Cooling hollow fibre cross-flow separators

• US 4,816,160 A
• Filed: 11/17/1986
• Issued: 03/28/1989
• Est. Priority Date: 03/28/1985
• Status: Expired due to Fees

• Current Assignee: Memtec Ltd. (Danaher Corporation)
• Original Assignee: Memtec Ltd. (Danaher Corporation)
• Inventors: Kopp, Clinton V., Anderson, Eric W., Ford, Douglas L.
• Primary Examiner(s): Sever, Frank
• Application Number:
  US06/945,870
• Time in Patent Office: 862 Days
• Field of Search: 210/636, 210/798, 210/175, 210/198.1, 210/200, 210/203, 210/257.2, 210/321.1, 210/321.2, 210/321.3, 210/333.01, 210/411, 210/425, 210/427, 210/433.2, 134/21, 134/22.11
• US Class Current: 210/636
• CPC Class Codes: B01D 2321/04 Backflushing
• CPC Class Codes: B01D 2321/18 Use of gases
• CPC Class Codes: B01D 2321/2083 By reversing the flow
• CPC Class Codes: B01D 61/147 Microfiltration
• CPC Class Codes: B01D 63/031 Two or more types of hollow fibres within one bundle or within one potting or tube-sheet
• CPC Class Codes: B01D 65/02 Membrane cleaning or sterilisation ; Membrane regeneration

Abstract

A method of treating a heated liquid suspension, which entails:

(a) applying a liquid suspension to elastic, microporous, hollow fibres within a shell or housing, and

(b) discharging solids retained on or in the fibres by applying to the fibre lumens a pressurized reverse flow of gas, and wherein the hollow fibres are cooled prior to applying the reverse flow of gas.

Claims

1. A method of treating a heated liquid suspension which comprises:

(a) applying a heated liquid suspension to elastic, microporous, hollow fibres having a pore size of about 0.01 to 10 μ

m within a shell or housing,

(b) discharging solids retained on or in the fibres by applying to the fibre lumins a pressurized reverse flow of gas and rapidly cooling the hollow fibres prior to applying the pressurized reverse flow of gas sufficient to enable reverse flow of cleaning gas through the fibres.

3. The method according to claim 1 or 2, wherein the application of the pressurized gas includes the steps of:

(a) initially applying the gas at a pressure below the bubble point of the walls of the fibres so as to substantially displace liquid from the fibre lumens,

(b) substantially sealing the shell and the external surfaces of the fibres with a liquid,

(c) increasing the pressure of the gas above the bubble point of the walls of the fibres, and

(d) releasing the liquid seal to allow the trapped gas to escape substantially uniformly through the fibre walls.

4. The method according to claim 1 or 2, wherein the fibres are cooled by passing gas down the lumens of the fibres.

5. The method according to claim 1 or 2, wherein the fibres are cooled by applying gas to the exterior surface of the fibres.

6. The method according to claim 1 or 2, wherein the steps of the method are carried out as a continuous process utilizing repetitive cycles of solids retention, fibre cooling and solids discharge.

2. A method of concentrating solids in a liquid suspension using a filter comprising a plurality of hollow, each fibre having an outer surface, an inner surface defining a lumen, and a porous wall therebetween, comprising the steps of:

(i) applying the liquid suspension to the outer surface of the elastic, microporous, hollow fibres having a pore size of about 0.01 to 10 μ

m;

sufficient that;

(a) a portion of the liquid suspension passes through the walls of the fibres, thereby being drawn off as clarified liquid from the fibre lumens,

(b) at least a portion of the solids of said suspension are retained on or in the fibres or otherewise within the shell while the remaining solids not being retained are removed from the shell with the remaining portion of the liquid suspension,

(ii) terminating the flow of liquid suspension, rapidly cooling the hollow fibres and then applying to the fibre lumens a gas at a pressure sufficient to stretch substantially all of the pores followed by

(a) maintaining the flow of the gas at said pressure through the lumens for a time sufficient to drive the liquid from the pores having a bubble point below the pressure of the gas so as to wash out any solids retained in those pores and to substantially dislodge solids retained in the outer surface of the fibres sufficient that the washed out and dislodged solids are removed from the shell to an external collection point, and then

(b) reducing the pressure of the gas sufficient to enable reverse flow of cleaning gas through said fibres so that the pores will return to substantially their original size whereupon the gas is removed so that a portion of the liquid suspension passes through the walls of the fibres to be drawn off as a clarified liquid from the fibre lumens.

7. A concentrator for concentrating fine solids of a liquid feed suspension, comprising:

(i) a shell, having a liquid feed suspension inlet and outlet, and at least one clarified liquid discharge port;

(ii) a plurality of elastic, hollow, microporous, polymer fibres having a pore size of about 0.01 to about 10 μ

m within a shell or housing;

(iii) means for supplying pressurized feed suspension to the outside of the fibres, through the inlet;

(iv) means for withdrawing clarified liquid from the fibre lumens, through the clarified liquid discharge port;

(v) means for introducing a cooling medium to the fibres for rapidly cooling said fibres sufficient to enable reverse flow of cleaning gas through said fibres; and

(vi) means for introducing a pressurized gas under pressure to the fibre lumens to effect a transmembrane cleaning of the fibres, the pressure of the gas being sufficient to stretch substantially all of the pores of the fibres and the flow of the gas being sufficient to ensure that the gas will pass through the larger pores of the fibres to substantially dislodge solids retained therein and to wash the outer surface of the fibres to substantially remove solids therefrom to an external collection point.

8. The concentrator according to claim 7, which further comprises means for sealing the feed suspension in the shell upon displacement of liquid from the fibre lumens by the pressurized gas so that the gas is trapped in the lumens at a pressure above the bubble point of the fibre walls, and means whereby the pressurized gas is released substantially uniformly through the fibre walls.