Cylindrical NMR bias magnet apparatus employing permanent magnets and methods therefor

• US 4,758,813 A
• Filed: 06/24/1987
• Issued: 07/19/1988
• Est. Priority Date: 06/24/1987
• Status: Expired due to Fees

• Current Assignee: Field Effects Incorporated
• Original Assignee: Field Effects Incorporated
• Inventors: Fisher, John C., Gluckstern, Robert L., Holsinger, Ronald F.
• Primary Examiner(s): Harris, George
• Application Number:
  US07/065,957
• Time in Patent Office: 391 Days
• Field of Search: 335/302, 335/306, 335/299, 335/296, 324/318, 324/319, 324/320, 29/599
• US Class Current: 335/306
• CPC Class Codes: G01R 33/383 using permanent magnets
• CPC Class Codes: H01F 7/0278 for generating uniform fields, focusing, deflecting electrically charged particles for magnetic separation by Lorentz force B03C1/023; specially adapted for NMR applications G01R33/383
• CPC Class Codes: Y10T 29/49014 Superconductor

Abstract

NMR bias magnet apparatus employing permanent magnets and methods therefor are provided in accordance with the teachings of the present invention. According to the present invention a plurality of insulating sleeves which may be rotated are disposed about the periphery of a structure having a curvilinear cross section such as a cylinder. Each of the plurality of insulating sleeves are filled with stacks of slabs of permanent magnet material forming slugs and having an anisotropic axis of magnetic orientation aligned at an azimuth corresponding to a=2φ. The length of slug sections or even of individual slabs within each sleeve may be varied for purposes of introducing desired harmonics, as may the manner in which each sleeve is filled, so long as quadrature symmetry is maintained.

Claims

1. Magnetic bias apparatus comprising:

a plurality of elongated sleeves each having a longitudinal axis and being disposed parallel to each other, said sleeves arranged around a closed curvilinear space to define a bore therein, each of said plurality of sleeves being rotatable about its longitudinal axis; and

a plurality of rectangular permanent magnet slabs mounted in each of said plurality of sleeves, each of said plurality of permanent magnet slabs having a length, width and thickness dimension and being stacked in the thickness dimension within each of said plurality of sleeves with said length dimension parallel to the longitudinal axis, each of said plurality of rectangular permanent magnet slabs having an anisotropic axis of magnetic orientation parallel to said thickness direction and stacked in a magnetically aiding relation in said thickness direction whereby the magnetic field exhibited through at least a portion of said bore may be maximized and rendered more uniform by rotation of said sleeves to a selected orientation.

2. The apparatus according to claim 1 wherein said plurality of sleeves define a cylindrical arrangement including a circular bore.

3. The apparatus according to claim 2 wherein said plurality of sleeves are disposed substantially adjacent one another about said bore and further comprising means for joining each sleeve to its adjacent sleeves.

4. The apparatus according to claim 3 wherein each of said plurality of sleeves is disposed a common radial distance from a central location of said circular bore and is positioned at an angle φ

from a vertical axis of said circular bore.

5. The apparatus according to claim 4 wherien said selected orientation for each of said plurality of sleeves is an orientation wherein said anisotropic axis of magnetic orientation of said plurality of rectangular permanent magnetic slabs stacked within each sleeve exhibits an azimuth a equal to twice said angle φ

.

6. The apparatus according to claim 1 wherein said plurality of sleeves are equally spaced about the periphery of said bore and the magnetic field exhibited by said apparatus displays substantial quadrature symmetry.

7. The apparatus according to claim 6 wherein said plurality of sleeves correspond in number to a whole number N where N/4 is also equal to a whole number.

8. The apparatus according to claim 7 wherein the magnetic characteristics of each sleeve within a grouping of N/4 sleeves may vary and the magnetic characteristics of each grouping of N/4 sleeves are substantially the same.

9. The apparatus according to claim 1 wherein at least two of said plurality of rectangular permanent magnet slabs mounted in at least certain ones of said plurality of sleeves are segmented in said length dimension to provide position adjustment of said at least two of said plurality of rectangular permanent magnet slabs in said length dimension.

10. The apparatus according to claim 9 wherein said plurality of rectangular permanent magnetic slabs mounted in each of said plurality of sleeves are symmetrically stacked.

11. The apparatus according to claim 10 wherein said plurality of rectangular permanent magnetic slabs display differing widths.

12. The apparatus according to claim 11 wherein said plurality of permanent magnetic slabs within a sleeve provides a cross sectional arrangement having quadrature symmetry within the sleeve.

13. The apparatus according to claim 12, and further comprising spacer material longitudinally positioned in the sleeve between at least a portion of the periphery of the slab and the sleeve.

14. The apparatus according to claim 13 wherein said spacer is of non-conductive, non-magnetic material.

15. The apparatus according to claim 9 wherein the slabs within each sleeve are stacked together to form slugs, said slugs being sectional longitudinally within each sleeve, and further comprising spacers positioned within the sleeve longitudinally between each adjacent slug section.

