Ceramic testing method

• US 4,559,824 A
• Filed: 05/24/1984
• Issued: 12/24/1985
• Est. Priority Date: 06/17/1983
• Status: Expired due to Term

• Current Assignee: NGK Insulators Limited
• Original Assignee: NGK Insulators Limited
• Inventors: Matsui, Minoru, Soma, Takao
• Primary Examiner(s): LINDSAY JR, ROBERT
• Application Number:
  US06/613,534
• Time in Patent Office: 579 Days
• Field of Search: 73/432 Z, 73/432 R, 374/4, 374/5, 374/10, 374/24, 374/45, 374/46, 374/57, 501/104, 501/103
• US Class Current: 73/866
• CPC Class Codes: G01N 17/00 Investigating resistance of materials to the weather, to corrosion, or to light
• CPC Class Codes: G01N 33/388 Ceramics

Abstract

A method for determining an amount of non-stabilized zirconia in a ceramic specimen involves subjecting the ceramic specimen to an environment having a controlled temperature and humidity and measuring mechanical and/or chemical properties of the specimen to determine if any deterioration of the specimen has occurred.

Claims

1. A ceramic testing method comprising the steps of heating a ceramic specimen containing tetragonal zirconia in water or a water vapor atmosphere containing not less than 2.5 g/l of water at a temperature in a range of 150°

-1,250°

C., for a time sufficient to result in deterioration of any non-stabilized zirconia that is present in said ceramic specimen, and measuring the degree of deterioration of the ceramic specimen to evaluate long term durability and reliability of the ceramic specimen.

4. A ceramic testing method as set forth in claim 1, wherein said ceramic specimen contains not less than 5% by weight of zirconia.

5. A ceramic testing method as set forth in claim 1, wherein said ceramic specimen contains not less than 50% by weight of zirconia.

6. A ceramic testing method as set forth in claim 1, wherein said measuring of the ceramic specimen comprises a process selected from the group consisting of visual inspection for surface cracks, dye-absorption crack testing, supersonic crack detecting, X-ray penetration detecting, thermal expansion measurement, X-ray diffraction measurement, strength measurement, thermal shock resistance measurement, shape measurement and ionic conductivity measurement.

7. A ceramic testing method as set forth in claim 1, wherein said heating is effected at a temperature in a range of 150°

-500°

C.

8. A ceramic testing method as set forth in claim 1, wherein said ceramic specimen is resistive against mechanical and thermal stresses including regular thermal stress, thermal shock stress, repeated stress, and repeated thermal stress.

9. A ceramic testing method as set forth in claim 1, wherein said ceramic specimen is resistive against acidic corrosion.

10. A ceramic testing method as set forth in claim 1, wherein said ceramic specimen is resistive against alkali corrosion.

2. A ceramic testing method comprising the steps of heating a ceramic specimen containing not less than 5% by weight of tetragonal zirconia in water or a water vapor atmosphere containing not less than 2.5 g/l of water at a temperature in a range of 150°

-500°

C. for a period of time between one hour and one hundred hours sufficient to result in deterioration of any non-stabilized zirconia that is present in said ceramic specimen, and measuring the degree of deterioration of the ceramic specimen to evaluate long term durability and reliability of the ceramic specimen.

3. A ceramic testing method as set forth in claim 2, wherein said measuring of the ceramic specimen comprises a process selected from the group consisting of visual inspection for surface cracks, dye-absorption crack testing, supersonic crack detecting, X-ray penetration detecting, thermal expansion measurement, X-ray diffraction measurement, strength measurement, thermal shock resistance measurement, shape measurement and ionic conductivity measurement.