Trapping assembly

• US 4,892,654 A
• Filed: 03/15/1989
• Issued: 01/09/1990
• Est. Priority Date: 03/15/1989
• Status: Expired due to Fees

• Current Assignee: Hewlett-Packard Company (HP Inc.)
• Original Assignee: Hewlett-Packard Company (HP Inc.)
• Inventors: Nickerson, Mark A.
• Primary Examiner(s): Therkorn, Ernest G.
• Application Number:
  US07/324,353
• Time in Patent Office: 300 Days
• Field of Search: 210/635, 210/656, 210/659, 210/198.2, 55/67, 55/386
• US Class Current: 210/198.2
• CPC Class Codes: B01D 15/40 using supercritical fluid as mobile phase or eluent
• CPC Class Codes: G01N 2030/085 using absorbing precolumn
• CPC Class Codes: G01N 30/02 Column chromatography
• CPC Class Codes: G01N 30/08 using an enricher
• CPC Class Codes: G01N 30/20 using a sampling valve
• CPC Class Codes: G01N 30/32 of pressure or speed G01N30/36 takes precedence

Abstract

Disclosed is a chromatographic trapping assembly suitable for use with supercritical fluids. The apparatus includes means suitable for electronic control of the expansion of pressurized fluid through an orifice into a fluid trapping assembly using an axially movable column to regulate fluid through the orifice.

Claims

1. In a fluid trapping assembly for use with fluid systems having a column for removing and collecting a solute component of said fluid, the combination comprising:

a fluid entrance located near the base of said column and a fluid outlet located near the top of said column,

a valve chamber surrounding the base of said column having a fluid inlet orifice for admitting fluid into said chamber,

a column seal surrounding said column and forming the upper part of said chamber, said seal being in sealing engagement with said column,

orifice engagement means attached to the base of said column adapted to engage said fluid inlet orifice and restrict the flow of fluid into said chamber and through said column,

axial movement means adapted to engage said column and move said orifice engagement means into and out of engagement with said orifice.

2. The assembly as defined in claim 1 wherein said axial movement means is driven by a solenoid.

3. The assembly as defined in claim 1 wherein said orifice engagement means is a conical projection extending from the base of said column.

4. The assembly as defined in claim 3 wherein the angel of the cone of said conical projection is between about 30 and 120 degrees.