Quantitative measurement of fat in dairy products

• US 4,663,530 A
• Filed: 03/21/1986
• Issued: 05/05/1987
• Est. Priority Date: 04/05/1983
• Status: Expired due to Fees

• Current Assignee: Multispec Ltd. (NWF Group PLC)
• Original Assignee: John Shields
• Inventors: Shields, John
• Primary Examiner(s): FALCONE, JANICE ARRINGTON
• Application Number:
  US06/842,312
• Time in Patent Office: 410 Days
• Field of Search: 250/339, 250/343
• US Class Current: 250/339.12
• CPC Class Codes: G01N 21/3577 for analysing liquids, e.g. polluted water
• CPC Class Codes: G01N 33/06 Determining fat content, e.g. by butyrometer
• CPC Class Codes: Y10S 250/91 Food sample analysis using invisible radiant energy source

Abstract

An infrared transmission/absorption technique for the quantitative determination of fat in dairy products, particularly high-fat dairy products having fat concentrations between 15 and 60 w/o. A wave band characteristic of bending and scissoring of saturated carbon hydrogen bonds is employed, preferably a wave band at about 6.84 microns. It is further preferred to use the double wavelength, single cuvette system. Variations in accuracy caused by lipolysis and degree of homogenization are substantially reduced.

Claims

1. A method for direct infrared measurement of milkfat concentration in the range of 15 to 60 w/o in dairy products such as cream and ice cream, said method comprising the steps of:

(a) transmitting infrared energy through a test sample of the dairy product,

(b) determining infrared absorption of the sample at a first wave band characteristic of bending and scissoring of saturated carbon-hydrogen bonds in milkfat fatty acid chains, and

(c) quantitatively determining fat concentration in the sample as a function of absorption at said first wave band.

2. The method set forth in claim 1 wherein said first wave band is in the range of about 6.75 to 7.1 microns.

3. The method set forth in claim 1 comprising the additional steps:

(d) determining infrared absorption of the sample at a second wave band adjacent to said first wave band but not characteristic of saturated carbon-hydrogen bonds, and

wherein said step (c) comprises the step comparing absorption at said first wave band to absorption at said second wave band.

4. The method set forth in claim 3 wherein said first wave band is centered at about 6.84 microns.

5. The method set forth in claim 4 wherein said second wave band is in the range of about 6.46 to 6.75 microns.

6. The method set forth in claim 4 wherein said second wave band is in the range of about 7.0 to 7.20 microns.

7. The method set forth in claim 6 wherein said second wave band is in the range of about 7.11 to 7.15 microns.

8. A method of measuring fat concentration in dairy products comprising the steps of:

irradiating a test sample with infrared energy, determining infrared absorption of said sample at a first wave band of said infrared energy characteristic of bending and scissoring of saturated carbon-hydrogen bonds, and quantitatively determining the fat concentration in said sample as a function of absorption at said first wave band.

9. The method set forth in claim 8 wherein said first wave band is from 6.75 to 7.1 microns.

10. The method set forth in claim 9 wherein said first wave band is at about 6.84 microns.

11. The method set forth in claim 10 wherein said method comprises the additional step of determining infrared absorption of said sample at a second wave band in the range of about 6.46 to 6.75 and 7.0 to 7.20 microns, and wherein said step of quantitatively determining fat concentration comprises the step of comparing absorption at said first wave band to absorption at said second wave band.

12. The method set forth in claim 11 wherein said second wave band is in the range of about 7.11 to 7.15 microns.

13. The method set forth in claim 11 comprising the additional step, prior to irradiating said sample, of reducing diameter of fat globules in said sample to not greater than 3.5 microns.

14. The method set forth in claim 10 wherein said first wave band has a band width of not greater than 110 mm.