Low moisture, sugarless, center-filled chewing gum

• US 4,683,138 A
• Filed: 09/08/1986
• Issued: 07/28/1987
• Est. Priority Date: 09/08/1986
• Status: Expired due to Term

• Current Assignee: Cadbury Adams USA LLC (Mondelez International, Inc.)
• Original Assignee: Warner-Lambert Company (Pfizer Inc.)
• Inventors: Glass, Michael, Orlandi, Daniel A., Hoholick, Joseph
• Primary Examiner(s): HUNTER, JEANETTE M
• Application Number:
  US06/905,373
• Time in Patent Office: 323 Days
• Field of Search: 426/3-6, 426/103
• US Class Current: 426/5
• CPC Class Codes: A23G 4/10 characterised by the carbohydrates used, e.g. polysaccharides containing dairy products A23G4/16
• CPC Class Codes: A23G 4/20 Composite products, e.g. centre-filled , multi-layer, laminated

Abstract

This disclosure relates to a low-moisture, sugarless, center-filled chewing gum and a process for the preparation thereof, in which a low moisture, liquid center-fill is incorporated into a cavity within a substantially anhydrous chewing gum shell. The center-filled chewing gum disclosed has improved non-staling properties and an extended shelf-life. The liquid center-fill has a water content of about 6% to about 8%, based on the total weight of the liquid center-fill, a viscosity of about 22,000 to about 85,000 centipoises at 25° C., and contains a natural or synthetic gum, a glycerin humectant and an additonal, water-miscible humectant.

Claims

1. A sugarless center-filled chewing gum piece having an outer sugarless chewing gum shell enclosing a cavity and a sugarless liquid center-fill within said cavity, said chewing gum piece comprising:

A. a chewing gum shell containing not more than about 2% by weight thereof water; and

B. a sugarless liquid center-fill comprising;

1. about 0.2% to about 1.5% by weight of a natural or synthetic gum selected from the group consisting of carboxymethylcellulose, pectin, propylene glycol alginates, agar and gum tragacanth;

2. about 85% to about 93% by weight of a glycerin humectant; and

3. about 6% to about 12% by weight of an additional water-miscible humectant ingredient selected from the group consisting of (a) sorbitol solution or (b) sorbitol solution and propylene glycol;

wherein said liquid center-fill has a water content of about 6% to about 8%, based on the total weight of the liquid center-fill, and a viscosity of about 20,000 to about 85,000 centipoises at 25°

C.

2. The sugarless center-filled chewing gum piece according to claim 1 wherein said liquid center-fill comprises about 0.2% to about 0.5% by weight of sodium carboxymethylcellulose, about 89% to about 93% by weight of glycerin, and about 6% to about 10% by weight of sorbitol solution, said liquid center-fill having a watr-content of about 6% to about 7.5%, based on the total weight of the liquid center-fill, and a viscosity of about 20,000 to about 80,000 centipoises at 25°

C.

3. The sugarless center-filled chewing gum piece according to Claim 1 wherein said liquid center-fill comprises about 1% to about 1.5% by weight of sodium carboxymethylcellulose, about 89% to about 93% by weight of glycerin, and about 6% to about 10% by weight of sorbitol solution, said liquid center-fill having a water content of about 6% to about 7.5%, based on the total weight of the liquid center-fill, and a viscosity of about 20,000 to about 80,000 centipoises at 25°

C.

4. The sugarless center-filled chewing gum piece acording to claim 1 wherein, additionally, the center-fill contains a material selected from the group consisting of a flavoring agent, a sweetening agent and mixtures thereof.

5. The sugarless center-filled chewing gum piece according to claim 4 wherein the flavoring agent is selected from the group consisting of peppermint oil, spearmint oil, cinnamon oil, oil of wintergreen (methylsalicylate), lemon oil, orange oil, grape oil, lime oil, grapefruit oil, apple essence, strawberry essence, cherry essence, pineapple essence and mixtures thereof.

6. The sugarless center-filled chewing gum piece according to claim 4 wherein the sweetening agent is selected from the group consisting of saccharin salts, cyclamate salts, Acesulfame-K salts, dipeptide based sweeteners, dihydrochalcone sweeteners, and mixtures thereof.

7. A sugarless center-filled chewing gum piece according to claim 1 wherein the liquid center-fill is incorporated into the chewing gum shell in an amount of about 11% to about 15% by weight of the chewing gum composition.

8. A sugarless liquid center-fill for incorporation into a cavity within a sugarless center-filled chewing gum piece, the shell of said chewing gum piece containing not more than about 2% by weight water, said center-fill comprising:

A. about 0.2% to about 1.5% by weight of a natural or synthetic gum selected from the group consisting of carboxymethylcellulose, pectin, propylene glycol alginates, agar and gum tragacanth;

B. about 85% to about 93% by weight of glycerin humectant; and

C. about 6% to about 12% by weight of an additional water-miscible humectant ingredient selected from the group consisting of (a) sorbitol solution or (b) sorbitol solution and propylene glycol;

wherein said sugarless center-fill has a water content of about 6% to about 8%, based on the total weight of the liquid center-fill, and a viscosity of about 20,000 to about 85,000 centipoises at 25°

C.

