Method for manufacturing filler-containing paper

• US 4,889,594 A
• Filed: 12/03/1987
• Issued: 12/26/1989
• Est. Priority Date: 12/03/1986
• Status: Expired due to Fees

• Current Assignee: MO OCH Domsjo AB
• Original Assignee: MO OCH Domsjo AB
• Inventors: Gavelin, Gunnar
• Primary Examiner(s): Chin, Peter
• Application Number:
  US07/128,653
• Time in Patent Office: 754 Days
• Field of Search: 162/183, 162/216, 162/123, 162/129, 162/149, 162/190, 162/189, 162/158, 162/130, 162/162, 162/181.1
• US Class Current: 162/123
• CPC Class Codes: D21H 23/16 Addition before or during pulp beating or refining disintegrating fibrous raw materials in mills in the presence of chemical agents D21B1/16; methods of beating D21D1/02; methods of refining D21D1/20
• CPC Class Codes: D21H 23/20 Apparatus therefor

Abstract

The invention relates to a method and apparatus for manufacturing paper or like products which contains retention agent and inorganic filler. The retention and technical properties of the paper are enhanced by coflocculating the filler with a cellulosic material having a large specific surface area (fine pulp) prior to introducing floc suspension into the stock, and by subjecting the flocs to a floc size-controlling shearing process in a particular reaction vessel to produce flocs that have a mean particle size within the range of 2-4 mm. The particular reaction vessel used herefor incorporates a mixing zone, a flocculation zone, separator means located between the mixing zone and flocculation zone, a shearing zone and a sedimentation zone.

Claims

1. A method of manufacturing paper using a paper machine in which stock is fed to a headbox of said machine to form the paper, said method comprising the steps of:

introducing filler and pulp containing a high proportion of pulp fines into a reaction vessel;

mixing said filler with said pulp containing a high proportion of pulp fines in said reaction vessel to form a resultant mixture;

admixing the resultant mixture with retention agent in said reaction vessel to form flocs which contain the filler and said pulp containing a high proportion of pulp fines (coflocculation);

subjecting the flocs to a size-controlling shearing process in said reaction vessel for breaking down large flocs and agglomerating small flocs to form flocs having a mean particle size in a range of 2 to 4 mm; and

feeding the flocs to the stock upstream of the headbox, wherein the size-controlling shearing process is effected in a shearing zone in the reaction vessel in which the floc suspension is imparted with a helical rotational motion in the flow direction thereby engendering a controllable shearing effect between adjacent layers at varying distances from the center of the rotation.

2. A method according to claim 1, wherein the mean particle size is caused to lie in the range of 2.5-3.5 mm.

3. A method according to claim 1, wherein prior to being charged to the stock the suspension of said flocs containing filler and fine pulp is thickened gravitationally, whereupon floc-free liquid is withdrawn from the lower part of the vessel and returned to the fine pulp.

4. A method according to claim 1, wherein the shearing effect is engendered with the aid of an eccentrically located stirrer means.

5. A method according to claim 1, wherein the size-controlling shearing effect is effected by withdrawing coflocculated suspension from a flocculation zone in the reaction vessel, circulating the coflocculated suspension through a branch pipe connected in parallel with the reaction vessel, and returning the coflocculated suspension to the shearing zone by injecting said suspension tangentially into said zone, and controlling the floc size of the particles by varying the rate of suspension flow in said branch pipe.

6. A method according to claim 1, wherein fine pulp and filler are mutually combined prior to being introduced into a mixing zone in the reaction vessel.

7. A method according to claim 1, wherein retention agent is introduced into the flocculation zone of the reaction vessel.

8. A method according to claim 1, wherein two or more mutually different retention agents are introduced into the flocculation zone.

9. A method according to claim 1, wherein non-reacted excess retention agent is recycled.

10. A method according to claim 5, wherein a fibre concentration in the flocculation zone of the reaction vessel is maintained within the range of 0.5-3.0% by weight.

11. A method according to claim 1, wherein size is added to the coflocculated particles of fine pulp (fraction) and filler in a sedimentation zone in the reaction vessel.

12. A method according to claim 11, wherein size solution is first added to the coflocculated particles in the sedimentation zone and then a size fixating agent is added thereto.

13. A method according to claim 1, wherein dye solution and dye fixating agent is added to the coflocculated particles of fine pulp (fraction) and filler in a sedimentation zone in the reaction vessel.

14. A method according to claim 1, wherein white water from the paper machine is introduced into the fine pulp prior to said coflocculation process.

15. A method according to claim 1, wherein at least one flow of coflocculated filler and fine pulp is delivered to at least one headbox in a paper machine provided with multiple headboxes.

16. A method according to claim 5, wherein a fiber concentration in the flocculation zone of the reaction vessel is maintained within a range of 1.0-3.0% by weight.

17. A method according to claim 14, wherein the white water is from a first section of the wire.

18. A method according to claim 1, wherein said pulp has a freeness in a range of 40 to 100 ml CSF (Canadian Standard Freeness).

19. A method according to claim 1, wherein said filler and pulp containing a high proportion of pulp fines are combined prior to introduction into said reaction vessel.