Method of and apparatus for analyzing atmosphere of a furnace

• US 4,565,561 A
• Filed: 12/05/1984
• Issued: 01/21/1986
• Est. Priority Date: 12/05/1984
• Status: Expired due to Term

• Current Assignee: PPG Industries Incorporated (Nouryon BV)
• Original Assignee: PPG Industries Incorporated (Nouryon BV)
• Inventors: Gagne, Robert
• Primary Examiner(s): Lindsay, Robert
• Application Number:
  US06/678,425
• Time in Patent Office: 412 Days
• Field of Search: 65/158, 65/162, 65/DIG. 13, 65/135, 73/23, 422/62, 422/111, 432/181, 432/182
• US Class Current: 65/134.2
• CPC Class Codes: C03B 5/237 Regenerators or recuperators specially adapted for glass-melting furnaces
• CPC Class Codes: C03B 5/24 Automatically regulating the melting process
• CPC Class Codes: G01N 1/24 Suction devices G01N1/22 - G01N1/2294 take precedence
• CPC Class Codes: G01N 2001/242 Injectors or ejectors
• CPC Class Codes: G01N 33/0009 General constructional details of gas analysers, e.g. portable test equipment G01N1/22 takes precedence
• CPC Class Codes: Y02P 40/50 Glass production, e.g. reusing waste heat during processing or shaping
• CPC Class Codes: Y10S 65/13 Computer control

Abstract

An apparatus for monitoring a negative pressure atmosphere, e.g. a regenerative furnace atmosphere during an exhaust cycle, has aspirating facilities for aspirating an atmospheric sample from the negative pressure atmosphere and moving the sample past an analyzer for content analysis thereof.

Claims

1. A method for monitoring the interior atmosphere of a furnace wherein the pressure of the furnace interior atmosphere is less than that of the furnace exterior atmosphere, including the steps of:

providing a fluid flow conductor communicating at one end with the furnace interior atmosphere and at its opposite end with the furnace exterior atmosphere;

creating at least a partial vacuum within said fluid flow conductor to aspirate a portion or sample of the furnace interior atmosphere through said fluid flow conductor to the furnace exterior atmosphere;

moving at least a portion of said sample past said analyzing means; and

analyzing said sample to monitor said sample with respect to its content.

2. The method as set forth in claim 1, wherein said analyzing step includes determining oxygen content in said sample, and wherein it further includes the step of controlling oxygen content in the chamber atmosphere in response to said analyzing step.

3. An apparatus for monitoring the interior atmosphere of a furnace, including:

means disposed exteriorly of the furnace for analyzing a portion of the furnace interior atmosphere having a pressure less than that of the furnace exterior atmosphere, said portions being defined as a sample; and

means for aspirating said sample from the furnace interior to said analyzing means for analysis of said sample, said aspirating means including;

a fluid flow conductor communicating at one end with the furnace interior atmosphere and at its opposite end with the furnace exterior atmosphere;

means for fluidly interconnecting said analyzing means and said fluid flow conductor; and

means for creating at least a partial vacuum within said fluid flow conductor for inducing said sample to flow from the furnace interior through said fluid flow conductor to the furnace exterior atmosphere, at least a portion of said sample being moved past said analyzing means for analysis of said sample.

4. The apparatus as set forth in claim 3, wherein said fluidly interconnecting means include a convection pipe loop having a sample entrance end and a sample exit end, said at least a portion of said sample being convected through said convection pipe loop, prior to exiting said fluid flow conductor, and past said analyzing means for analysis of said sample.

5. The apparatus as set forth in claim 4, wherein said fluid flow conductor includes:

a refractory adaptor block having a sample passageway extending between and through first and second ends of said adaptor block;

means for mounting said adaptor block in an outside wall of said furnace at a location such that said sample passageway communicates at one end with said furnace interior atmosphere; and

a sample conduit fluidly connected at one end with the opposite end of said sample passageway, and at its opposite end with said furnace exterior atmosphere, and intermediately to said convection pipe loop.

