Optical apparatus for identifying the individual multiparametric properties of particles or bodies in a continuous flow

• US 4,606,636 A
• Filed: 10/25/1983
• Issued: 08/19/1986
• Est. Priority Date: 10/25/1983
• Status: Expired due to Fees

• Current Assignee: Universite de Saint-Etienne
• Original Assignee: Universite de Saint-Etienne
• Inventors: Faure, Bernard, Soldat, Georges, Monin, Jean, Healy, Jean-Claude
• Primary Examiner(s): NOT, DEFINED
• Assistant Examiner(s): Harringa, Joel L.
• Application Number:
  US06/545,100
• Time in Patent Office: 1,029 Days
• Field of Search: 356/336, 356/338, 356/339, 356/410, 356/318, 250/574, 250/576
• US Class Current: 356/338
• CPC Class Codes: G01N 15/1436 the optical arrangement forming an integrated apparatus with the sample container, e.g. a flow cell
• CPC Class Codes: G01N 2015/1477 Multiparameters
• CPC Class Codes: G01N 2015/1486 Counting the particles
• CPC Class Codes: G01N 2015/1493 Particle size
• CPC Class Codes: G01N 2021/4702 Global scatter; Total scatter, excluding reflections
• CPC Class Codes: G01N 2021/6469 Cavity, e.g. ellipsoid

Abstract

Apparatus for identifying multiparametric properties of particles, comprising:

a non-divergent quadric reflector,

a transparent capillary tube passing through the focus of said reflector,

at least one means of irradiating the focus,

a mask obstructing the non-reflected scattered rays,

a photosensitive cell receiving the reflected scattered rays,

and means of processing the signals.

An application to the monitoring of latex particle size distribution is described.

Claims

1. An optical apparatus for identifying individual multiparametric properties of particles or bodies moving in a continuous flow, said apparatus comprising:

an open-ended, non divergent quadric reflector having a focal point,

a transparent, continuous capillary tube passing through said focal point of said reflector and providing for the movement, individually, of particles in suspension in a fluid medium,

radiating means capable of directing a beam of radiation normal to the direction of particle movement in said capillary tube through said focal point, said beam of radiation upon striking said particle producing different rays,

a mask obstructing a portion of said diffracted rays scattered by a particle intersecting the incident beam of the radiating means at the reflector focus and not striking the reflector,

a detecting means for receiving the various reflected scattered rays for producing a signal thereof,

and means for processing and using said signals supplied by said detecting means.

2. An apparatus as in claim 1, wherein said capillary tube passes through the apex of said reflector and extends along the axis of revolution of said reflector and wherein at least one radiating means is provided, comprising a source positioned in radial relation to the reflector and emitting a beam aimed at said reflector focus.

3. An apparatus as in claim 2, wherein said mask is supported by said tube.

4. An apparatus as in claim 1, wherein said capillary tube is installed in a plane perpendicular to the reflector'"'"'s axis of revolution, said capillary tube passing through said focus where it intersects the beam of at least one radiating means.

5. An apparatus as in claim 2, comprising a plurality of radiating means each emitting at a different wavelength.

6. An apparatus as in claim 5, wherein a borehole is provided through the reflector for each radiating means at a point diametrically opposite the point occupied by said means.

7. An apparatus as in claim 1, wherein the radiating means provides an irradiated spot at the focus on the same order of size as the particle to be identified.

8. An apparatus as in claim 1, wherein the radiating means comprises a laser beam source.

9. An apparatus as in claim 1, wherein the detecting means consists of a photosensitive sensor.

10. An apparatus as in claim 1, wherein the transparent capillary tube has a useful internal cross-section substantially related to the average dimension of the particles under study so as to allow only a particle by particle progress through the measuring space intersected by the radiating means.

11. An apparatus as in claim 1, wherein the detecting means consists of an optical scanner.

12. An apparatus as in claim 1, wherein the detecting means consists of a video camera.