cell.

6. A cell according to claim 5, wherein said third and fourth terminals form means protecting the second and first terminals respectively.

7. A cell according to claim 2, wherein the external electrode has a first thermal expansion coefficient, the material of the first and second electrically insulating annular members has a second thermal expansion coefficient, the material of the first and second electrically conductive annular members has a third thermal expansion coefficient, the internal electrode has a fourth thermal expansion coefficient, the male element of the centering means has a fifth thermal expansion coefficient, and the internal electrode is mounted on said male element by means having a sixth thermal expansion coefficient;

and wherein said first, second and third thermal expansion coefficients are sufficiently close to said fourth, fifth and sixth thermal expansion coefficients for the relative positioning of the internal and external electrodes not to be substantially modified by variations in temperature.

8. A cell according to claim 7, wherein at least two of said first, second and third thermal expansion coefficients are identical.

9. A cell according to claim 7, wherein at least two of said fourth, fifth and sixth thermal expansion coefficients are identical.

10. A cell according to claim 1, including means thermostatically controlling said external electrode.

11. A cell according to claim 10, wherein said thermostatically controlling means comprises fluid circulation conduits of the external electrode for the circulation of a fluid in heat-conducting relation therewith, and means electrically insulating a fluid in said fluid circulation conduits from said external electrode.