Near infrared measuring instrument with sample holder

• US 4,692,620 A
• Filed: 05/31/1985
• Issued: 09/08/1987
• Est. Priority Date: 05/31/1985
• Status: Expired due to Term

• Current Assignee: Trebor Industries Incorporated (Brownie's Marine Group Incorporated)
• Original Assignee: Trebor Industries Incorporated (Brownie's Marine Group Incorporated)
• Inventors: Rosenthal, Robert D.
• Primary Examiner(s): FIELDS, CAROLYN
• Application Number:
  US06/739,679
• Time in Patent Office: 830 Days
• Field of Search: 356/246, 356/440, 356/436, 356/409, 356/414, 250/328, 250/339, 250/341, 250/359.1, 250/343
• US Class Current: 250/343
• CPC Class Codes: G01N 2021/5973 where the cuvette or tube is moved
• CPC Class Codes: G01N 21/3554 for determining moisture content
• CPC Class Codes: G01N 21/3563 for analysing solids; Preparation of samples therefor
• CPC Class Codes: G01N 21/359 using near infrared light
• CPC Class Codes: Y10S 250/91 Food sample analysis using invisible radiant energy source

Abstract

Near infrared instrument for measuring constituents such as moisture, protein and oil in materials has a movable sample holder of predetermined thickness depending upon the particular material being measured. The sample holder is moved past a source of near infrared radiation and detector by a mechanical drive.

Claims

1. A near infrared measuring instrument for measuring a constituent of a material, the instrument being of the type having a source of near infrared radiation, a detector for near infrared radiation, a means for holding a sample between the source and the detector, and means for data processing connected to the detector to read the detector and measure a constituent in a sample of the material by the amount of near infrared radiation transmitted through the sample, with the improvements comprising:

(a) means for providing a plurality of different predetermined uniform thicknesses of samples to be measured, comprising at least one cuvette for holding a sample between the source and the detector, the cuvette having opposing faces with at least a portion thereof being transparent to near infrared radiation, the cuvette providing at least one predetermined uniform thickness between the source and the detector in order to hold a predetermined uniform thickness of sample,

(b) means for moving the cuvette relative to the near infrared radiation source and the detector and for stepwise placing a plurality of locations of the radiation-transparent portion of the cuvette and the at least one predetermined uniform thickness of sample into relative stationary alignment between the source and the detector,

(c) means for reading the detector when the cuvette is stationary, and

(d) means in the cuvette for measuring the temperature of the sample.

2. An instrument as in claim 1 wherein the cuvette includes a movable wall means for uniformly varying sample thickness in order to accommodate different samples.

3. An instrument as in claim 1 wherein the cuvette is mounted in a track for moving the cuvette relative to the near infrared radiation source and the detector.

4. An instrument as in claim 3 wherein the means for moving the cuvette includes a mechanical eccentric driven by a motor.

5. An instrument as in claim 4 further comprising means for sealing the cuvette and the inside of the instrument from ambient light.

6. An instrument as in claim 1 wherein the thickness between the walls of the cuvette is equal to one layer of a cereal grain sample.

7. An instrument as in claim 6 wherein the cuvette has means therein for positioning individual grains a single layer thick, and wherein the faces of the cuvette which allow transmission of near infrared radiation have small holes in them for the transmission of such radiation.

8. An instrument as in claim 3 wherein the means for moving the cuvette includes an intermittently moving electric motor connected to an eccentric, the eccentric contacting the cuvette.

9. An instrument as in claim 1 wherein the means for moving the cuvette includes a mechanical eccentric driven by a motor, and wherein the cuvette is mounted in a track for movement by gravity and the eccentric driven by the motor opposes the gravity.

10. An instrument as in claim 1 wherein the temperature sensing means in the cuvette is a thermister and the connections are through slidably connected conductors on the edges of the cuvette.

11. An instrument as defined in claim 1 wherein the cuvette is filled with a calibration sample and sealed.

12. An instrument as defined in claim 1 wherein the cuvette comprises means for holding a liquid sample.

13. An instrument as defined in claim 1 wherein the cuvette comprises means for holding a powder sample or other granular material sample.

14. An instrument as defined in claim 1 wherein the cuvette comprises means for holding a paste sample.

15. The instrument as defined in claim 1 wherein the means for providing a plurality of different thicknesses of samples is comprised of a plurality of cuvettes of different thicknesses.