16. The apparatus according to claim 15 wherein said spacer material is non-conductive and non-magnetic.

17. The apparatus according to claim 15 wherein said spacer material is air.

18. The apparatus accoding to claim 15 wherein each slug section ends in a planar arrangement.

19. The apparatus according to claim 15 wherein the slug section arrangement differs longitudinally from sleeve to sleeve.

20. The apparatus according to claim 15 and further comprising means for adjusting the longitudinal position of each slug section within its sleeve to permit tuning for elimination of selective harmonics.

21. The apparatus according to claim 1 wherein certain of said plurality of rectangular permanent magnet slabs mounted in at least one fourth of said plurality of sleeves are segmented in said length dimension to provide for introduction of selected harmonics in the magnetic bias apparatus.

22. The apparatus according to claim 1 and further comprising support longitudinally positioned along the length of the assembly of sleeves for supporting the sleeves.

23. Magnetic bias apparatus comprising:

N nonconductive elongated sleeves each having a longitudinal axis, said sleeves disposed parallel to each other and arranged around a closed curvilinear space to define a bore therein, each of said N sleeves being rotatable about an axis parallel to said longitudinal axis;

nonconductive permanent magnet material mounted in each of said N sleeves, said permanent magnet material having a length, width and thickness dimension and exhibiting an anisotropic axis of magnetic orientation parallel to said thickness direction, said nonconductive permanent magnet material being segmented in said length dimension to provide for introduction of selected magnetic harmonics whereby the magnetic field exhibited through at least a portion of said bore may be maximized and rendered more uniform by rotation of said sleeves to a selected orientation; and

where N and N/4 are whole numbers and the magnetic characteristics of each sleeve within a grouping of N/4 sleeves may vary and the magnetic characteristics of each grouping of N/4 sleeves are substantially the same.

24. The apparatus according to claim 23 wherein said plurality of sleeves defining a cylindrical arrangement including a circular bore.

25. The apparatus according to claim 24 wherein each of said N sleeves is disposed a common radial distance from a central location on said circular bore and is positioned at an angle φ

from a vertical axis of said circular bore.

26. The apparatus acording to claim 23 wherein said N sleeves are equally spaced about the periphery of said bore and the magnetic field exhibited by said apparatus displays substantial quadrature symmetry.

27. The apparatus according to claim 24 wherein said permanent magnet material mounted in each of said N sleeves takes the form of a plurality of rectangular magnetic slabs mounted in each of the sleeves, each of said plurality of rectangular permanent magnetic slabs having a length, width and thickness dimension and being stacked in the thickness direction with said length dimension parallel to said longitudinal axis, each of said plurality of rectangular permanent magnetic slabs having an anisotropic axis of magnetic orientation parallel to said thickness direction and stacked in a magnetically aiding relation in said thickness direction.

28. The apparatus according to claim 27 wherein the slabs of each sleeve are respectively stacked together to form a slug, the cross sectional area of the slug within the sleeve having quadrature symmetry.

29. The apparatus according to claim 28 wherein the slug within each sleeve is sectional, slug sections within a sleeve being longitudinally spaced apart by spacers.

30. The apparatus according to claim 28 wherein the longitudinal arrangement of slug sections differs from sleeve to sleeve.

31. The apparatus according to claim 27 wherein at least two of said plurality of rectangular permanent magnet slabs mounted in certain of said N sleeves are segmented in said length dimension to provide position adjustment of said at least two of said plurality of rectangular permanent magnet slabs in said length dimension.

32. A method of fabricating a magnetic bias assembly comprising the steps of:

configuring a plurality of sleeves;

disposing a plurality of rectangular permanent magnet slabs in each of said plurality of sleeves, each of said plurality of rectangular permanent magnet slabs having a length, width and thickness dimension and being stacked in the thickness dimension within each said sleeve, said plurality of rectangular permanent magnet slabs each having an anisotropic axis of magnetic orientation parallel to said thickness direction and stacked in a magnetically aiding relation in said thickness direction within each sleeve;

placing the plurality of sleeves parallel to each other than forming them around a curvilinear space to enclose a bore;

rotatably mounting said plurality of sleeves in said curvilinear space to arrange each of said plurality of sleeves rotatable about an axis parallel to the longitudinal axis of the sleeve; and

maximizing the magnetic field exhibited through at least a portion of said bore by rotation of said sleeves to a selected orientation.

33. The method of fabricating according to claim 32 additionally comprising the steps of introducing selected harmonics by employing segmented selected ones of said plurality of rectangular magnet slabs and axially positioning said segmented selected ones within said sleeves.

34. The method of fabricating according to claim 32 wherein said step of rotatably mounting is performed in a manner to produce quadrature symmetry.

35. The method of fabricating according to claim 32 wherein the slabs for each sleeve are stacked together to form a slug, the slug being segmented longitudinally within the sleeve with longitudinal spacers separating adjacent slug sections.