6. An apparatus for monitoring the interior atmosphere of a regenerative glassmaking furnace, including:

means disposed exteriorly of the furnace for analyzing a portion of the furnace interior atosphere defined as a sample;

means for aspirating said sample from the furnace interior to said analyzing means for analysis of said sample, said aspirating means including;

a refractory adaptor block having a sample passageway extending between and through first and second ends of said adaptor block;

means for mounting said adaptor block in an outside wall of the furnace at a location such that said sample passageway communicates at one end with the interior atmosphere of the furnace;

a sample conduit fluidly connected at one end with the opposite end of said sample passageway, and at its opposite end with the furnace exterior atmosphere;

a convection pipe loop having a sample entrance end and a sample exit end disposed in fluid communication with said sample conduit at spaced points intermediate said ends of said sample conduit, at least a portion of said sample being convected through said convection pipe loop, prior to exiting said sample conduit, and past said analyzing means for analysis of said sample; and

a vacuum creating means, including;

a portion of said sample conduit located downstream of said convection pipe loop, wherein said portion is bent so as to project substantially laterally with respect to the other or unbent portion of said sample conduit;

an aperture provided through a wall of said sample conduit opposite a central portion of the interior of said bent portion; and

means for directing pressurized fluid from a source of pressurized fluid through said aperture and thence through said central portion of said bent portion interior to said furnace exterior atmosphere, to thereby create at least a partial vacuum within said sample conduit; and

wherein the pressure differential between the furnace interior and the furnace exterior is negative.

7. The apparatus as set forth in claim 6, wherein said directing pressurized fluid means includes an aspirator conduit fluidly interconnecting said pressurized fluid source with said bent portion interior central portion through said aperture.

8. The apparatus as set forth in claim 7, wherein said directing pressurized fluid means further includes means for amplifying the flow of said pressurized fluid through said bent portion interior central portion, to maximize the vacuum created in said sample conduit and to minimize pressurized fluid consumption.

9. The apparatus as set forth in claim 8, wherein said amplifying means includes:

an elongated tube having an unsealed end portion fluidly connected to said aspirator conduit and a diametrically decreasing tapered, sealed opposite end portion; and

a slot provided through said tube around at least a portion of the periphery thereof between said end portions thereof for directing said pressurized fluid therethrough and thenceforth along at least a portion of said tapered, sealed opposite end portion in close relation thereto to establish a fluid flow pattern corresponding to the shape of said opposite end portion, to thereby entrain a portion of the interior atmosphere of said sample conduit to flow therewith through said bent portion interior to said furnace exterior atmosphere, to thereby create at least a partial vacuum within said sample conduit.

10. The apparatus as set forth in claim 8, wherein said amplifying means includes a flow amplifier of the type sold by Vortec Corporation of Cincinatti, Ohio under their trademark flo-gain®

nozzle.

11. The apparatus as set forth in claim 6, wherein it further includes means for minimizing material buildup and sample residue within the interior of said sample conduit to minimize distortion of said analysis performed by said analyzing means due to dilution of said sample by material buildup and sample residue within said sample conduit.

12. The apparatus as set forth in claim 11, wherein the furnace is a regenerative furnace characterized by a pair of opposed first and second regenerators flanking and fluidly communicating with a combustion chamber, wherein each regenerator has an upper plenum communicating with the combustion chamber, a lower plenum communicating with the furnace exterior atmosphere, and a refractory packing bed interposed therebetween, wherein air for combustion passes upwardly through said first regenerator where it is preheated by passing over said refractory packing bed of said first regenerator and then into said combustion chamber, where it combines with fuel in said chamber, whereupon flames issue into said chamber and hot exhaust gases issue into said second regenerator, the hot exhaust gases passing over and heating said refractory packing bed of said second regenerator, the mode of operation, defined as a firing cycle with respect to said first regenerator and an exhaust cycle with respect to said second regenerator, being cyclically reversed.

13. The apparatus as set forth in claim 12, wherein the furnace interior atmosphere is the interior atmosphere of said first regenerator or said second regenerator when said first or said second regenerator, respectively, is in an exhaust cycle, and wherein further, said sample includes a portion of said hot exhaust gases issuing from said combustion which takes place within said chamber.

14. The apparatus as set forth in claim 13, wherein said minimizing means includes means for directing pressurized fluid from a pressurized fluid source through the interior of said sample conduit, and thenceforth through said sample passageway into said first or said second regenerator interior atmosphere during the firing cycle of said first or said second generator.

15. The apparatus as set forth in claim 14, wherein the jointure between said sample conduit and said sample passageway includes refractory cement and is fluidly sealed by a flange and gasket assembly mounted to the furnace exterior face of said adaptor block.

16. The apparatus as set forth in claim 15, wherein said analyzing means includes a sensing device for quantitatively monitoring presence of a selected gas or gases in said sample.

17. The apparatus as set forth in claim 16, wherein said selected gas is oxygen and said regenerative furnace is of the type used for melting and/or fining glass.

18. The apparatus as set forth in claim 17, wherein it further includes means for controlling oxygen content in the chamber in response to said analyzing means.