Water purification process

• US 4,808,287 A
• Filed: 12/21/1987
• Issued: 02/28/1989
• Est. Priority Date: 12/21/1987
• Status: Expired due to Fees

• Current Assignee: Ernst F. Hark
• Original Assignee: Ernst F. Hark
• Inventors: Hark, Ernst F.
• Primary Examiner(s): CINTINS, IVARS C
• Application Number:
  US07/136,406
• Time in Patent Office: 435 Days
• Field of Search: 210/638, 210/641, 210/652, 210/668, 210/669, 210/694, 210/137, 210/266, 210/900, 210/637, 210/257.2, 210/259, 204/182.5
• US Class Current: 210/637
• CPC Class Codes: B01D 2311/06 Specific process operations in the permeate stream
• CPC Class Codes: B01D 2311/14 Pressure control
• CPC Class Codes: B01D 2311/2603 Application of an electric field, different from the potential difference across the membrane
• CPC Class Codes: B01D 2311/2619 UV-irradiation
• CPC Class Codes: B01D 61/025 Reverse osmosis; Hyperfiltration
• CPC Class Codes: B01D 61/026 comprising multiple reverse osmosis steps
• CPC Class Codes: B01D 61/04 Feed pretreatment
• CPC Class Codes: B01D 61/422 Electrodialysis
• CPC Class Codes: B01D 61/58 Multistep processes
• CPC Class Codes: C02F 1/001 Processes for the treatment of water whereby the filtration technique is of importance C02F1/44 takes precedence; construction of filters in general B01D24/00 - B01D41/00
• CPC Class Codes: C02F 1/045 for obtaining ultra-pure water
• CPC Class Codes: C02F 1/283 using coal, charred products, or inorganic mixtures containing them
• CPC Class Codes: C02F 1/32 with ultraviolet light
• CPC Class Codes: C02F 1/42 by ion-exchange ion-exchange in general B01J
• CPC Class Codes: C02F 1/441 by reverse osmosis
• CPC Class Codes: C02F 1/469 by electrochemical separation, e.g. by electro-osmosis, electrodialysis, electrophoresis
• CPC Class Codes: C02F 1/4693 electrodialysis
• CPC Class Codes: C02F 1/68 by addition of specified substances, e.g. trace elements, for ameliorating potable water medicinal water A61K
• CPC Class Codes: C02F 2103/04 for obtaining ultra-pure water
• CPC Class Codes: C02F 9/00 Multistage treatment of water, waste water or sewage
• CPC Class Codes: Y10S 210/90 : Ultra pure water, e.g. conductivity water

Abstract

Potable water from a municipal water supply is treated to remove suspended solids, organic and inorganic dissolved solids, dissolved carbon dioxide gas and metal contaminants so as to produce ultra-pure water in the 16 megohm-cm³ and greater range. The process involves prefilteration of the water; activated carbon filtration; secondary guard filtration; double reverse osmosis treatment of the water. The process further involves the use of either an anion exchange or electrodialysis unit to remove further impurities from the water. A method for recycling part of the discharged water is also provided.

Claims

1. A method for purifying water comprising:

prefiltering the water by passing it through a one to five micron filter;

passing the water flowing from the prefiltration through an activated charcoal filter;

passing the water from the activated charcoal filter through a second activated charcoal filter;

passing the water from the second charcoal filter through a guard filter, the quard filter beinq one to five microns in size;

pressurizing the water from the guard filter to between 30 and 400 pounds per square inch by means of a first pressure pump;

subjecting the water leaving the first pressure pump to a first reverse osmosis treatment to remove dissolved particles;

pressurizing the water leaving the reverse osmosis treatment to between 0 and 400 pounds per square inch by means of a second pressure pump;

subjecting the pressurized water from the second pressure pump to a second reverse osmosis treatment; and

recycling the brine from the second reverse osmosis treatment to a ooint before the first reverse osmosis treatment.

2. The method of claim 1 further comprising the steps of subjecting the purified water from the second reverse osmosis treatment to electrodialysis to remove additional impurities and recvclino the brine from said electrodialvsis treatment to a ooint before the second osmosis treatment.

3. The method of claim 2 further comprising the steps of sterilizing the water using ultraviolet sterilization.

4. The method of treating water of claim 1, further comprising the step of treating the brine from the first reverse osmosis treatment to electrodialysis to remove impurities and returning the treated water from the electrodialysis treatment to the flow of the water teeatment system at a point before the first reverse osmosis treatment.

5. An apparatus for the treatment of water comprising:

a prefiltration system to remove sediments from the water;

a first activated charcoal filter which removes dissolved organic impurities from the water leaving the prefiltration system;

an activated charcoal guard filter through which the water from the first activated charcoal filter passes, the guard filter being designed to prevent water backwashed from the first activated charcoal filter from entering the filtration system;

a second guard filter which removes any activated charcoal particles from the water leaving the activated charcoal guard filter;

a first pressure pump which pressurizes the water from the second guard filter;

a first reverse osmosis unit which receives pressurized water from the first pressure pump and removes impurities from said water;

a second pressure pump which pressurizes the purified water, from the first reverse osmosis unit;

a second reverse osmosis unit which receives the purified water from the second pressure pump and removes additional impurities from the purified water; and

a brine recycle unit which recycles the brine from the second reverse osmosis unit to a point before the first reverse osmosis unit.

6. The apparatus of claim 5 further comprising a pressure regulation system which controls the pressure in said reverse osmosis units to prevent damage to the reverse osmosis units.

7. The apparatus of claim 5 further comprising a second brine recycling unit which recycles brine from the first reverse osmosis unit to a point just before the first reverse osmosis unit.

8. The apparatus of claim 7 further comprising an electrodialysis unit which cooperates with the second brine recycling unit to remove impurities from the recycled brine prior to the brine being reintroduced into the purification system.

9. The apparatus of claim 5 further comprising an electrodialysis unit which receives the treated water from the second reverse osmosis unit and removes additional impurities from the treated water and an electrodialysis recycling unit which recycles the brine from the electrodialysis unit to a point before the second reverse osmosis unit.