Apparatus and method for measuring viscoelastic properties of materials

• US 4,601,195 A
• Filed: 04/11/1985
• Issued: 07/22/1986
• Est. Priority Date: 04/11/1985
• Status: Expired due to Term

• Current Assignee: Chemcial Bank, National Westminster Bank PLC, Waters Technologies Corporation (Waters Corporation)
• Original Assignee: Rheometrics, Inc.
• Inventors: Garritano, Ronald F.
• Primary Examiner(s): Levy, Stewart J.
• Assistant Examiner(s): WILLIAMS, HEZRON
• Application Number:
  US06/722,150
• Time in Patent Office: 467 Days
• Field of Search: 73/59, 73/60, 73/841, 73/843
• US Class Current: 73/54.34
• CPC Class Codes: G01N 11/10 by moving a body within the material

Abstract

Apparatus and method for measuring the viscous component and the elastic component of forces within a viscoelastic test specimen placed in shear, the test specimen being coupled to a platen having a rest position, the platen being displaceable from the rest position rotationally and axially relative to a fixed axis in response to rotational and axial forces exerted by the test specimen upon the platen as a result of the viscous component and the elastic component, the apparatus and method including an arrangement of component parts and a plurality of steps for establishing a rotational counterforce for balancing the rotational force on the platen and simultaneously establishing an axial counterforce for balancing the axial force on the platen to maintain the platen at the rest position, and indicating the magnitude of the counterforces necessary to maintain the platen at the rest position, whereby the viscous component and the elastic component of forces are measured at zero compliance.

Claims

1. Apparatus for measuring the viscous component and the elastic component of forces within a viscoelastic test specimen placed in shear, the test specimen being coupled to a platen having a rest position, the platen being displaceable from the rest position rotationally and axially relative to a fixed axis in response to rotational and axial forces exerted by the test specimen upon the platen as a result of said viscous component and said elastic component, the apparatus comprising:

a first transducer coupled with the platen for applying a rotational counterforce to the platen for biasing the platen toward the rest position;

a first detector for detecting rotational movement of the platen away from the rest position;

first drive means for actuating the first transducer in response to the first detector to balance the rotational force exerted by the test specimen upon the platen with the rotational counterforce exerted by the first transducer upon the platen and maintain the platen at the rest position;

first indicating means for indicating the magnitude of the rotational counterforce;

a second transducer coupled with the platen for applying an axial counterforce to the platen for biasing the platen toward the rest position;

a second detector for detecting axial movement of the platen away from the rest position;

second drive means for actuating the second transducer in response to the second detector to balance the axial force exerted by the test specimen upon the platen with the axial counterforce exerted by the second transducer upon the platen and maintain the platen at the rest position; and

second indicating means for indicating the magnitude of the axial counterforce;

whereby the first indicating means provides a measure of the viscous component of forces within the test specimen and the second indicating means provides a measure of the elastic component of forces within the test specimen when the platen is at the rest position.

2. The invention of claim 1 including a spindle coupled with the platen for rotational movement with the platen about the fixed axis and for axial movement with the platen along the fixed axis, and wherein the first transducer and the second transducer are coupled with the spindle such that the rotational counterforce and the axial counterforce are applied simultaneously upon the platen, and the first and second indicating means simultaneously provide a measure of the viscous component and the elastic component of the forces within the test specimen.

3. The invention of claim 2 wherein the spindle is constructed of a non-magnetic material.

4. The invention of claim 3 wherein the first and second transducers each include at least one movable component part coupled for movement with the spindle and each said movable component part is constructed of non-magnetic materials.

5. The invention of claim 2 wherein the first detector and the second detector both are coupled with the spindle.

6. The invention of claim 5 wherein the spindle is constructed of a non-magnetic material.

7. The invention of claim 6 wherein the first and second detectors each include at least one movable member coupled for movement with the spindle and each said movable member is constructed of non-magnetic materials.

8. The invention of claim 7 wherein the first and second transducers each include at least one movable component part coupled for movement with the spindle and each said movable component part is constructed of non-magnetic materials.

9. The invention of claim 2 wherein at least one of the first detector and the second detector comprises variable capacitance means coupled to the spindle.

10. The invention of claim 9 wherein at least one of the first detector and the second detector includes a first capacitive element and a second capacitive element, the second capacitive element being carried by the spindle for movement relative to the first capacitive element to change the capacitance of the variable capacitance means.

11. The invention of claim 10 including means mounting the second capacitive element of the first detector for rotational movement with the spindle to change the capacitance of the variable capacitance means.

12. The invention of claim 11 wherein the second capacitive element of the first detector is movable with the spindle axially relative to the first capacitive element without a change in the capacitance of the variable capacitance means.

13. The invention of claim 10 including means mounting the second capacitive element of the second detector for axial movement with the spindle to change the capacitance of the variable capacitance means.

14. The invention of claim 13 wherein the second capacitive element of the second detector is movable with the spindle rotationally relative to the first capacitive element without a change in the capacitance of the variable capacitance means.

15. The invention of claim 10 wherein the spindle and the second capacitive element both are constructed of non-magnetic materials.

16. The invention of claim 1 wherein at least one of the first detector and the second detector comprises variable capacitance means responsive to movement of the platen.

17. The invention of claim 16 wherein at least one of the first detector and the second detector includes a first capacitive element and a second capacitive element, the second capacitive element being coupled with the platen for movement relative to the first capacitive element to change the capacitance of the variable capacitance means.

18. The invention of claim 17 including means mounting the second capacitive element of the first detector for rotational movement with the platen to change the capacitance of the variable capacitance means.

19. The invention of claim 18 wherein the second capacitive element of the first detector is movable with the platen axially relative to the first capacitive element without a change in the capacitance of the variable capacitance means.

20. The invention of claim 17 including means mounting the second capacitive element of the second detector for axial movement with the platen to change the capacitance of the variable capacitance means.

21. The invention of claim 20 wherein the second capacitive element of the second detector is movable with the platen rotationally relative to the first capacitive element without a change in the capacitance of the variable capacitance means.

22. The method of measuring the viscous component and the elastic component of forces within a viscoelastic test specimen placed in shear, the test specimen being coupled to a platen having a rest position, the platen being displaceable from the rest position rotationally and axially relative to a fixed axis in response to rotational and axial forces exerted by the test specimen upon the platen as a result of said viscous component and said elastic component, the method comprising the steps of:

applying a rotational counterforce to the platen for biasing the platen toward the rest position;

balancing the rotational force exerted by the test specimen upon the platen with the rotational counterforce applied to the platen to maintain the platen at the rest position;

determining the magnitude of the rotational counterforce necessary to balance the rotational force;

applying an axial counterforce to the platen for biasing the platen toward the rest position;

balancing the axial force exerted by the test specimen upon the platen with the axial counterforce applied to the platen to maintain the platen at the rest position; and

determining the magnitude of the axial counterforce necessary to balance the axial force;

whereby the magnitude of the rotational counterforce provides a measure of the viscous component of forces within the test specimen and the magnitude of the axial counterforce provides a measure of the elastic component of forces within the test specimen when the platen is at the rest position.

23. The invention of claim 22 wherein the rotational counterforce and the axial counterforce are applied simultaneously to the platen, and the magnitudes of the rotational counterforce and the axial counterforce are determined simultaneously.