Digestion and sterilization methods and apparatus

• US 4,877,624 A
• Filed: 04/19/1988
• Issued: 10/31/1989
• Est. Priority Date: 04/11/1985
• Status: Expired due to Term

• Current Assignee: CEM Global LLC
• Original Assignee: CEM Global LLC
• Inventors: Hargett, Wyatt P. Jr., Floyd, Terry S.
• Primary Examiner(s): Alvo, Steve
• Application Number:
  US07/185,250
• Time in Patent Office: 560 Days
• Field of Search: 422/113, 220/209, 222/402.21, 222/494, 137/496, 137/468, 137/522, 137/859, 426/241, 426/234, 426/243, 99/337, 99/338, 99/359, 99/369, 219/10.55 R, 219/10.55 M
• US Class Current: 426/241
• CPC Class Codes: A23L 3/10 by heating materials in packages which are not progressively transported through the apparatus
• CPC Class Codes: B01J 19/126 Microwaves
• CPC Class Codes: B01J 2219/1209 Features relating to the reactor or vessel
• CPC Class Codes: B01J 2219/1215 Single reactor
• CPC Class Codes: B01J 3/002 Component parts of these vessels not mentioned in B01J3/004, B01J3/006, B01J3/02 - B01J3/08; Measures taken in conjunction with the process to be carried out, e.g. safety measures
• CPC Class Codes: F16K 17/02 opening on surplus pressure on one side; closing on insufficient pressure on one side check valves F16K15/00
• CPC Class Codes: H05B 6/6408 Supports or covers specially adapted for use in microwave heating apparatus
• CPC Class Codes: Y10T 137/7876 With external means for opposing bias

Abstract

A valve that opens and closes in response to changes in the physical environment of the valve. This valve is particularly suited as a relief valve in a microwave system-based, closed vessel digestion procedure. This valve includes a pressure-deformable, resilient wall member having a fluid vent port, and an obstructing member that cooperates with the wall member to open and close the valve.

Also provided is a lidded vessel employing this improved valve, an apparatus that includes a microwave system and this lidded vessel, and methods using this improved valve.

Claims

1. Digestion or sterilization apparatus which comprises a microwave system comprising a microwave heating means, and a lidded vessel comprising a container and a self-opening and self-closing temperaturesensitive valve assembly, said valve assembly being made entirely of microwave radiation transparent, thermoplastic material, and said valve assembly comprising a temperaturesensitive, pressure-deformable, resilient wall member located for direct contact with a hot gas when said lidded vessel is closed, said wall member having an outlet port, and obstructing means normally engaged to block outflow through said outlet port such that said lidded vessel is closed, said wall member being only dome-shaped or planar;

wherein said valve assembly is structured so that internal fluid pressure impinging on said wall member, causes outward bulging of said wall member, the pressure-deformed wall member being domeshaped, wherein outflow through said outlet port occurs in response to a certain internal fluid pressure impinging on and deforming said wall member; and

wherein said valve assembly lacks a coil spring member.

2. The apparatus of claim 1, wherein said wall member is an integral part of the vessel lid.

3. The apparatus of claim 1, wherein said container is formed of a thermoplastic material.

4. The apparatus of claim 1, wherein said microwave system comprises a corrosion resistant chamber, a corrosion resistant exhaust system capable of providing high volume air flow through the chamber, means for absorbing excess reflected radiation, and computer-controlled variable power means.

5. The apparatus of claim 1, wherein said wall member is dome-shaped when said lidded vessel is closed.

6. The apparatus of claim 1, wherein said wall member comprises means for manual relief of internal pressure.

7. A high pressure, closed vessel digestion method comprising

(a) introducing sample to be digested, and an amount of a digesting agent suitable for effecting digestion into a thermoplastic container capable of withstanding high internal pressure;

(b) placing onto said container, a self-opening and self-closing temperature-sensitive valve assembly, said valve assembly being made entirely of microwave radiation transparent, thermoplastic material, and said valve assembly comprising a temperature-sensitive, pressure-deformable, resilient wall member located for direct contact with a hot gas when said lidded vessel is closed, said wall member having an outlet port, and obstructing means normally engaged to block outflow through said outlet port such that said container is closed, said wall member being only dome-shaped or planar;

wherein said valve assembly is structured so that internal fluid pressure impinging on said wall member, causes outward bulging of said wall member, the pressure-deformed wall member being dome-shaped, wherein outflow through said outlet port occurs in response to a certain high internal fluid pressure impinging on and deforming said wall member; and

wherein said valve assembly lacks a coil spring member;

(c) digesting said sample by applying microwave energy to the contents of the closed container, wherein a high internal fluid pressure is produced that causes outward bulging of said wall member yet said valve assembly remains closed, said high internal fluid pressure being less than said certain high internal fluid pressure; and

(d) recovering the digested sample from said container.

8. A method for producing a sterile object in a sealed container, said method comprising

(a) introducing an object and water into a container;

(b) placing onto said container, a self-opening and self-closing temperature-sensitive valve assembly, said valve assembly being made entirely of microwave radiation transparent, thermoplastic material, and said valve assembly comprising a temperature-sensitive, pressure-deformable, resilient wall member located for direct contact with a hot gas when said lidded vessel is closed, said wall member having an outlet port, and obstructing means normally engaged to block outflow through said outlet port such that said container is closed, said wall member being only dome-shaped or planar;

wherein said valve assembly is structured so that internal fluid pressure impinging on said wall member, causes outward bulging of said wall member, the pressure-deformed wall member being dome-shaped, wherein outflow through said outlet port occurs in response to a certain internal fluid pressure impinging on and deforming said wall member; and

wherein said valve assembly lacks a coil spring member;

(c) sterilizing said object by applying microwave energy to the contents of the closed container, wherein an internal pressure is produced that causes outward bulging of said wall member; and

(d) cooling said container.

9. The method of claim 8, wherein said object is a foodstuff, and a canned food is produced.