Preparation of sintered magnets

• US 4,734,253 A
• Filed: 03/25/1987
• Issued: 03/29/1988
• Est. Priority Date: 03/25/1986
• Status: Expired due to Fees

• Current Assignee: TDK Corporation
• Original Assignee: TDK Corporation
• Inventors: Sato, Kazuo, Yamashita, Shinichi
• Primary Examiner(s): Lechert, Jr., Stephen J.
• Application Number:
  US07/029,955
• Time in Patent Office: 370 Days
• Field of Search: 148/108, 148/105, 75/244, 75/246, 252/62.55, 419/38, 419/30, 419/44, 419/62, 419/66
• US Class Current: 419/30
• CPC Class Codes: B22F 3/12 Both compacting and sintering by forging B22F3/17
• CPC Class Codes: H01F 1/0577 sintered

Abstract

A sintered magnet of Fe-B-rare earth alloy having an axis of easy magnetization oriented at an angle to a major axis can be directly produced from the alloy material by (a) press molding the material in an applied magnetic field into a compact of the dimensions determined by taking into account factors of shrinkage expected in X, Y and Z directions, and (b) sintering the compact.

Claims

1. A process for preparing a sintered magnet, comprising the steps of:

(a) press molding a magnetic powder into a compact in an applied magnetic field, said compact having coordinates (X/Sx, Y/Sy, Z/Sz) where Sx, Sy and Sz are predetermined factors of shrinkage occurring in a magnetization direction and directions perpendicular to the magnetization direction upon subsequent sintering, and

(b) sintering the compact into a sintered magnet having a major axis and an axis of easy magnetization oriented at an angle to the major axis, the sintered magnet having coordinates (X, Y, Z) with X axis aligned with the axis of easy magnetization of the sintered magnet.

2. The process of claim 1 wherein the sintered magnet is an iron-boron-rare earth metal magnet.

3. The process of claim 2 wherein Sx has a value of 0.75 to 0.85, and Sy and Sz have values of 0.85 to 0.95.

4. The process of claim 1 wherein the shrinkage factors Sx, Sy and Sz are previously determined by press molding a magnetic powder into a rectangular parallelepiped compact under the same magnetic field as applied in (a), but applied parallel to one edge of said rectangular parallelepiped compact, and sintering the compact under the same conditions as applied in (b).

5. The process of claim 1 wherein the sintered magnet is of a columnar shape having parallel extending major surfaces.

6. The process of claim 5 wherein said major surfaces are substantially parallel to the axis of easy magnetization.

7. The process of claim 6 wherein each said major surface is a quadrangular surface having two parallel sides.

8. The process of claim 7 wherein the following equations are met:

##EQU6## where each said major surface of the sintered magnet has four apexes A, B, C and D, side BC being parallel to side AD,

sides AB, BC, CD and DA have lengths a, b, c and d, respectively

angles DAB and CDA are equal to α and

β

, respectively,

the distance between the major surfaces is equal to e,

the angle of intersection between the axis of easy magnetization and side BC is equal to θ

,

the major surface of the compact has four apexes A'"'"', B'"'"', C'"'"' and D'"'"', side B'"'"'C'"'"' being parallel to side A'"'"'D'"'"',

sides A'"'"'B'"'"', B'"'"'C'"'"', C'"'"'D'"'"' and D'"'"'A'"'"' have lengths a'"'"', b'"'"', c'"'"' and d'"'"', respectively,

angles D'"'"'A'"'"'B'"'"' and C'"'"'D'"'"'A'"'"' are equal to α

'"'"' and β

'"'"', respectively,

the distance between the major surfaces is equal to e'"'"', and

the angle of intersection between the axis of easy magnetization and side B'"'"'C'"'"' is equal to θ

'"'"'.

9. A method for fabricating a sintered magnet assembly, comprising the steps of:

(a) press molding a magnetic powder into a compact in an applied magnetic field, said compact having coordinates (X/Sx, Y/Sy, Z/Sz) where Sx, Sy and Sz are predetermined factors of shrinkage occurring in a magnetization direction and directions perpendicular to the magnetization direction upon subsequent sintering,

(b) sintering the compact into a sintered magnet having parallel extending major surfaces with two parallel extending sides and having a major axis within the plane of the major surface and an axis of easy magnetization oriented at an angle to the major axis, the sintered magnet having coordinates (X, Y, Z) with X axis aligned with the axis of easy magnetization of the sintered magnet,

(c) repeating steps (a) and (b) to prepare a plurality of sintered magnets having axes of easy magnetization oriented at different angles to the respective major axes, and

(d) arranging the plurality of sintered magnets in a ring configuration whereby a predetermined magnetic field is produced within the ring.

10. The method of claim 9 wherein a unidirectional, substantially parallel extending magnetic field is produced within the ring.

11. The method of claim 9 wherein the sintered magnet is an iron-boron-rare earth metal magnet.

12. The method of claim 11 wherein Sx has a value of 0.75 to 0.85, and Sy and Sz have values of 0.85 to 0.95.

13. The method of claim 9 wherein the shrinkage factors Sx, Sy and Sz are previously determined by press molding a magnetic powder into a rectangular parallelepiped compact under the same magnetic field as applied in (a), but applied parallel to one edge of said rectangular parallelepiped compact, and sintering the compact under the same conditions as applied in (b).

14. The method of claim 9 wherein the following equations are met:

##EQU7## where each said major surface of the sintered magnet has four apexes A, B, C and D, side BC being parallel to side AD,

sides AB, BC, CD and DA have lengths a, b, c and d, respectively,

angles DAB and CDA are equal to α and

β

, respectively,

the distance between the major surfaces is equal to e,

the angle of intersection between the axis of easy magnetization and side BC is equal to θ

,

the major surface of the compact has four apexes A'"'"', B'"'"'C'"'"'and D'"'"', side B'"'"'C'"'"' being parallel to side A'"'"'D'"'"',

sides A'"'"'B'"'"', B'"'"'C'"'"', C'"'"'D'"'"' and D'"'"'A'"'"' have lengths a'"'"', b'"'"', c'"'"' and d'"'"', respectively,

angles D'"'"'A'"'"'B'"'"' and C'"'"'D'"'"'A'"'"' are equal to α

'"'"' and β

'"'"', respectively,

the distance between the major surfaces is equal to e'"'"', and

the angle of intersection between the axis of easy magnetization and side B'"'"'C'"'"' is equal to θ

'"'"'.