Vacuum impregnation of sintered materials with dry lubricant

• US 4,655,610 A
• Filed: 11/22/1985
• Issued: 04/07/1987
• Est. Priority Date: 02/13/1985
• Status: Expired due to Fees

• Current Assignee: International Business Machines Corporation
• Original Assignee: International Business Machines Corporation
• Inventors: Al-Jaroudi, Mohammed Y.
• Primary Examiner(s): Lusignan, Michael R.
• Application Number:
  US06/800,881
• Time in Patent Office: 501 Days
• Field of Search: 252/12, 252/12.2, 252/29, 252/30, 427/294, 427/295, 427/385.5, 384/13, 384/279, 384/909
• US Class Current: 384/13
• CPC Class Codes: B22F 3/26 Impregnating making ferrous alloys by impregnation C22C33/0242
• CPC Class Codes: F16C 33/12 Structural composition; Use of special materials or surface treatments, e.g. for rust-proofing
• CPC Class Codes: Y10S 384/909 Plastic

Abstract

A method for vacuum impregnation of sintered materials, preferably vacuum impregnation of sintered bearings parts, with dry lubricants is disclosed. The impregnation is performed in the following way. The cleaned parts to be impregnated are placed in a glass basin containing a mixture of, for example, molybdenum disulphide and graphite, a thermosetting resin, a solvent and a thermosetting resin extender. The glass basin is placed in a vacuum chamber and the vacuum chamber is then vacuum pumped for a sufficiently long time in order to evacuate the air from the pores of the sintered parts. After that air is again let in into the vacuum chamber until normal air pressure is reached. The sintered parts are taken out and are allowed to air dry. The coating is then cured.

Claims

1. A method for vacuum impregnation of a sintered material with a dry lubricant comprising the steps of:

placing the sintered material in a basin containing a mixture of effective amounts of the dry lubricant and a thermosetting resin dissolved in a solvent;

placing the basin in a vacuum chamber;

vacuum pumping the vacuum chamber for a sufficiently long time in order to evacuate the air from the pores of the sintered material;

letting air into the vacuum chamber until normal air pressure is reached, thereby driving said mixture into said evacuated pores;

air drying the sintered material; and

curing the dry lubricant, said dry lubricant extending slightly above said pores.

2. The method according to claim 1, wherein the dry lubricant comprises molybdenum disulphide and graphite.

3. The method according to claim 2 wherein the mixture further comprises a thermosetting resin extender.

4. The method according to claim 1 wherein the mixture further comprises a thermosetting resin extender.

5. The method according to claim 1 wherein the step of curing comprises bringing the substrate temperature to 180°

C. for one hour or to 210°

C. for thirty minutes.

6. The method according to claim 2 wherein the step of curing comprises bringing the substrate temperature to 180°

C. for one hour or to 210°

C. for thirty minutes.

7. The method according to claim 3 wherein the step of curing comprises bringing the substrate temperature to 180°

C. for one hour or to 210°

C. for thirty minutes.

8. The method according to claim 4 wherein the step of curing comprises bringing the substrate temperature to 180°

C. for one hour or to 210°

C. for thirty minutes.

9. The methods according to claim 1 wherein the step of air drying the sintered material comprises:

removing the sintered material from the vacuum chamber; and

allowing the sintered material to air dry for 10 to 15 minutes.

10. The method according to claim 2 wherein the step of air drying the sintered material comprises:

removing the sintered material from the vacuum chamber; and

allowing the sintered material to air dry for 10 to 15 minutes.

11. The method according to claim 3 wherein the step of air drying the sintered material comprises:

removing the sintered material from the vacuum chamber; and

allowing the sintered material to air dry for 10 to 15 minutes.

12. The method according to claim 4 wherein the step of air drying the sintered material comprises:

removing the sintered material from the vacuum chamber; and

allowing the sintered material to air dry for 10 to 15 minutes.

13. The method according to claim 5 wherein the step of air drying the sintered material comprises:

removing the sintered material from the vacuum chamber; and

allowing the sintered material to air dry for 10 to 15 minutes.

14. The method according to claim 6 wherein the step of air drying the sintered material comprises:

removing the sintered material from the vacuum chamber; and

allowing the sintered material to air dry for 10 to 15 minutes.

15. The method according to claim 7 wherein the step of air drying the sintered material comprises:

removing the sintered material from the vacuum chamber; and

allowing the sintered material to air dry for 10 to 15 minutes.

16. The method according to claim 8 wherein the step of air drying the sintered material comprises:

removing the sintered material from the vacuum chamber; and

allowing the sintered material to air dry for 10 to 15 minutes.

17. A wear resistant bearing for reducing wear between said bearing and a second bearing part, said wear resistant bearing comprising:

a sintered bearing having a plurality of pores;

a dry lubricant integrally contained within and extending slightly above said pores, said dry lubricant further comprising effective amounts of molybdenum disulphide, graphite and a cured resin, wherein said dry lubricant constitutes the only contact between said wear resistant bearing and said second bearing part.