9. The sugarless, liquid center-fill according to claim 8 comprising about 0.2% to about 0.5% by weight of sodium carboxymethylcellulose, about 89% to about 93% by weight of glycerin, and about 6% to about 10% of weight of sorbitol solution, said liquid center-fill having a water-content of about 6% to about 7.5%, based on the total weight of the liquid center-fill, and a viscosity of about 20,000 to about 80,000 centipoises at 25°

C.

10. The sugarless liquid center-fill according to claim 8 comprising about 1% to about 1.5% by weight of sodium carboxymethylcellulose, about 89% to about 93% by weight of glycerin, and about 6% to about 10% by weight of sorbitol solution, said liquid center-fill having a water-content of about 6% to about 7.5%, based on the total weight of the liquid center-fill, and a viscosity of about 20,000 to about 80,000 centipoises at 25°

C.

11. The sugarless, liquid center-fill according to claim 8 wherein, additionally, the center-fill contains a material selected from the group consisting of a flavoring agent, a sweetening agent, and mixtures thereof.

12. The sugarless liquid center-fill according to claim 11 wherein the flavor is selected from the group consisting of peppermint oil, spearmint oil, cinnamon oil, oil of wintergreen (methylsalicylate), lemon oil, orange oil, grape oil, lime oil, grapefruit oil, apple essence, strawberry essence, cherry essence, pineapple essence and mixtures thereof.

13. The sugarless, liquid center-fill according to claim 11 wherein the sweetening agent is selected from the group consisting of saccharin salts, cyclamate salts, acesulfame K salts, dipeptide based sweeteners, dihydrochalcone sweeteners, and mixtures thereof.

14. A process for preparing the sugarless liquid center-fill of claim 8 which comprises:

A. mixing the natural or synthetic gum with the glycerin humectant in a weight ratio of from about 1;

3 to about 1;

24, based on the weight of gum to the weight of glycerin, for a time sufficient to disperse said gum in said glycerin;

B. blending the additional water-miscible humectant with an equal weight of glycerin and heating the blend to a temperature of about 60°

C. to about 80°

C.;

C. mixing the dispersion of (A) with the heated blend of (B) until a homogenous mixture is formed; and

D. adding the remaining glycerin to (C) and mixing for a time sufficient to fully hydrate the natural or synthetic gum with the water present in the reaction mixture and obtain a center-fill having a viscosity of about 20,000 to about 85,000 centipoises at 25°

C.

15. The process according to claim 14 wherein, in step (A) the natural or synthetic gum is a low viscosity carboxymethylcellulose gum and wherein the ratio of said gum to said glycerinis from about 1:

3 to about 1;

6.

16. The process according to claim 14 wherein, in step (A), the natural or synthetic gum is a high viscosity carboxymethylcellulose gum and wherein the ratio of said gum to said glycerin is from about 1:

12 to about 1;

24.

17. The process according to claim 14 wherein, in step (B) the additional water-miscible humectant is sorbitol solution.

18. The process according to claim 14 wherein the viscosity of the liquid center-fill is about 20,000 to about 80,000 centipoises at 25°

C.

19. The process according to claim 14 wherein, additionally, a material selected from the group consisting of a flavoring agent, a sweetening agent, and mixtures thereof, is added to the mixture of step (D) in an amount sufficient to impart taste thereto.

20. A process for preparing a sugarless center-filled chewing gum piece having a substantially anhydrous, sugarless outer chewing gum shell enclosing a cavity, which comprises incorporating within said cavity a sugarless liquid center-fill comprising:

(A) about 0.2% to about 1.5% by weight of a natural or synthetic gum selected from the group consisting of carboxymethylcellulose, pectin, propylene glycol alginates, agar and gum tragacanth;

(B) about 85% to about 93% by weight of a glycerin humectant; and

(C) about 6% to about 12% by weight of an additional water-miscible humectant ingredient selected from the group consisting of (a) sorbitol solution or (b) sorbitol solution and propylene glycol;

wherein said liquid center-fill has a water content of about 6% to about 8%, based on the total weight of the liquid center-fill, and a viscosity of about 20,000 to about 85,000 centipoises at 25°

C.

21. The process according to claim 20 wherein the liquid center-fill comprises about 0.2% to about 0.5% by weight of sodium carboxymethylcellulose, about 89% to about 93% by weight of glycerin, and about 6% to about 10% by weight of sorbitol solution, said liquid center-fill having a water-content of about 6% to about 7.5%, based on the total weight of the liquid center-fill and a viscosity of about 20,000 to about 80,000 centipoises at 25°

C.

22. The process according to claim 20 wherein the liquid center-fill comprises about 1% to about 1.5% by weight of sodium carboxymethylcellulose, about 89% to about 93% by weight of glycerin, and about 6% to about 10% by weight of sorbitol solution, said liquid center-fill having a water-content of about 6% to about 7.5%, based on the total weight of the liquid center-fill, and a viscosity of about 20,000 to about 80,000 centipoises at 25°

C.

23. The process according to claim 20 wherein the liquid center-fill is incorporated into the chewing gum shell in an amount of about 11% to about 15% by weight of the chewing gum piece.