Deodorization process for triglyceride oil

• US 4,838,997 A
• Filed: 11/13/1987
• Issued: 06/13/1989
• Est. Priority Date: 05/25/1983
• Status: Expired due to Term

• Current Assignee: NIRO A/S (GEA Group AG)
• Original Assignee: Atlas-Danmark A/S
• Inventors: Merk, Werner
• Primary Examiner(s): Lacey, David L.
• Assistant Examiner(s): MANOHARAN, VIRGINIA
• Application Number:
  US07/122,548
• Time in Patent Office: 578 Days
• Field of Search: 203/92, 203/40, 203/95, 203/DIG. 21, 203/91, 202/185.3, 202/182, 202/197, 202/205, 260/419, 260/428, 426/488
• US Class Current: 554/205
• CPC Class Codes: B01D 5/0012 Vertical tubes
• CPC Class Codes: B01D 5/0036 Multiple-effect condensation; Fractional condensation
• CPC Class Codes: C11B 1/108 after-treatment, e.g. of miscellae
• CPC Class Codes: C11B 3/14 with the use of indifferent gases or vapours, e.g. steam
• CPC Class Codes: Y10S 203/22 Accessories

Abstract

Process for deodorizing triglyceride oil comprises passing dry steam through the oil, the oil being at a temperature between 160° and 280° C. and under a pressure of between 0.1 to 8.0 mbar and condensing by indirect condenser means a vapor phase having a Reynolds number less than 2300 and comprising steam, volatile materials from the oil and less than 100 mg neutral oil per m³ of steam when measured under the conditions prevailing in the headspace above the oil. The condensate can be solid or liquid form. In either case the condensate can be readily removed from the condenser.

Claims

1. A process for deodorizing a triglyceride oil to produce a condensate without undesirable emulsions, comprising the steps of:

(a) heating the oil in a chamber to a temperature of about 160°

-280°

C. under a headspace pressure of about 0.1-8.0 mbar;

(b) passing dry steam through the heated oil to form a vapor including steam, volatile materials, and oil;

wherein said dry steam comprises steam in which the equilibrium vapor pressure of water is more than the pressure under which the steam is maintained prior to passage through the oil, and wherein the velocity of the steam is between about 1.7 and 16.0 kg/hr per m² cross-sectional area of headspace above the oil;

(c) maintaining the oil content in the vapor to about 0.01-100 mg/m³ ;

(d) increasing the pressure of the vapor to above about 10 mbar by mechanical pump means;

(e) directing the pressurized vapor into the inlet of an indirect condenser;

(f) passing the vapor through the indirect condenser along a flow path of decreasing cross-sectional area at a pressure less than about 60 mbar and at a substantially constant flow rate having a Reynolds number less than about 2300;

wherein the decrease is such that the ratio of the cross-sectional area of the inlet to the outlet of the indirect condenser is between about 50;

1 and 5;

1;

(g) indirectly condensating the vapor by passing coolant at a temperature of about 0°

-25°

C. along another separate flow path through the indirect condenser;

(h) collecting the resultant condensate from the indirect condenser; and

(i) exhausting the remaining vapor from the outlet of the indirect condenser.